Microwave heating synthesis of HgS and PbS nanocrystals in ethanol solvent

A novel route was developed to prepare PbS and HgS nanocrystals in ethanol solvent in the presence of sodium hydroxide by microwave heating method. PbS and HgS nanocrystals were obtained with an average size of approximately 10 and 6 nm, respectively. In the reaction, mercury acetate and lead acetate were used as mercury and lead source; sulfur powder was employed as chalcogenide source. The products were characterized by X-ray powder analysis (XRD), transmission electron microscopy (TEM), X-ray photoelectron spectroscopy (XPS) and UV–Vis absorption spectroscopy. The probable mechanism was presented.     

Analytical solution for the axisymmetric plane strain electroelastic dynamics of a special non-homogeneous piezoelectric hollow cylinder

By virtue of the introduction of a dependent variable and the separation of variables technique, the axisymmetric plane strain electroelastic dynamic problem of a special non-homogeneous piezoelectric hollow cylinder is transformed to a Volterra integral equation of the second kind about a function with respect to time, which can be solved successfully by means of the interpolation method. Then the solutions of displacements, stresses, electric displacements and electric potential are obtained. The present method is suitable for a piezoelectric hollow cylinder with an arbitrary thickness subjected to arbitrary mechanical and electrical loads. Numerical results are finally presented.     

Generalized eigenvectors and fractionalization of offset DFTs and DCTs

The offset discrete Fourier transform (DFT) is a discrete transform with kernel exp[-j2/spl pi/(m-a)(n-b)/N]. It is more generalized and flexible than the original DFT and has very close relations with the discrete cosine transform (DCT) of type 4 (DCT-IV), DCT-VIII, discrete sine transform (DST)-IV, DST-VIII, and discrete Hartley transform (DHT)-IV. In this paper, we derive the eigenvectors/eigenvalues of the offset DFT, especially for the case where a+b is an integer. By convolution theorem, we can derive the close form eigenvector sets of the offset DFT when a+b is an integer. We also show the general form of the eigenvectors in this case. Then, we use the eigenvectors/eigenvalues of the offset DFT to derive the eigenvectors/eigenvalues of the DCT-IV, DCT-VIII, DST-IV, DST-VIII, and DHT-IV. After the eigenvectors/eigenvalues are derived, we can use the eigenvectors-decomposition method to derive the fractional operations of the offset DFT, DCT-IV, DCT-VIII, DST-IV, DST-VIII, and DHT-IV. These fractional operations are more flexible than the original ones and can be used for filter design, data compression, encryption, and watermarking, etc.     

Synthesis of diamond crystals and films using an oxygen-acetylene flame under atmosheric pressure

Diamond growth with rates up to 100 to 140 μm/hr was achieved using an oxygen-acetylene combustion spraying technique in an atmospheric environment. Investigations on the processing indicated that the gas flow ratio, substrate position, substrate temperature, temperature distribution, and substrate pretreatment were the most important factors affecting the growth of diamond crystals. Evaluation by means of X-ray diffraction, Raman spectroscopy, scanning electron microscopy, and electron probe microanalysis showed that the synthesized diamond was nearly perfect in morphology, structure, and purity.     

PERIODIC DYADIC GREEN''S FUNCTION FOR FIELD ANALYSIS IN EMC CHAMBER

Herein a novel Dyadic Green's Function (DGF) is presented to calculate the field in ElectroMagnetic Compatibility (EMC) chamber. Due to the difficulty of simulating the whole chamber environment, the analysis combines the DGF formulation and the FEM method, with the latter deals with the reflection from absorbers. With DGF formulation for infinite periodic array structures, this paper investigates electromagnetic field in chamber with truncated arrays. The reflection from the absorber serves as the virtual source contributing to the total field. Hence the whole chamber field calculation can be separated from the work of absorber model set-up. Practically the field homogeneity test and Normal Site Attenuation (NSA) test are carried out to evaluate the chamber performance. Based on the method in this paper, the simulation results agree well with the test, and predict successfully the victim frequency points of the chamber.     

在役油气管道安全评定软件

PSAforWindows是运行在Windows系统下的油气管道安全评定软件。该软件既可以用于在开挖中发现的管道局部缺陷的剩余强度的精确评定 ,又可以用于腐蚀检测之后对管道全线的安全评定与剩余寿命预测。软件中采用了非线性有限元分析、失效评定图和概率性的评定方法等最新成果。介绍该软件的结构、模块、软件特点、主要功能和操作界面     

基于欧玛技术的大学英语考试总评成绩计算方法

以基于欧玛技术的阅卷系统为例,介绍了用Excel实现大学英语分类成绩的接口及合并计算总评成绩的基本方法与步骤.     

Nonlinear Stress-Strain Relationship of Soil Reinforced with Flexible Geofibers

A nonlinear stress-strain relationship of soil reinforced with flexible geofibers under static loading is derived based on a nonlinear elastic stress-strain relationship of soil and a linear elastic stress-strain relationship of geofibers in the paper. This investigation includes the following aspects: First, the homogenization technique is introduced to find the volume average stress tensor and volume average strain tensor and further an elastic incremental stress-strain relation is introduced to describe deviatoric shear stress-axial strain relationship of equivalent homogeneous geofiber-reinforced soil. Second, the relation of geofiber numbers, content, mechanical behavior, distribution, and geometrical features to shear modulus of geofiber-reinforced soil is expressed and assessed by employing an elastic energy method. Third, the deviatoric shear stress and axial strain curves of geofiber-reinforced soil are calibrated by laboratory testing data of geofiber reinforced soil samples. Finally, the theoretical computational curves of geofiber reinforced soil are compared with the curves calibrated by testing data of geofiber reinforced soil. The model prediction has a good agreement with experimental results.     

BKX-Ⅰ型并联机床的谐响应分析

应用有限元分析软件(ANSYS),对BKXⅠ型并联机床进行谐响应分析,分别得到了机床各节点沿机床的虚拟轴X、Y和Z向的位移谐响应曲线。在此基础上,还分析了该机床的谐响应规律,并明确了谐响应的特点,为改善此类机床的动态特性提供了一定的参考依据。