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101.
Biomimetic synthesis of spherical nano-hydroxyapatite in the presence of polyethylene glycol 总被引:1,自引:0,他引:1
Spherical nano-hydroxyapatite (nano-HA) was synthesized successfully by a biomimetic method using Ca(NO3)2·4H2O and (NH4)3PO4·3H2O as reagents in the presence of polyethylene glycol (PEG). The crystalline phase, microstructure, chemical composition, and morphology of the obtained samples were characterized by X-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), and transmission electron microscopy (TEM). The results show that spherical nano-HA with diameter of 30–50 nm can be synthesized in the presence of a certain concentration (2–6%) of PEG. The crystallinity of HA powder synthesized in the presence of PEG was higher than that synthesized in the absence of PEG, but the crystallinity of HA reduced with increasing the concentration of PEG. The electrical conductivity (EC) of the solution revealed that PEG reduced the transfer rate of Ca2+ in the process of HA crystallization, indicating the interaction between PEG and HA. The possible mechanism of formation spherical nano-HA was discussed. 相似文献
102.
本文阐述对贵冶动力车间二期反渗透进行改造的成功实践 ,主要从反渗透系统设计、反渗透系统中容易出现的问题及解决方法等进行介绍。 相似文献
103.
Ying‐Hung So 《Polymer International》2006,55(2):127-138
Poly(2,4‐dimethyl‐1,4‐phenylene oxide) (PPO), poly(benzo[1,2‐d:5,4‐d′]bisoxazole‐2,6‐diyl‐1,4‐phenylene) (PBO) and poly(benzo[1,2‐d:4,5‐d′]bisthiazole‐2,6‐diyl‐1,4‐phenylene) (PBZT), which are polymers with extended conjugated structures, undergo a self‐sensitized photo‐induced electron‐transfer reaction. A second component is not required. This article presents many similar observations on these polymers when they are exposed to light and evidence to support the proposed photo‐induced electron‐transfer mechanism. Methods to stabilize these polymers against photo‐oxidation are also described. Workers investigating other conjugated polymeric systems may find the experimental methods, observations and polymer stabilization approaches discussed in this review useful. Copyright © 2005 Society of Chemical Industry 相似文献
105.
A two‐phase flow CFD model using the volume of fluid (VOF) method is presented for predicting the hydrodynamics of falling film flow on inclined plates, corresponding to the surface texture of structured packing. Using the proposed CFD model the influence of the solid surface microstructure, liquid properties and gas flow rate on the flow behavior was investigated. From the simulated results it was shown that under the condition of no gas flow the liquid flow patterns are dependent on the microstructure of the plates, and proper microstructuring of the solid surface will improve the formation of a continuous liquid film. It was also found that liquid properties, especially surface tension, play an important role in determining the thin‐film pattern. However, there are very different liquid film patterns under the action of gas flow. Thinner liquid films break easily, but thicker liquid films can remain continuous even at higher gas flow rates, which demonstrates that all factors affecting the liquid film thickness will affect the liquid film patterns under conditions of counter‐current two‐phase flow. 相似文献
106.
Ming-yan Liu Wen Leng Ai-hong Qiang 《Chemical Engineering and Processing: Process Intensification》2008,47(12):2066-2075
In this work, the instantaneous data of inner wall temperatures obtained at given axial positions but for different heated tubes or at various axial positions but at the same heated tube in a tube-bank fluidized bed evaporator with a vapor–liquid–solid external natural circulation flow were analyzed by employing linear and nonlinear time series analysis methods, including correlation dimension and Kolmogorov entropy analyses besides time domain, power spectrum and autocorrelation analyses. It is found that nonlinear characteristics of the wall temperature time series vary with spatial position in the evaporator at given operation conditions, and thus the multi-phase flow boiling behavior. However, the signals obtained at given axial position but different heated tubes in the evaporator exhibit more similar nonlinear evolution behavior, and those measured in the same heated tube but at different axial heights in the evaporator undergo more distinct nonlinear dynamic behavior. Multi-scale phenomena in different spatial positions are also found and discussed. These transient aspects of inner wall temperatures are closely related to the average holdup of solid particles and motion of vapor bubbles in vapor–liquid–solid flow. These results can provide some valuable information on the system modeling and controlling from the point of view of nonlinearity. 相似文献
107.
中式快餐发展战略与人才培养 总被引:2,自引:0,他引:2
本文讨论了我国快餐业的发展现状,进一步研究中式快餐发展战略,以及中式快餐业有关人才的培养现状和满足发展各类人才培养途径。 相似文献
108.
In CFD simulation of diesel combustion, the predictive capabilities of the spray model play the most important role. Consequently, under the strict guidelines of the V&V, a method to adjust parameters of diesel spray model WAVE to accompany with the in-cylinder physical progress has been investigated in this paper. Moreover, the simulation of the spray has been validated by high-speed photography experiments and verified by the equation proposed by Hiroyasu. Finally, a modified setup for the WAVE spray model has been proposed and applied in the spray and combustion simulation for Deutz1013 diesel in different engine speed. 相似文献
109.
The long‐term thermal‐oxidative aging behavior of polyamide 6 (PA6) was studied by comparison with the stabilized sample in this work. The variation of mechanical properties of the pure and the stabilized samples of PA6 with aging time at 110°C, 130°C, and 150°C were investigated, respectively. The aging mechanism of PA6 under heat and oxygen was studied in terms of the reduced viscosity, crystallization behavior, dynamic mechanical behavior, and chemical composition through the methods of polarized light microscopy (PLM), differential scanning calorimetry (DSC), dynamic mechanical analysis (DMA), X‐ray photoelectron energy spectrum (XPS), and so on. The results indicated that at the initial stage of aging, the molecular crosslinking reaction of PA6 dominated resulting in the increase of the mechanical strength, reduced viscosity, and the glass transition temperature of the sample. And the molecular degradation dominated in the subsequent aging process resulting in the decrease of the melting temperature, the increase of the crystallinity, and the formation of the oxides and peroxides products. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献
110.
Biphenol monoacrylate (AL) was combined with a traditional hindered phenolic‐based binary antioxidant system to form a ternary stabilization system for the purpose of further improving the thermal–oxidative stability of polyamide 6 (PA6). The thermal stabilization effect of the antioxidant AL on PA6 was studied in terms of the reduced viscosity, the chemical structure, the yellow index, and the mechanical properties. The results showed that the antioxidant AL, with the proper chemical structure, could improve the thermal stability of PA6 effectively through a unique bifunctional stabilizing mechanism. The interaction of the molecules of PA6 with the antioxidant AL was investigated. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献