Synthesis,Functionalization, and Bioconjugation of Monodisperse,Silica‐Coated Gold Nanoparticles: Robust Bioprobes

Herein, we report an efficient process for preparing monodisperse Au@SiO₂ nanoparticles using homogeneous shaking and without the use of surface‐coupling silane agents or large stabilizers. The resulting pure‐silica surface of the Au@SiO₂ nanoparticles is very important for straightforward surface functionalization with different functional groups via well‐established silica surface chemistry. Subsequent covalent bioconjugation of the aldehyde‐functionalized Au@SiO₂ nanoparticles with various biomolecules is successfully employed to make robust nanoprobes for fast, colorimetric DNA and protein detection based on the sequence‐specific hybridization properties of DNA and the specific binding affinity between proteins, respectively.     

Diagnosis and treatment of iatrogenic ureteral injury

Diagnosis and treatment of 17 patients who sustained 20 iatrogenic ureteral injuries were analyzed. Primary operations in which ureteral injury occurred are almost gynecologic procedures and general surgery. Injuries were managed by ureteroureterostomy in four, ureteral stent in one, removal suture ligation and ureteral double J-catheter in one, ureteroneocystostomy in ten, psoas-hitch technique and ureteroneocystostomy in one, nephrectomy in two. All patients with appropriate repair were followed-up periods of three to five years. Renal function of these patients had optimal results. When ureteral injury occurs, B-US, IVU, cystoscopy, retrograde ureterography or infusion of dye may be useful. An appropriate repair should be chosen according to length and position of ureteral injuries. Reoperation was optimal in two to three weeks. Immediate recognition of accidental ureteral injury provides optimal results. Patients with unrecognized injuries had suboptimal results.     

Ohmic contact and transport properties of II–VI Green/Blue laser diodes

The employment of the Zn(Se,Te) pseudo-graded contacting scheme to p-type ZnSe-based alloys contributes directly to the recent demonstration of room temperature continuous-wave operation of II– VI green-blue laser diodes. Contact ohmicity is maintained down to cryogenic temperatures which enabled the investigation of electrical transport properties associated with the p-type nitrogen-doped ZnSe, Zn(S,Se), and (Zn,Mg)(S,Se). The observation of both persistent photoconductivity and a metastable population of holes which are in thermodynamic equilibrium with hydrogenic acceptors having reduced activation energy suggests the presence of a DX-like behavior for holes in p-type (Zn,Mg)(S,Se).     

项目实训中的协同编程方法研究

在高职院校的软件项目实训环节中,大多项目需要团体协作进行编程。针对如果有效提高学生的协同编程效率、团队合作意识以及合作学习能力的问题,提出了基于Dillenbourg原则的协同编程方法。通过实践证明,该方法取得了良好的实训效果。     

Probability-confidence-kernel-based localized multiple kernel learning with lp norm

Localized multiple kernel learning (LMKL) is an attractive strategy for combining multiple heterogeneous features in terms of their discriminative power for each individual sample. However, models excessively fitting to a specific sample would obstacle the extension to unseen data, while a more general form is often insufficient for diverse locality characterization. Hence, both learning sample-specific local models for each training datum and extending the learned models to unseen test data should be equally addressed in designing LMKL algorithm. In this paper, for an integrative solution, we propose a probability confidence kernel (PCK), which measures per-sample similarity with respect to probabilistic-prediction-based class attribute: The class attribute similarity complements the spatial-similarity-based base kernels for more reasonable locality characterization, and the predefined form of involved class probability density function facilitates the extension to the whole input space and ensures its statistical meaning. Incorporating PCK into support-vectormachine-based LMKL framework, we propose a new PCK-LMKL with arbitrary l(p)-norm constraint implied in the definition of PCKs, where both the parameters in PCK and the final classifier can be efficiently optimized in a joint manner. Evaluations of PCK-LMKL on both benchmark machine learning data sets (ten University of California Irvine (UCI) data sets) and challenging computer vision data sets (15-scene data set and Caltech-101 data set) have shown to achieve state-of-the-art performances.     

The calcium-phosphorus and the simultaneous calcium-oxygen and calcium-sulfur equilibria in liquid iron

The equilibrium Ca₃P_2(s) = 3[Ca] + 2[P] was studied at 1600 ° by equilibrating liquid iron, saturated with Ca₃P₂, and contained in a TiN crucible, with Ca vapor. The source of Ca was liquid Ca contained in an Mo crucible, and the vapor pressure of Ca was varied by varying the position of the Mo crucible in the temperature gradient of a vertical tube furnace. A least-squares analysis of the data gave and. The simultaneous equilibria CaO_(s) = [Ca] + [O] and CaS_(s) = [Ca] + [S] were studied at 1600 ° by equilibrating liquid iron, contained in a pressed and sintered CaO-CaS crucible with Ca vapor. The advantage of this technique is that two equilibrium constants,K _cas andK _cao, and two interaction coefficients, and can be determined from one set of experiments. It was determined that, at 1600 °,K _cas = 5.9 × 10⁻⁸ K _cao = 5.5 × 10⁻⁹,, and. Formerly Graduate Students     

低电压氧化锌压敏电阻器的研究

研究了一种制造低电电压氧化锌压敏电阻器的方法。在基本成分的基础上适当加入二氧化钛可降低梯度电压（Ｖ１ｍＡ／ｍｍ），适量掺硼和改进热处理工艺可减小元件的漏电流和提高其稳定性。     

An Analytical Model Including Interface Traps and Temperature Effects in Negative Capacitance Double Gate Field Effect Transistor

Silicon - In this paper, an analytical model for negative capacitance double gate field effect transistor (NC-DG-FET) is proposed. This model includes interface traps and temperature effects, which...     

Measurement of the rheological properties of polymer melts with annular rheometer

An annular die has been designed having a very thin gap distance between two coaxial cylinders. The die was then used to measure wall normal stresses along the longitudinal direction of polymer melts flowing through the thin annulus. The materials investigated were high-density polyethylene, low-density polyethylene, polypropylene, and polystyrene. Also investigated were blends of polystyrene and polypropylene, and blends of polystyrene and high-density polyethylene The measurements of wall normal stresses were used to determine the rheological properties of the melts, namely, the melt viscosity from the slope of axial wall normal stress profiles and the melt elasticity from exit pressures. The interpretation of the experimental data was made possible by the fact that the narrow-gap annular die can be considered as a substitute for a thin slit die. It has been found that the results obtained in the present study are consistent with those reported earlier by the author, who at that time used both capillary and slit dies.     

Guerbet十四醇的合成与表征

以正庚醇为原料 ,通过Guerbet反应合成Guerbet十四醇 (2 戊基壬醇 ,C14 GA)。用IR、NMR和元素分析测定了C14 GA的结构 ,并研究了反应温度和用料比对其产率的影响。实验结果如下 :(1)在较优化的反应条件下 (正庚醇的总加入量为 1mol,在实验过程中 ,先加入 1/ 3mol庚醇和 1/ 4mol的KOH ,在 16 0℃下反应 2h ,然后再加入剩下的 2 / 3mol庚醇和 4g 5 %Pd -C催化剂 ,在 15 5℃下反应 6h)合成产物 ,其产率可达到 5 4 2 0 % ;(2 )所合成的产物与试图要得到的Guerbet十四醇 (2 戊基壬醇 ,C14 GA)含有相同的基团 (2×—CH3、10×—CH2 —、1×CH、1×—CH2 —O—和 1×—OH) ,而且 ,所合成的产物中 ,w (C) =79 0 6 % ,w (H ) =13 6 2 % ,与从Guerbet十四醇分子式计算的理论值w(C) =78 5 0 % ,w (H) =14 0 1%基本一致。可见所合成的产物正是Guerbet十四醇 (C14 GA)