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61.
62.
Iqra Hameed Lei Li Xiao Qiang Liu Xiang Ming Chen 《Journal of the American Ceramic Society》2022,105(3):2010-2019
(Mg1 − xCax)2SiO4 dense ceramics (x ≥ 0.15) were prepared, and their microwave dielectric characteristics were investigated together with the structure evolution. The sintering temperature for Mg2SiO4 ceramics was reduced significantly with Ca2+substitution. (Mg1 − xCax)2SiO4 ceramics exhibited a small increase in dielectric constant (εr) correlated with increased crystallite size, and ultra-high quality factor Qf value was achieved throughout the compositional range. Temperature coefficient of resonant frequency (τf) was considerably tuned from −70 ppm/°C to −33 ppm/°C, and this improvement was deeply linked with the decreased bond valance. At x = 0.075, (Mg1 − xCax)2SiO4 ceramics exhibited the best combination of microwave dielectric characteristics: εr = 7.2, Qf = 199,800 GHz at 26 GHz, τf = −33 ppm/°C. The present ceramics could be expected as promising candidate of dielectric materials for millimeter wave applications. 相似文献
63.
I. M. Inuwa Azman Hassan S. A. Samsudin M. K. Mohamad Haafiz M. Jawaid K. Majeed N. C. Abdul Razak 《应用聚合物科学杂志》2014,131(15)
Recently, graphene and its derivatives have been used to develop polymer composites with improved or multifunctional properties. Exfoliated graphite nanoplatelets (GNP) reinforced composite materials based on blend of polyethylene terephthalate (PET), and polypropylene (PP) compatibilized with styrene–ethylene–butylene–styrene‐g‐maleic anhydride is prepared by melt extrusion followed by injection molding. Characterization of the composites' microstructure and morphology was conducted using field emission scanning electron microscopy, transmission electron microscopy (TEM), X‐ray diffraction analysis (XRD), and Fourier transform infrared spectroscopy (FTIR). Tensile and impact strengths of test specimens were evaluated and the results showed maximum values at 3phr GNP in both the cases. Morphological studies showed that the GNPs were uniformly dispersed within the matrix. Results from XRD analysis showed uniformly dispersed GNPs, which may not have been substantially exfoliated. FTIR spectroscopy did not show any significant change in the peak positions to suggest definitive chemical interaction between GNP and the matrix. © 2014 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2014 , 131, 40582. 相似文献
64.
Rare earth-doped ZnO hierarchical micro/nanospheres were prepared by a facile chemical precipitation method and characterized by X-ray diffraction, field-emission scanning electron microscopy, energy-dispersive X-ray spectroscopy, UV-visible diffuse reflectance spectroscopy and photoluminescence spectroscopy. The results showed that the as-synthesized products were well-crystalline and accumulated by large amount of interleaving nanosheets. It was also observed that the rare earth doping increased the visible light absorption ability of the catalysts and red shift for rare earth-doped ZnO products appeared when compared to pure ZnO. The photocatalytic studies revealed that all the rare earth-doped ZnO products exhibited excellent photocatalytic degradation of phenol compared with the pure ZnO and commercial TiO2 under visible light irradiation. Nd-doped ZnO had the highest photocatalytic activity among all of the rare earth-doped ZnO products studied. The optimal Nd content was 2.0 at% under visible light irradiation. The enhanced photocatalytic performance of rare earth-doped ZnO products can be attributed to the increase in the rate of separation of photogenerated electron–hole pairs and hydroxyl radicals generation ability as evidenced by photoluminescence spectra. 相似文献
65.
66.
Rohanda Anis Waris Abdul Kurniadi Rizal Bakhri Syaiful Pardi Pardi Haryanto Dwi 《核技术(英文版)》2020,31(11):1-11
Nuclear Science and Techniques - This study presents the RF design of a linear accelerator (linac) operated in single-bunch mode. The accelerator is powered by a compressed RF pulse produced from a... 相似文献
67.
The potentials of silty clay(SC), acquired from Chaman, Balochistan, were investigated as adsorbent for Ni(Ⅱ)and Cd(Ⅱ) removal from contaminated media. The influence of different operating factors like dose, pH, temperature, and time of contact was explored, and optimum values were noted under batch adsorption method. Isothermal study was conducted with varying concentrations of solutions on optimized conditions and different adsorption models i.e., Langmuir, Freundlich, Temkin and Dubinin–Radushkevich(D–R) isotherm, which were employed to interpret the process. The isothermal data of both Ni(Ⅱ) and Cd(Ⅱ) were well fitted to Langmuir isotherm suggesting the formation of monolayer of metal ions on silty clay. The values of adsorption capacity noted for Ni(Ⅱ) and Cd(Ⅱ) were 3.603 mg·g~(-1) and 5.480 mg·g~(-)1, respectively. Kinetic studies affirmed that pseudo second order(PSO) kinetics was being obeyed by the removal of Ni(Ⅱ) and Cd(Ⅱ). Thermodynamic variables like free energy change(ΔG°), enthalpy change(ΔH°) and entropy change(ΔS°) were calculated. The negative value of ΔG° and the positive values of ΔH° and ΔS° unfolded that the removal process of both metal ions of by SC was spontaneous, endothermic and feasible. 相似文献
68.
Sabiha Sultana Haq Nawaz Bhatti Farah Yasmin Abdul Naeem Khan Imran Rehan Kamran Rehan Noor-ul-Amin 《应用聚合物科学杂志》2020,137(7):48376
In the current study, graphene oxide (GO) was prepared using green chemistry with modified Hummer's method without incorporating sodium nitrate (NaNO3). Solvent casting was employed to fabricate GO-doped poly(ethylene oxide) (PEO), that is, PEO/GO composites with various proportion of Na2SO4 and were then subjected to characterization via advanced spectroscopic techniques for different physicochemical aspects to estimate their potential applications as marketable products. XRD analysis explored that fabricated composites are more crystalline than neat PEO. PEO/GO/Na2SO4 composite films offered maximum crystallinity. SEM displayed the same trend. TG/DTA thermogram exposed better thermal stability than pristine polymer. FTIR studies confirmed complexation among hybrid's components. Elongation-at-break and Young's modulus displayed an enhancing behavior with an incremental loading of salt and filler. In terms of mechanical performance, composite of PEO with 0.37 wt % GO and 0.08 g salt was found to be an ideal composition during the course of study. © 2019 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2020 , 137, 48376. 相似文献
69.
Industrialization has led to a number of environmental problems, such as release of toxic metals and other toxic organic and inorganic compounds to the environment. Among all, the rapid expansion of leather related industries in Pakistan have resulted in considerable environmental problems and effluents from processing of both domestic and imported hides and skins have increased pollution to alarming levels. Some tannery effluents of Peshawar area investigated in the present study showed high concentrations of Cr(Ⅵ) (2.7-12.6 mg/L), Cu(Ⅱ) (2.6-11.4 mg/L) and phenol (0.1-4.2 mg/L). These contaminants are very toxic and must be removed from effluents before releasing into water bodies. A new technique of gamma irradiation has been investigated to decrease the load of COD and concentrations of Cr(Ⅵ), Cu(Ⅱ) and phenol associated with tannery effluents to the permitted values. It was observed that concentration of Cr(Ⅵ) in the effluents can be brought to the permitted level by applying radiation dose of 3 kGy. A radiation dose of 2.5 kGy was required to remove more than 95% of Cu(Ⅱ) and 100 % degradation of phenol in tannery effluents could be achieved by only one kGy of radiation dose. 相似文献
70.
The effects of physical refining on the formation of 3-monochloropropane-1,2-diol esters in relation to palm oil minor components 总被引:2,自引:0,他引:2
The formation of 3-monochloropropane-1,2-diol (3-MCPD) esters in refined palm oil during deodorisation is attributed to the intrinsic composition of crude palm oil. Utilising D-optimal design, the effects of the degumming and bleaching processes on the reduction in 3-MCPD ester formation in refined palm oil from poor-quality crude palm oil were studied relative to the palm oil minor components that are likely to be their precursors. Water degumming remarkably reduced 3-MCPD ester formation by up to 84%, from 9.79 mg/kg to 1.55 mg/kg. Bleaching with synthetic magnesium silicate caused a further 10% reduction, to 0.487 mg/kg. The reduction in 3-MCPD ester formation could be due to the removal of related precursors prior to the deodorisation step. The phosphorus content of bleached palm oil showed a significant correlation with 3-MCPD ester formation. 相似文献