防水墙技术初探

防水墙技术是一种防止内部信息向外扩散的技术。论文给出了防水墙的定义及功能特性,并通过对防水墙系统WaterBox的介绍分析,探讨了利用防水墙技术构筑内网信息安全的可行性及发展趋势。     

Ring‐opening polymerization of D,L‐lactide by rare earth 2,6‐dimethylaryloxide

Ring‐opening polymerization of D,L ‐lactide (LA) has been successfully carried out by using rare earth 2,6‐dimethylaryloxide (Ln(ODMP)₃) as single component catalyst or initiator for the first time. The effects of different rare earth elements, solvents, monomers and catalyst concentration as well as polymerization temperature and time on the polymerization were investigated. The results show that La(ODMP)₃ exhibits higher activity to prepare poly(D,L ‐lactide) (PLA) with a viscosity molecular weight of 4.5 × 10⁴ g mol^?1 and the conversion of 97 % at 100 °C in 45 min. The catalytic activity of Ln(ODMP)₃ has following sequence: La > Nd > Sm > Gd > Er > Y. A kinetic study has indicated that the polymerization is first order with respect to both monomer and catalyst concentration. The apparent activation energy of the polymerization of LA with La(ODMP)₃ is 69.6 kJ mol^?1. The analyses of polymer ends indicate that the LA polymerization proceeds according to ‘coordination–insertion’ mechanism with selective cleavage of the acyl–oxygen bond of the monomer. Copyright © 2004 Society of Chemical Industry     

对称配筋小偏心受压构件的截面设计

对小偏心受压构件在对称配筋情况下的截面配筋计算，提出用最佳一次逼近多项式简化基本公式，直接按二次方程求解ξ的近似方法，具有精度高，相对误差小，计算方便等优点，可供工程设计人员参考。     

Thomson scattering diagnostic systems in the ITER divertor

A diagnostic array has been developed for studying the operating modes of the divertor in the ITER tokamak-reactor using the Thomson scattering technique. The aim of this study is to measure the spatial profiles of the electron temperature and density. The structure of the diagnostic setup was selected on the basis of a classical diagnostic geometry and the high-resolution LIDAR system, which provide access to different regions of the divertor plasma. A severe radiation environment, limited access to the plasma in the ITER divertor, and a high-dust environment (the divertor plate erosion material) in the divertor volume pose many problems for performing diagnostics under unique conditions having no analogs in the tokamaks that are now in operation. Different methods for protecting optical surfaces from plasma-enriched deposition are proposed and analyzed. The efficiency of these methods has been demonstrated in bench tests. The concept of laser and detector systems and diffraction polychromators capable of operating at different electron temperatures with a lower limit of 1 eV, has been justified and approved.     

大窝山隧道进口围岩快速掘进施工组织与管理

结合工程概况及工程特点,从机械设备配置、劳动力组织、现场管理等方面介绍了大窝山隧道进口Ⅱ级,Ⅲ级围岩段的快速掘进施工组织与管理措施,为类似隧道的快速掘进施工组织与管理提拱了相关经验.     

PURIFICATION AND PROPERTIES OF TRANSGLUTAMINASE FROM STREPTOVERTICILLIUM MOBARAENSE

Transglutaminase (TGase) was separated from the culture broth of an isolated strain of Streptoverticillium mobaraense. The crude enzyme was prepared by centrifugation, ultrafiltration, precipitation by alcohol, centrifugation and freeze‐drying. The yield after these processes was 65–70%. Then the enzyme was purified to homogeneity by chromatography on CM‐cellulose and Sephadex G‐75 on which the yields were about 70% and 80%, respectively; the purified folds reached 2.5–4.7 and 1.08–2.06, respectively. The molecular weight of this TGase was 39,500–40,100 Da by gel filtration chromatography. Optimum enzyme activity was observed in the pH range of 5.0–7.0, and it was maintained stable at 20–40C. The optimal temperature and pH was 52C and 6.0, respectively. At 1 mM and 5 mM metal ion or inhibitors concentration, TGase activity was strongly inhibited by Zn²⁺ and NEM, and not affected obviously by Ba²⁺, Ca²⁺, Co²⁺, Cu²⁺, Fe²⁺, Fe³⁺, Mg²⁺, Mn²⁺, Na⁺ as well as PMSF and EDTA. The effects of these additions on this TGase were compared with those of other microbial TGases.     

固有频率在车轮设计有限元分析中的应用

以三维软件进行车轮造型,用CAD软件建立固有频率分析数学模型,对车轮固有频率进行分析和处理.结合其他试验的分析,对车轮进行优化设计.