A Study on NMR and GC/MS Spectra of the Isomers of Linear Hexyl Naphthalene

The GC/MS and NMR analysis of the reaction products of naphthalene with 1-bromohexane were reported. The products obtained were suggested to have six isomers of linear hexylnaphthalene and the structure of each isomer was determined by GC/MS and NMR spectra. For the first time, the unique chemical shift data were obtained. The content of each isomer calculated by ¹H NMR and ¹³C NMR spectra was consistent with that by GC/MS spectra, which confirmed the accuracy of NMR data.     

VS2005—高校实验设备网络化管理的利器

高校实验设备实施网络化管理,能够极大提高设备信息的透明度,提高实验设备管理的效率,进一步优化管理工作.VS2005是开发高校设备管理网站的一种简单易学、功能强大的工具.现给出了一个基本的高校实验设备管理网站开发的全过程.     

从事放射性个人剂量监测分析与防护调查

为了能及时了解放射性工作人员的受照剂量，以便能够更好地保障放射工作人员的健康与安全，采用热释光测量法对包头地区从事放射性工作的工作人员进行了个人剂量监测，并对他们的剂量当量频数分布进行了统计与分析，对工作环境的防护进行了调查对比，就今后的工作提出建议。     

Al-Zn-Ce非晶合金的相选择与组织结构演化

本文研究了具有典型分解特征的Al-Zn-Ce非晶合金的形成和晶化过程，探讨了各种相的生成顺序。XRD和DSC测试结果表明强烈的化合物短程序有利于Al-Zn-Ce非晶合金的形成。在Al-Zn-Ce非晶合金的晶化过程中存在复杂的相选择行为，多种相的竞争形核和有限生长使其具有复杂的结构特点。同时，结果也表明冷速对该体系非晶的形成有很大影响。     

实践在马克思主义哲学理论中的意蕴——读《关于费尔巴哈的提纲》有感

马克思以实践为出发点和指导原则，创立了马克思主义哲学理论。正确理解和把握马克思主义实践哲学的科学意蕴，具有重要意义。     

Finite-element analysis and experimental study on tensile fatigue behaviour of bitumen–stone adhesion

Tensile fatigue behaviours of bitumen–stone adhesion were investigated using a dynamic mechanics analyser under stress‐controlled mode at two temperatures of 5 and 25°C and various controlled‐stress levels. Failure characteristics including interfacial failure and cohesive failure were examined using image analysis of fracture surfaces. Finite‐element analysis on stress distributions was conducted under different temperatures, film thickness and interfacial bonding conditions. A Coulomb–Mohr like criterion in combination with shear and normal stresses is proposed to deal with the extreme thin adhesive layer, which can be further simplified into an adhesive zone without significant loss of accuracy for stress analysis.     

控轧技术在H型钢生产中的应用

根据钢板的控轧经验，结合H型钢轧制的特点分析控轧在轧制中运用的具体问题，制定H型钢控轧工艺方案。介绍了实际应用情况，并提出改进的措施。     

Model of Primary Austenite Dendrite Structure in Hypoeutectic Cast Iron

Ｉｔｗａｓｒｅｐｏｒｔｅｄ[1] ｔｈａｔｔｈｅｍｉｃｒｏ ｓｔｅｒｅｏｓｔｒｕｃｔｕｒｅｏｆｐｒｉｍａｒｙａｕｓｔｅｎｉｔｅｉｎｃａｓｔｉｒｏｎｃｏｎｓｉｓｔｓｏｆｐｒｉｍａｒｙｓｔｅｍｓａｎｄｓｅｃｏｎｄａｒｙａｒｍｓｔｈａｔ ｇｒｏｗａｃｃｏｒｄｉｎｇｔｏｄｅｎｄｒｉｔｅｃｒｙｓｔａｌｓｂｒａｎｃｈｒｕｌｅ ,ａｎｄｓｏｍｅｏｆｐｒｉｍａｒｙａｕｓｔｅｎｉｔｅｅｖｅｎｈａｖｅｔｈｉｒｄａｒｍｓ .ＭｉｙａｋｅＨｅｔａｌ[2 ]ｐｒｏｐｏｓｅｄａｃｏｎｃｅｐｔｏｆｒｅｇｉｏｎｍｏｄｅｌｂｙｓｔｕｄｙｉｎｇ…     

Hydrogen Permeation and Diffusion in Amorphous Alloy Ni_(68)Cr7_Si_8B_(14)Fe_3 at Elevated Temperature

The behaviour of hydrogen permeation and diffusion in amorphous alloy Ni68Cr7Si8B14Fe3 hasbeen investigated by an ultrahigh vacuum gas permeation technique. A comparison experimentwas carried out between the as-quenched and annealed States (400℃/2h) of the amorphousalloy. The results show that, for both states of the amorphous alloy in the temperature rangeof 200～350℃, the diffusivity and permeability of hydrogen are in agreement with Arrheniusrelationship, there does not exist H-trapping effect, and the activation energies of diffusion andpermeation almost keep the same.