浅谈创业教育

按照《面向21世纪教育振兴行动计划》提出的目标，我国高等教育到2010年入学率接近15％，这个目标有可能提前实现；若按每年新出生人口为2000万计算，高等学校在校生规模将达到1500万，每年毕业生将在500万以上。面对这样沉重的就业压力，转变大学生毕业就是到社会上寻求工作岗位的就业观念，树立和加强创业教育，引导毕业生走自己的路，就显得有十分重要的特殊意义了。     

丙烯酸接枝线形低密度聚乙烯的热学行为及结晶形态

利用差示扫描量热仪研究了丙烯酸接枝线形低密度聚乙烯（PE-LLD-g-AA）的热学行为，结果表明，与纯线形低密度聚乙烯（PE—LLD）相比，PE-LLD-g-AA的熔融温度（Tm）略有增加，结晶温度（Tc）增加大约4℃，熔融焓（AHm）随AA含量的增加而降低。还利用差示扫描量热仪研究了PE—LLD和PE—LLD-g—AA的等温结晶动力学，用扫描电子显微镜观察了PE—LLD-g—AA等温结晶形态。结果表明，PE-LLD-g-AA的结晶速率大于纯PE—LLD的，随着接枝率的增加，PE-LLD的球晶半径减小，接枝到PE—LLD分子链上的AA分子起到了成核剂的作用。     

射流流化床内流体力学行为的模拟研究

以流化床应用为代表的气固流动系统是许多化工过程中的重要组成部分 ,CFD( computational fluid dynamics)方法能够为其优化设计和放大提供所需要的信息 .本文采用双欧拉模型 ,与 Gidaspow等的实验结果进行了对比 ,模拟了二维射流流化床内气泡的形成规律 ,得到了带锥型分布器的流化床内瞬时空隙率和气固相速度分布等流体力学参数 .对锥型分布器流化床的实验结果表明 ,模拟得到的气泡的形状与实验现象相接近 .     

HIPS-g-PMMA的合成及其在HIPS/PVC共混体系中的增容作用

采用自由基引发的溶液聚合法合成了高抗冲聚苯乙烯接枝聚甲基丙烯酸甲酯(HIPS-g-PMMA)增容剂，考察了引发剂用量、反应温度及反应时间对增容剂的接枝率及支链摩尔质量的影响；同时对增容剂对HIPS／PVC共混体系的增容效果作了考察。结果表明：最佳反应条件是反应温度80℃，反应时间4h，引发剂用量以0．2～0．25g为宜；增容剂HIPS-g-PMMA对HIPS／PVC共混体系表现出较好的增容效果，共混物的拉伸强度、屈服强度及断裂伸长率明显增加，冲击强度增大，电镜照片显示两相界面变得更加模糊。     

Vinyl‐containing silicone resin as the crosslinking agent of heat‐curable silicone rubber

Heat‐curable silicone rubber (HCSR) was prepared by using vinyl‐containing silicone resin (VSR) as the crosslinking agent instead of polyvinylsilicone oil (C gum). Mechanical properties and crosslink density of the vulcanizates were measured. The results indicate that VSR is a good crosslinking agent for HCSR. The tensile strength, tearing strength, elongation at break, and hardness of the vulcanizate can reach 10.2 MPa, 29.1 kN/m, 720%, and 58 SHA, respectively. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 83: 3123–3127, 2002; DOI 10.1002/app.10054     

以显微荧光检验法检测常用盖印材料

显微荧光检验法是显微检验的一个重要角度,由于缺少基础性研究,这一方法在文件检验中的运用并不广泛.着重考虑曝光时间这一因素,以盖印材料的荧光特性为观察角度,运用显微荧光检验法对大量常用盖印材料进行系统、全面的观察和研究.研究表明,绝大部分盖印材料可被激发出荧光,每种盖印材料的荧光特性都有各自的规律性特点.     

Morphologies-Controlled Synthesis and Optical Properties of Bismuth Tungstate Nanocrystals by a Low-Temperature Molten Salt Method

Well-crystallized bismuth tungstate (Bi₂WO₆) powders with different morphologies were successfully synthesized via a low-temperature molten salt method. The powders were characterized by X-ray diffraction, transmission electron microscopy, and UV-Vis, respectively. It was found that the variation of morphology of the obtained Bi₂WO₆ powder mainly depends on the different reaction temperatures and the weight ratio of LiNO₃–NaNO₃ salt to precursor. In addition, the UV-Visible absorption spectra showed that the synthesized powders had strong light absorption properties not only in the ultraviolet light but also in the visible light region.     

Nanocrystalline CeO2 in SBA-15: Performance of Pt/CeO2/SBA-15 Catalyst for Water-gas-shift Reaction

CeO₂ particles confined within the pores of an SBA-15 mesoporous silica host were prepared by incipient wetness impregnation (IMP) and deposition precipitation (DP) methods. The materials were characterized by XRD, N₂-adsorption and temperature programmed reduction (TPR) to evaluate the structure, texture, and redox properties. The preparation procedure had significant impact on the assembling mode of CeO₂ inside the SBA-15 mesopores. A high dispersion of CeO₂ particles was achieved via DP, whereas the dispersion of CeO₂ prepared by IMP was found to be inhomogeneous and CeO₂ partially blocked the pores. The CO conversion in the water-gas-shift reaction was enhanced over 1 wt% Pt supported on CeO₂-modified SBA-15 obtained by DP.     

英汉情感隐喻的共性与差异

为进一步了解情感隐喻的实质,以人类基本情感的隐喻表达作讨论对象,对英汉语言中的基本情感隐喻进行共性与差异分析。     

A novel shaft-less double suction mini pump

A novel double suction shaft-less mini pump was developed for heat control of small energy systems in this study.The mini pump impeller with an exit diameter of 40 mm was combined with the motor rotor supported by the hybrid dynamic bearing.The specific speed of the pump was 125 min-1 m3 min-1 m.The hydraulic performance of the pump was investigated experimen-tally under four rotational speeds.From the test results,it was recognized that the pump could provide a flow discharge of 5 L/min and head of 1.5 m,w...