负载型固体碱催化合成亚苄基丙酮

研究了用固体碱 KOH/Al_2O_3催化合成苯叉丙酮,确定了合成的最佳工艺条件:n(苯甲醛)∶n(丙酮)=1∶4.催化剂用量2g,催化剂最佳负载量12mmol/g,反应温度40～45℃,反应时间为3h,产率达88%以上。     

苏北-南黄海盆地构造演化

苏北及南黄海盆地是由多期、多类盆地叠加的复合残留盆地,地质概况基本相似,成因演化近同,自元古界下扬子板块形成后,主要经历了古-中生代地台、中生代前陆盆地、走滑拉分盆地时期以及新生代断陷、坳陷盆地时期.在古生代-中生代发展过程中是一个整体,晚白垩世盆地演化出现分化,发育伸展盆地群,形成一系列叠置在中、古生代盆地之上的箕状断陷,箕状断陷的发育及分布明显受中-古生界内部先存逆冲断裂的控制.     

新的启迪

说点心里的话，建筑设计对青年人来讲是一条漫长的道路。建筑是一个载体，有精神一面，也有物质一面。有些建筑师拿着模型或未建成的设计来炒作，为了求名，生怕别人不知道。这对个人是小事，但若贻误了青年学子，那就是不可取的。     

Structured optimal and robust control with multiple criteria: a convex solution

In this paper, the design of controllers that incorporate structural and multiobjective performance requirements is considered. The control structures under study cover nested, chained, hierarchical, delayed interaction and communications, and symmetric systems. Such structures are strongly related to several modern-day and future applications including integrated flight propulsion systems, platoons of vehicles, micro-electro-mechanical systems, networked control, control of networks, production lines and chemical processes. It is shown that the system classes presented have the common feature that all stabilizing controllers can be characterized by convex constraints on the Youla-Kucera parameter. Using this feature, a solution to a general optimal performance problem that incorporates time domain and frequency domain constraints is obtained. A synthesis procedure is provided which at every step yields a feasible controller together with a measure of its performance with respect to the optimal. Convergence to the optimal performance is established. An example of a multinode network congestion control problem is provided that illustrates the effectiveness of the developed methodology.     

Mesh结构P/G布线网络层次化快速分析方法

本文提出了一个基于网络划分的P／G布线网络层次化快速分析方法。其中，对于子网运算，通过对Cholesky分解法三角化对称正定阵的图模型分析，并基于Mesh结构网络的自身特点，提出了一个基于图顶点排序的加速子网分析运算策略；并用基于MPI的并行结构实现了P／G布线网络分析的并行运算。     

Mesh-Tree两级层次结构P/G网布线优化方法

本文采用Mesh-Tree两级层次结构作为P／G网布线拓扑结构，并提出了一个对于该结构的线宽优化方法，使超大型P／G网的布线优化速度大大提高。     

High-Tc dc-SQUID magnetometer and its application in eddy current non-destructive evaluation

We have fabricated and tested a high-T_c dc-SQUID magnetometer patterned on a YBCO thin film deposited on a SrTiO₃ bicrystal substrate. The measurement of noise spectrum at 77 K showed that the magnetometer has a white noise of 333 fT/Hz^1/2 without superconducting shield, corresponding to a flux sensitivity of 14.5 μΦ₀/Hz^1/2. We constructed a test system for eddy current non-destructive evaluation of conducting aluminum plates by using the magnetometer. Flaws over 10 mm below the surface can be clearly identified. By mapping the magnetic field distribution, we can locate the flaw position. The signals caused by flaw were expanded due to the use of double-D type driving coil with a wider central slit. The experimental results confirmed that this test system could operate in a magnetic unshielded environment.     

化学气相沉积铜薄膜研究进展

本文综术了集成电路工艺的Cu布线中Cu薄膜化学气相沉积(CVD)的研究背景,详细介绍了CVD生长Cu金属薄膜的国内外研究进展及CVD对前趋物的要求,并对前趋物的一些物理、化学性质进行了总结,最后,对薄膜沉积的计算机摸拟作了简要介绍。     

垂直管吸收器内泡式吸收过程的数值研究

建立垂直管吸收器管内泡式吸收过程中传热传质的数学物理模型，对其泡式吸收过程进行数值研究，获得泡式吸收方式的一些传热传质特性，为吸收器的优化设计提供一定理论指导。     

氧气顶吹转炉溅渣护炉试验研究

采用水力模型研究方法 ,针对马钢 2 0t转炉进行溅渣护炉冷态模拟试验 ,得出最佳工艺参数为 :枪位 1680mm ,氮气流量为 110 0 0m3/h ,大流渣量 ,渣粘度适中。此外 ,在满足炼钢生产的条件下 ,采用夹角为 13°的喷头溅渣效果好