Preparation and photocatalytic activity of nano-TiO2 codoped with fluorine and ferric

Nano-F /Fe^3＋/TiO2 particles were prepared by hydrolysis of tetrabutyl titanate in a mixed CF3COOH-Fe（NO3）3-H2O solution. The photocatalytic decomposition of methylene blue in aqueous solution was used as a probe to evaluate their photocatalytic activities. The powders were characterized by X-ray diffraction （XRD）, energy dispersion X-ray spectrum （EDS） and Brunauer-Emmett-Teller （BET） surface area analysis. The results show that F- and Fe^3＋ are doped into TiO2. The F^- and Fe^3＋ doping can help to enhance the nano-TiO2 photocatalytic activity greatly. The appropriate codoping conditions for F-Fe are n（F）/n（TiO2）=2%, n（Fe）/n（TiO2）=0.05%, and the degradation rate of methylene blue at l h is improved from 73.2% to 87.5%. The codoped nano-F /Fe^3＋/TiO2 particles have higher BET specific surface area, smaller crystallite size and higher photocatalytic activity than those of undoped TiO2 particles.     

高耐蚀性热镀锌板的钝化处理工艺探讨

介绍了热镀锌板钝化膜的形成机理 ;针对攀钢热镀锌板出现白锈、黑斑等问题 ,分析了钝化液pH值、添加剂及操作条件对钝化膜质量的影响 ,同时提出了改进热镀锌板耐蚀性能的措施     

远场涡流技术检测带翼片管的研究

远场涡流检测对高导电管的管壁上的缺陷非常敏感，具有透壁性。探讨应用远场涡流技术检测带翼片(散热片或金属隔板组件)钢管的有关问题，分析了管外翼片对远场涡流的耦合特性和缺陷信号的影响，得出了翼片响应信号与缺陷信号的关系及缺陷信号的提取方法。     

A novel binder and binder extraction method for powder injection molding of tungsten cemented carbide

1　INTRODUCTIONPowderinjectionmolding (PIM ) ,whichisde rivedfromplasticinjectionmolding ,isakindofnet shapepowdermetallurgyformingprocess[13] .Com bininghigh partcomplexitywithhigh productionquantities ,itsupplementstheestablishedprocesseslikediecompaction ,machiningandinvestmentcasting[4 6 ] .Comparingtoconventionalpressing/sinteringprocess,thePIMhasgreattechniqueandcostadvantagesforthepro ductionofcementedcarbidecomponentswithcomplexshapes[7,8] .Sincehydraulicpressureisappliedduringi…     

有效优化扩展I/O点提高PLC系统的性价比

在利用PLC对复杂化的设备进行控制及改造时,常常遇到PLC的I/O点数不够用的情况。本文从软件和硬件两方面介绍了PLC在实际应用中优化扩展I/O点的几种常规有效方法,这些方法可大大降低硬件成本,在机床电气控制及改造中具有很高的实用价值。     

高强度ZL205A合金大型铸件"白点"偏析研究

对ZL205A合金某大型铸件进行探伤检测,在底片上发现了白色点状偏析组织(以下简称“白点”偏析)。铸造工艺调整以及热处理不能使之减轻或消除。文中对ZL205A合金白点偏析进行研究,测试了偏析组织的力学性能,分析了偏析组织的微观形貌及化学成分,并探讨了其形成机理及防止措施。     

摆动式TIG焊焊缝跟踪技术

介绍以弧压为传感信号的摆动式TIG焊焊缝跟踪技术。硬件设计方面，采用两级滤波的方法，前级主要用来保护控制电路，后级主要用来滤除杂波。软件处理方面，针对搭接TIG焊的特点，采用摆动焊接方法，利用积分比较法，实现了焊缝的自动跟踪；提出加权处理的方法，对积分比较法进行修正，进一步保证了跟踪的实现，提高了跟踪精度。试验证明，该技术控制可靠，焊缝跟踪效果好。     

我国典型地区大气腐蚀性的综合评价

运用模糊综合评价方法,选择合适的隶属函数,根据国际标准化组织ISO9223大气腐蚀性评价分级标准和我国大气腐蚀网站的腐蚀数据,对我国典型地区的大气腐蚀性进行了综合评价,其结果与单因素评价进行了对比。综合评价结果能较好地反映我国典型地区大气环境的腐蚀性。     

Preparation ofAZ91 alloy by powder metallurgy method

Magnesium alloy AZ91 was prepared by powder metallurgy method, and the effect of sintering temperature on the densities and microstructures of the alloys was investigated. The results show that tight control of the sintering temperature within a narrow range around the liquidus level generates structures with high integrity and reduces some of the disadvantages caused by the higher temperatures. The matrix consists of α-Mg grains/cells surrounds by discontinuous precipitates of Mg17Al12 intermetallics which are normally located at the grain boundaries and triple junction.     

铝铁合金的研究进展与应用状况

综述了Al-Fe合金的国内外研究现状，阐述了共晶、过共晶铝铁合金及其在快速凝固条件下的凝固特点，概述了添加Ca、Mg、Mn、RE等微量元素及采用热速处理、电流处理、交变磁场、超声振动等工艺条件对Al-Fe合金微观组织的影响规律，叙述了目前Al-Fe合金的应用状况，并对铝铁合金的研究及应用前景进行了展望。