含氯取代基的聚间苯二甲酰间苯二胺的合成与表征

以 2 ,5 -二氯对苯二甲酰氯作为第三单体 ,将其与间苯二甲酰氯、间苯二胺在N ,N -二甲基乙酰胺中进行低温溶液共缩聚反应 ,合成了含氯取代基的聚间苯二甲酰间苯二胺。研究了单体摩尔浓度、反应初始温度、叔胺添加剂种类、第三单体用量等对共聚物相对分子质量的影响 ,并用红外光谱、热重分析等方法对共聚物进行了表征。     

浅析2020年前美军事战略重点的转变--从装备发展看美国军事战略重点可能的变化

美国21世纪前期的军事战略重点将是争夺外空优势，夺取制天权和制信息权。分析了美国夺取外空优势的原因，及其为夺取外空优势在国家政策、航天发展和技术准备等方面采取的措施。     

双河油田特高含水后期开发阶段注采结构调整的实践与应用

针对双河油田的注采结构的现状及特征,通过近几年来在注采结构调整方面的实践与应用,总结出了油田在特高含水后期开发阶段,实现油田控水稳油目标的途径和方法,注水结构调整主要是结合地质特点,减少欠注层段,减少和控制不合理超注井层段和改善吸水剖面;在采液结构调整上,控制高含水层段的注入,加强中低渗透层段的注入,封堵高渗透、高水淹干扰层段,解放动用较差的中低渗透层段,改善平面上采出不平衡的状况。通过实施注采结构调整,双河油田在特高含水后期实现了高效开发。     

MB8镁合金薄板的搅拌摩擦焊

针对我国航空航天工业常用的MB8镁合金。采用搅拌摩擦焊工艺进行焊接，对其焊缝的成形特点、组织特征和力学性能进行分析。结果表明，采用搅拌摩擦焊焊接镁合金效果良好。     

模糊数学识别火山岩岩性

针对火岩地层岩性识别成功率低的状况，应用模糊数学原理，建立模糊数学识别火山岩岩性模式，识别和划分火山岩地层岩性，以便进一步深入研究火山岩油气藏储层，选择8个反映火山岩岩性测井参数，确定阈值；利用所建立的火山岩岩性识别模式，对火山岩岩性进行分类；依据最大隶属原则，识别火山岩岩性，应用实地研究资料，识别10种火山岩岩性，并与岩心鉴定统计分析结果对比，一致性达85％。表明该方法识别火山岩岩性精度较高，在地质上具有很好的应用前景。     

隔震结构在省防震减灾中心大楼工程中的应用

结合工程实例介绍了隔震结构在工程设计中的应用     

一种语音混沌保密通信方案的研究与硬件实现

在硬件实验研究的基础上，建立一种环形蔡氏电路，提出用环蔡氏电路实现语音混沌保密通信的一种闭环逆系统方案，其特点是利用环形蔡氏电路的单向耦合原理，通过反馈的方法形成一个包括有用信号在内的极联闭合环路，从而实现改善端与接收端之间混沌系统的严格同步而不受有用信息调制的影响。理论分析与硬件实验结果证明，该方案同现有的其它混沌通信方案相比较，具有非线性失真小、保真度高的优点，完全能够满足传送语音信号的要求。     

用迭代法消除数字图像放大后的模糊

用迭代法对数字图像经过插值放大后产生的模糊问题进行了研究，把数字图像插值放大造成的模糊看成是点扩散函数与清晰图像卷积的结果，根据插值算法可以得到点扩散函数，由于数字图像解卷积是典型的解线性方程组的问题，用雅可比（Jacobi）迭代法得到了很好的结果。与频谱空间变换的方法相比，迭代法没有分母为0的问题和空间变换过程造成的舍入误差。     

Discrete singular convolution and its application to the analysis of plates with internal supports. Part 2: Applications

Part 2 of this series of two papers presents the applications of the discrete singular convolution (DSC) algorithm. The main purpose of this paper is to explore the utility, test the accuracy and examine the convergence of the proposed approach for the vibration analysis of rectangular plates with internal supports. Both partial internal line supports and complex internal supports are considered for 21 square plates of various combinations of edge support conditions. The effects of different size, shape and topology of the internal supports and different boundary conditions on the vibration response of plates are investigated. The partial internal line supports may vary from a central point support to a full range of cross or diagonal line supports. Several closed‐loop supports, such as ring, square and rhombus, and their combinations are studied for complex internal supports. Convergence and comparison studies are carried out to establish the correctness and accuracy of the DSC algorithm. The DSC results are compared with those in the available literature obtained by using other methods. Numerical results indicate that the DSC algorithm exhibits controllable accuracy for plate analysis and shows excellent flexibility in handling complex geometries, boundary conditions and support conditions. Copyright © 2002 John Wiley & Sons, Ltd.     

Trace elements in particles of motor vehicle exhaust in Shanghai

A nuclear microprobe with high spatial resolution and high analytical sensitivity was applied to analyze trace elements,especially lead,in vehicle exhaust of Shanghai city.The result shows that the chemical composition and its corresponding x-ray relative intensity are different among different vehicle exhausts.There are many kinds of metal elements in particles of vehicle exhaust.most are harmful to people,such as Ti,Cr,Mn,Pb,etc.We found that the lead concentration was 6820μg/g and the bromine concentration was 5300μg/g in the exhaust from Santana using leaded gasoline(SULG).which is higher than any other kinds of vehicle exhausts.We have also detected the minimum lead in the particles of unleaded gasoline and its content varies from one to another.Its mean concentration was 450μg/g and the highest reached 6210μg/g.The unleaded gasoline‘s Pb existed in the whole particle while the leaded gasoline‘s enriched in the surface of the particle and was more harmful to the human beings.