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Guo Dong Zhu Jing Xu Xue Jian Yan Jie Li Zhi Gang Zeng Miao Shen Li Zhang 《Thin solid films》2006,510(1-2):181-183
This paper introduces the Force Modulation technique to the study of crystallization process in ferroelectric vinylidene fluoride and trifluoroethylene copolymer films. Using this technique we have successfully visualized ferroelectric crystalline domains and observed that these ferroelectric domains grow out from amorphous phase, unite into strip-like structures, and finally congregate into a union. Force Modulation can weaken the influence of topography on imaging of ferroelectric domains, and reveal more details, which are difficult to be observed in topographical image. 相似文献
64.
Y1.94-xMgxO2S:0.06Ti (0≤x≤0.10) phosphors with long afterglow were synthesized by solid state reaction route. The photoluminescence spectra, decay curves, thermoluminescent spectra and chromaticity coordinate curves were investigated. The results show that the luminescence intensity of Y1.94-xMgxO2S:0.06Ti (0≤x≤0.10) phosphors decrease gradually with increasing Mg2 ion content, and the shape of luminescence spectra and chromaticity coordinate change as well. Furthermore, two thermoluminescent peaks in single Ti-doped Y2O2S sample are found at 91.8 and 221.5 ℃, respectively. Nevertheless, significant different spectra were found for the Mg, Ti co-doped Y2O2S samples that three thermoluminescence peaks appear at 52.3, 141.7 and 226.8 ℃, respectively. These results indicate that the co-doped Mg ion changes the inherent trap depth of single Ti-doped Y2O2S:Ti phosphor, and induces simultaneously a new trap level in the Y1.94-xMgxO2S:0.06Ti phosphor. Based on the analysis of thermoluminescent spectra, photoluminescent spectra, decay curve and crystal structure defect, it was proposed that the varied structure defect and introduced new trap level by the doped Mg2 ions should be responsible for reducing luminescence intensity and varying color in the Y1.94-xMgxO2S:0.06Ti phosphor. 相似文献
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Qiang Wang Yi Shen Ye Zhang Jian Qiu Zhang 《IEEE transactions on instrumentation and measurement》2003,52(4):1041-1047
Hyperspectral image fusion is a key technique of hyperspectral data processing. In recent years, many fusion methods have been proposed, but there is little work concerning evaluation of the performances of different image fusion methods. In this paper, a method called quantitative correlation analysis (QCA) is proposed, which provides a quantitative measure of the information transferred by an image fusion technique into the output image. Using the proposed method, the performances of different image fusion methods can be compared and analyzed directly based on the images of before and after performing the fusion. The correlation information entropy, based on the developed QCA, is also proposed and testified by numerical simulations. Typical hyperspectral data are applied to the proposed method. The results show that the method is effective, and its conclusions agree with the classification results in applications. 相似文献
68.
The electron spin resonance (ESR) spectra of end‐group spin labelled poly(ethylene oxide) (SLPEO) using 2,2,6,6‐tetramethyl‐piperdine‐1‐oxyl nitroxide and its blends with poly(styrene‐co‐4‐vinylphenol) (STVPhs) of different hydroxyl contents were recorded over a wide temperature range. For a blend of SLPEO and pure polystyrene (PS), the ESR spectrum was composed of a single motion component, indicating that PS was immiscible with PEO. For blends composed of SLPEO and different‐hydroxyl‐content STVPhs, two spectral components with different motion rates were observed over a certain temperature range. The difference between the motion rates should be attributed to micro‐heterogeneity in the blends, with the faster rate corresponding to a nitroxide radical motion trapped in the PEO‐rich domain and the slower rate corresponding to a nitroxide radical motion trapped in the STVPh‐rich domain. Variations in the values of a number of the ESR parameters (Ta, Td and T50G) and the apparent activation energy (Ea) with hydroxyl content in the blends indicated that the miscibility of the blends increased with increasing hydrogen‐bonding density due to specific interactions between the hydroxyl groups in STVPh and the ether oxygens in PEO. Copyright © 2004 Society of Chemical Industry 相似文献
69.
Yanhan Shen Rongrong Qi Qiaochu Liu Yanling Wang Yapeng Mao Juan Yu 《应用聚合物科学杂志》2008,110(4):2261-2266
The grafting of a polymer can lead to the improvement and modification of the polymer and thus expand its applications. Grafting methods include solution grafting in organic solvents, melt grafting at high temperatures, and light grafting with radioactive sources. These methods have their advantages and disadvantages. The disadvantages include waste treatment, consumption of energy, and so on. In this study, a hydrothermal process which is called the green approach, was developed to prepare graft copolymers. The effect of various factors on the grafting degree was investigated in detail. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献
70.
Novel calix[4]arene‐poly(ethylene glycol) crosslinked polymer (CCP) has been synthesized by the polycondensation reaction between a p‐tert‐butylcalix[4]arene derivative and dihydroxyl capped poly(ethylene glycol) (DHPEG, Mn = 1000) catalyzed by neodymium tosylate. The hydrogel, consisted of 66.9% water and 33.1% CCP, can selectively extract aromatic organic molecules from aqueous solution according to the diameter of the guest molecules, which infers that the diameter of the calix[4]arene cavity is about 5.4 Å and the conformation of calix[4]arene units altered from cone conformation to 1,3‐alternate conformation during the polycondensation reaction. Furthermore, CCP can also adsorb naphthalene from gas phase, showing much higher capacity than active carbon does, which may have some potential applications in the field of separation and environment protection. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献