溶胶-凝胶法制备磷钨酸-硅胶催化合成苹果酯

采用溶胶-凝胶法制备了一系列磷钨酸-硅胶催化剂(PW/SG),考察了该催化剂催化乙酰乙酸乙酯与乙二醇液相缩合制备苹果酯的反应性能。实验结果表明,PW质量分数为40%时的PW/SG催化剂表现出最佳的催化活性;40%PW/SG催化剂制备苹果酯的最佳工艺条件为:n(乙酰乙酸乙酯)∶n(乙二醇)=1∶1.2,催化剂用量占反应物质量的0.36%,带水剂环己烷用量占反应物体积的30%,反应温度383K,反应时间90min;在此条件下,乙酰乙酸乙酯的转化率可达95.5%,苹果酯的选择性大于97%;催化剂稳定性实验表明,经5次重复使用,40%PW/SG催化剂的活性基本保持不变,乙酰乙酸乙酯转化率稳定在95.0%左右。     

朗江电站水库洪水调度探讨

文章根据朗江水库工程实际情况,介绍了水库洪水成因及特性,通过洪水设计、调洪演算计算分析,指出了闸门操作程序,对"以峰控制"的中、小型水库的洪水调度具有一定的参考价值。     

Ranking with uncertain labels and its applications

The techniques for image analysis and classification generally consider the image sample labels fixed and without uncertainties. The rank regression problem studied in this paper is based on the training samples with uncertain labels, which often is the case for the manual estimated image labels. A core ranking model is designed first as the bilinear fusing of multiple candidate kernels. Then, the parameters for feature selection and kernel selection are learned simultaneously by maximum a posteriori for given samples and uncertain labels. The provable convergency Expectation Maximization (EM) method is used for inferring these parameters in an iterative manner. The effectiveness of the proposed algorithm is finally validated by the extensive experiments on age ranking task and human tracking task. The popular FG-NET and the large scale Yamaha aging database are used for the age estimation experiments, and our algorithm outperforms those state-of-the-art algorithms ever reported by other interrelated literatures significantly. The experiment result of human tracking task also validates its advantage over conventional linear regression algorithm. A short version of this paper appeared in ICME07.     

地层测试资料在实际应用中若干问题浅析

华北油田冀中地区在十几年实践过程中，陆续开展了200多层次地层测试（或三开抽汲）及该试油层常规抽汲试油工作。通过对1300次测试资料特别是对200层复试资料的分析对比，认为测试资料对自喷层和中高产非自喷井是准确的，可以不必进行三开抽汲。对井壁深部污染、低渗透和特低渗透层还存在一些偏差，为解决探井中一些疑难问题，需要配合抽汲。     

Is layering, harmful? [remote procedure call]

Remote procedure call (RPC) mechanisms over the US Department of Defense transmission control protocol. (TCP) can produce behavior analogous to the silly window syndrome because of a mismatched interface between the socket and the TCP modules. The detection and diagnosis of the problem are addressed. Some pointers to a design approach that could avoid the problems of mismatched communication layers are provided     

高层钢结构的安装测控技术

介绍了高层钢结构安装测控的基本方法和工艺流程 ,并对高层钢结构安装中的控制要点和控制方法进行了详细论述。     

大庆油田深层岩石力学特性参数的试验研究

通过对岩石可钻性、硬度、抗压强度等参数的测量 ,对大庆油田深井不同深度、不同层位、不同岩性的具有广泛代表性的岩心进行试验。并通过线性回归分析 ,建立了适用性较广的钻井岩石力学特性参数预测模型 ,为深井钻头选型提供了依据。     

长途传输波分复用系统的设计

随着波分复用（WDM）技术的广泛应用，在工程调测和系统的运行过程中出现了由于系统的适应能力较差和灵活性不够而引起系统优化时间过长的问题，给运营商带来了许多不便，同时，WDM已经由一般的长途应用向超长距离传输和城域网方面发展，适应性和灵活性成为WDM系统网络应用的主要要求，本文将介绍WDM系统的关键技术，重点论述WDM网络设计的一些原则，最后提出WDM系统设计的注意事项。     

钕玻璃激光放大器反转粒子数的荧光测定法

本文报道了通过测量钕玻璃激光放大器在一定泵浦功率下的荧光波形的方法,获得放大器中反转粒子数密度随时间的变化关系,进而得到反转粒子数密度达到最大值的时刻的测定方法及实验结果。