锡或锑在无取向电工钢中的研究进展

近年来,在节能减排背景之下,国内外众多研究者对无取向电工钢磁性能的提升做了大量研究。为了探索无取向电工钢磁性能提升的方法,对锡或锑对无取向电工钢磁性能的作用机制(晶粒尺寸和晶体织构的控制)进行分析。基于该作用机制,介绍锡或锑的添加对无取向电工钢磁性能的影响。经研究发现,适量的锡或锑在晶界偏聚,不会阻碍晶界的移动并且致使晶粒尺寸降低;与此同时,锡或锑在晶界偏聚不仅抑制{111}织构在原始晶界处形核及生长,还降低(100)晶粒表面能,促进(100)晶粒生长。因此,适量添加锡或锑,可使无取向电工钢铁损下降、磁感提升。最后结合生产工艺,建议无取向电工钢的研究方向应为稀土含量对高牌号无取向硅钢夹杂物尺寸和数量分布的影响,锡或锑的添加量和常化工艺参数(常化时间、常化温度)对常化晶粒尺寸的影响。     

饰品金合金微量添加元素研究现状

从提高强度、防止氧化、提高铸造性能以及细化晶粒几个方面综述了饰品金合金中微量添加元素的一些研究现状。对不同微量添加元素对饰品金合金性能的影响、相应的副作用,作用机理以及加入量的确定等方面进行了综合评述。并对饰品金合金微量添加元素的发展进行了展望。     

Preparation and electrochemical performance of nanosized Co3O4 via hydrothermal method

The hydrotalcite-type cobalt compounds were prepared through oxidation of Co（OH）2 gel using NH4OH as precipitating agent and H2O2 as oxidant. These hydrotalcite-type cobalt compounds were transformed into Co3O4 through hydrothermal decomposition with nanostructural deformation. The precursor and product were characterized by Fourier-transform infrared（FT-IR） spectrum, X-ray diffractometry（XRD） and transmission electron microscopy（TEM）. The electrochemical performances of as-prepared nanosized Co3O4 as anode materials in lithium-ion batteries were tested by charge-discharge test in the voltage range of 0-3.0 V. The influence of morphology of Co3O4 particle on the capacity and cycling performance was studied. The results show that the shape and size of the final product can be controlled by altering cobalt sources. The irregular cubic Co3O4 with the average particle size of about 10 nm shows the best electrochemical performance. After 10 charge-discharge cycles, the specific charge capacity retains 555 mA.h/g.     

Synthesis of Ti3SiC2 by spark plasma sintering(SPS)of elemental powders

Ti3SiC2 materials have been fabricated by spark plasma sintering of the elemental powders with the addition of Al.At the heating rate of 80℃/min and under the pressure of 30MPa,the ideal synthesis temperature of Ti3SiC2 is in the range of 1150-1250℃.The addition of Al is in favor of the formation of Ti3SiC2.The synthesized compound has the molecular of Ti3Si0.8Al0.2C2 and lattice parameters of α=0.3069nm,c=1.7670nm.Its grain is plane-shape with a size of about 50μm in the elongated dimension.The prepared material has Vickers hardness of 3.5-5.5GPa(at 1N and 15s) and is as readily machinable as graphite‘s.     

烧结参数对温压Fe-2Ni-2Cu-1Mo-1C材料抗拉强度的影响

采用温压方法制备了高密度Fe-2Ni-2Cu-1Mo-1C材料,并研究了烧结温度和烧结时间对温压Fe-2Ni-2Cu-1Mo-1C材料烧结密度和抗拉强度的影响。结果表明:常规温压和模壁润滑温压的烧结密度和抗拉强度随烧结温度和时间的变化而变化,模壁润滑温压的烧结密度和抗拉强度均大于常规温压的;温压材料的抗拉强度为烧结温度和烧结时间的函数,常规温压和模壁润滑温压的抗拉强度随烧结温度和时间变化的线性回归方程(R为相关系数)分别为σb=575 211 153 6f(t,T),R=0.972和σb=595 208 688 3f(t,T),R=0.997。     

Effects of Thermal Exposure on the Tensile and Fatigue Properties of Cast Ti—47Al—2Cr—2Nb--0.15B Alloy

测量了铸造Ti—47Al—2Cr—2Nb-0．15B(原子分数，％)合金的高温疲劳强度以及650℃／100h和800℃／100h热暴露后的拉伸性能和疲劳强度，采用X射线衍射和扫描电镜等方法分析了经热暴露后合金基体组织的变化和表面层的结构．随暴露温度的提高，合金的室温塑性和疲劳强度降低，650℃附近有一转折点，大于650℃时上述性能加速下降；合金高温疲劳性能具有相似的变化规律．显微分析表明，在热暴露或高温疲劳实验时，表面形成的脆性层是导致合金性能降低的直接原因；而随温度的提高，表面层由渗氧层转变为氧化层是导致合金性能随温度变化出现转折的原因．     

使用Visual C+ +实现串行通讯

以VisualC 为工具，探讨了在RS-232C接口协议下DTE设备之间通讯的实现问题。     

高温烟气过滤筒制作工艺研究

本文对除尘净化设备常用的过滤材料进行了综述对比 ,提出了一种新型的过滤材料 ,该过滤材料可以在高温下直接使用 ,有利于简化除尘净化设备。同时对用这一新型的过滤材料制作过滤筒的工艺进行了初步探讨和研究。     

软包装标牌模具的设计和加工

分析了零件的工艺特点 ,介绍了此类软包装高速冲模的结构 ,以及模具中的计数装置、凸模上吹气卸料和收料装置 ,并对该模具的加工工艺做了详细的介绍     

Tribological behavior of high specific strength PTFE-Al alloy composite

Solid lubricants lead to substantial weight savings relative to the use of liquid lubricant, especially in the weight-conscious aerospace industry. A new PTFE-Al alloy composite（A） containing 60% area proportion of PTFE composite was developed. Another type of common metal-plastics multilayer composite, also called DU, was selected for a comparative investigation. Friction and wear tests were carried out in an oscillating sliding tribotester in air at an oscillating frequency of 0.13 Hz and contact mean pressures from 10 to 80 MPa. The composites slid against a 38CrMoAlA steel shaft. The results show that the composite A exhibits low coefficient of dry sliding friction less than 0.1 and long wear life of 2 000 m. This is because the composite A can provide a sufficient solid lubrication during the whole tests. SEM examination of the transfer films for the composite A confirms that uniform, thin and coherent transfer films are prerequisites for low friction and good wear resistance.