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51.
The synthesis of rare-earth perovskite-type composition thin films of LaNiO3 by means of the inorganic-sol-gel (ISG) method was studied. The structural stability under high temperature in reducing atmospheres and the oxygen-sensitivity mechanism of the LaNiO3 thin films were examined. It is shown that under the experimental conditions, LaNiO3 decomposes and the valance states of nickel are +2 and +3.  相似文献   
52.
过渡金属对Au-Pd/TiO_2-Al_2O_3催化剂加氢脱硫性能的影响   总被引:2,自引:1,他引:1  
研究了掺杂过渡金属Ru,Ni,Co对Au-Pd/TiO2-Al2O3催化剂催化噻吩加氢脱硫活性的影响,并采用X射线衍射、电感耦合等离子发射光谱、程序升温还原和程序升温脱附等方法对TiO2-Al2O3复合载体、Au-Pd/TiO2-Al2O3和Au-Pd-TM/TiO2-Al2O3(TM表示过渡金属)催化剂进行了表征。实验结果表明,掺杂过渡金属未改变Au-Pd/TiO2-Al2O3催化剂的结构;掺杂Ru或Ni增强了Au-Pd/TiO2-Al2O3催化剂的活性组分与TiO2-Al2O3复合载体的相互作用,降低了反应活化能,提高了催化剂活性组分的分散度和活性比表面积,改善了Au-Pd/TiO2-Al2O催化剂的吸附性能,从而提高了Au-Pd/TiO2-Al2O3催化剂催化噻吩加氢脱硫的活性;而掺杂Co的效果则与之相反。  相似文献   
53.
The two-dimensional finite-element method is applied to analyze the shrinkage and splitting of microcracks regularly arranged on or perpendicular to a grain boundary under pressure. Grain-boundary and surface diffusions are coupled by the boundary conditions at the triple point of the microcrack surface and the grain boundary. The shrinkage and splitting processes for the two kinds of microcracks are revealed by detailed finite-element analyses. For the microcrack lying on a grain boundary, it first shrinks to a small void shape, then the void is split by the grain boundary and the two split voids assume a cylindrical shape under the capillary force of the surface. For the microcrack perpendicular to the grain boundary, it is split into two segments by the grain boundary during the early stage of shrinkage. Then, the split microcracks stop shrinking and evolve into two cylindrical channels with a circular section by the capillary force of the surface. These evolution processes are controlled by the applied pressure, microcrack spacing, ratio of grain-boundary diffusion to surface diffusion, and equilibrium dihedral angle, defined by surface and grain-boundary tensions. The influences of these controlled parameters on the evolution processes are numerically clarified based on a great number of finite-element analyses.  相似文献   
54.
多功能半导体激光医疗仪电源的研制   总被引:1,自引:0,他引:1  
根据“多功能半导体激光医疗仪”整机的要求,采用同一电源对667nm和808nm半导体激光器实施供电。为避免电源在开、关机时对半导体激光管产生浪涌冲击,电源在设计中采用了适当的逻辑功能。并可保证对667nm激光器供电时,即使打开808nm激光器供电开关,也不对808nm半导体激光器供电,反之亦然。电源设有手动、计算机两种控制方法,及恒定功率、电流两种工作方式。  相似文献   
55.
This paper is concerned with the inversion of confluent Vandermonde matrices. A novel and simple recursive algorithm for inverting confluent Vandermonde matrices is presented. The algorithm is suitable for classroom use in both numerical as well as symbolic computation. Examples are included to illustrate the proposed algorithm.  相似文献   
56.
BACKGROUND: It has been suggested that excessive formation of nitric oxide (NO) is responsible for the hyperdynamic circulation observed in portal hypertension. Substance P is a neuropeptide partly cleared by the liver and causes vasodilatation through the activation of the endothelial NO pathway. However, there are no previously published data concerning the plasma level of substance P in cirrhotic rats and its relationship to NO. METHODS: Plasma concentrations of substance P and nitrate/nitrite (an index of NO production) were determined in control rats and cirrhotic rats with or without ascites using an enzyme-linked immununosorbent assay and a colorimetric assay, respectively. In addition, systemic and portal hemodynamics were evaluated by a thermodilution technique and catheterization. RESULTS: Cirrhotic rats with and without ascites had a lower systemic vascular resistance (2.6 +/- 0.2 and 3.9 +/- 0.4 mmHg ml(-1) x min x 100 g body weight, respectively) and higher portal pressure (14.6 +/- 0.6 and 11.3 +/- 1.8 mmHg) than control rats (6.5 +/- 0.3 mmHg x ml(-1) x min x 100 g BW and 6.8 +/- 0.2 mmHg, respectively, P < 0.05), and cirrhotic rats with ascites had the lowest systemic vascular resistance. Plasma levels of nitrate/nitrite progressively increased in relation to the severity of liver dysfunction (control rats, 2.7 +/- 0.5 nmol/ml; cirrhotic rats without ascites, 5.6 +/- 1.3 nmol/ml; cirrhotic rats with ascites, 8.3 +/- 2.2 nmol/ml; P < 0.05). Cirrhotic rats with ascites displayed higher plasma values of substance P (57.7 +/- 5.9 pg/ml) than cirrhotic rats without ascites (37.9 +/- 3.1 pg/ml, P < 0.05) and control rats (30.1 +/- 1.0 pg/ml, P < 0.05). There was no significant difference in plasma substance P values between control rats and cirrhotic rats without ascites (P > 0.05). No correlation was found between plasma levels of substance P and nitrate/nitrite (r = 0.318, P > 0.05). CONCLUSIONS: Excessive formation of NO may be responsible, at least partly, for the hemodynamic derangements in cirrhosis. Although substance P may not participate in the initiation of a hyperdynamic circulation in cirrhosis, it may contribute to the maintenance of the hyperdynamic circulation observed in cirrhotic rats with ascites.  相似文献   
57.
通过对已产生纵向裂缝、倾斜和基部风化剥蚀严重的高危烟囱的定向(向倾斜相反方向)倒塌爆破实践表明:设计中选用爆破参数及施工措施是有效的。  相似文献   
58.
Motivated by field data which showed a large number of link changeovers and incidences of link oscillations between in-service and out-of-service states in common channel signalling (CCS) networks, a number of analyses of the link error monitoring procedures in the SS7 protocol were performed by the authors. This paper summarizes the results obtained thus far and include the following: (a) results of an exact analysis of the performance of the error monitoring procedures under both random and bursty errors; (b) a demonstration that there exists a range of error rates within which the error monitoring procedures of SS7 may induce frequent changeovers and changebacks; (c) an analysis of the performance of the SS7 level-2 transmission protocol to determine the tolerable error rates within which the delay requirements can be met; (d) a demonstration that the tolerable error rate depends strongly on various link and traffic characteristics, thereby implying that a single set of error monitor parameters will not work well in all situations; and (e) some recommendations on a customizable/adaptable scheme of error monitoring with a discussion on their implementability. These issues may be particularly relevant in the presence of anticipated increases in SS7 traffic due to widespread deployment of advanced intelligent network (AIN) and personal communications service (PCS) as well as for developing procedures for high-speed SS7 links currently under consideration by standards bodies  相似文献   
59.
介绍了火烧山原油的物性与破乳剂结构和配比的关系、TA1031破乳剂的室内脱水评价及性能特点、TA1031的现场应用效果、破乳剂现场用药量与室内最佳用药量的关系、原油现场脱水过程中破乳剂用药量与污水含油的关系。  相似文献   
60.
文章阐述了实验窀检验在科研生产中的作用及发挥作用的巨大潜力。  相似文献   
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