Attenuation of ultrasonic waves in V, Nb and Ta at low temperatures

Variation of ultrasonic attenuation and velocities with temperature have been evaluated in the temperature range 5-50 K due to electron-phonon interaction mechanism in transition metals vanadium, niobium and tantalum for longitudinal and shear waves. For this evaluation, we have also computed the second order elastic constants using Morse potential. Behaviour of acoustical phonons in these bcc metals is different from other normal metals, intermetallics, semimetallics and alloys. Some characteristic features of these materials connected to ultrasonic parameters are discussed.     

Amperometric determination of tyramine in sauce and beer by epoxy resin biocomposite membrane bound tyramine oxidase

A method is described for construction of an amperometric biosensor for specific determination of tyramine, using black gram tyramine oxidase immobilized covalently on an epoxy resin membrane. The biosensor had optimum response within 10 s at pH 8.5 and 35 °C. A linear relationship was observed between tyramine concentrations and current (mA) in the range of 0.24 to 3.47 mg/dL. The biosensor was employed for determination of tyramine in beer and sauce. The detection limit of sensor was 0.24 mg/dL. The mean analytical recovery of added tyramine (0.5 and 1.0 mg/dL) was 97.3 ± 2.3 and 95.9 ± 3.4%. Within and between batch coefficient of variation were 5.1 and 5.34%, respectively. Enzyme electrode showed 35% loss in its initial activity after its regular use over a period of 2 months. The biosensor has the advantage that it does not suffer from leaching of enzyme and measures tyramine specifically.     

Isatin compounds as corrosion inhibitors for N80 steel in 15% HCl

The inhibition effect of two synthesized isatin compounds namely 1-morpholinomethyl-3-(1-N-dithiooxamide)iminoisatin [MMTOI] and 1-diphenylaminomethyl-3-(1-N-dithiooxamide)iminoisatin [PAMTOI] on the corrosion inhibition of N80 steel in 15% HCl solution was studied by polarization, EIS and weight loss measurements. It was found that both the inhibitors were effective and their inhibition efficiency was significantly increased with increasing concentration. Polarization curves revealed that the used inhibitors represent mixed-type inhibitors. Adsorption of these inhibitors led to a reduction in the double layer capacitance and an increase in the charge transfer resistance, and was found also to obey Langmuir isotherm.     

NAFLA – Ein Simulationswerkzeug zur analytischen Abschätzung von Schadstofffahnenlängen

Groundwater pollution with organic contaminants remains a world-wide problem. Before selection of any remediation technique, it is important to pre-assess contaminated sites with respect to their hazard. For this, several analytical and numerical approaches have been used and an initial assessment of contaminated sites the MS-Excel^© tool “NAFLA” was developed. “NAFLA” allows a quick and straightforward calculation and comparison of some analytical approaches for the estimation of maximum plume length under steady-state conditions. These approaches differ from each other in source geometry, model domain orientation, and in the consideration of (bio)chemical reaction within the domain. In this communication, we provide details about the development of “NAFLA”, its possible usage and information for users. The tool is especially designed for application in student education, by authorities and consultants.     

Implementation Issues in Turbo Decoding for 3GPP FDD Receiver

In the Frequency Division Duplex (FDD) mode of the Third Generation Partnership Project (3GPP) standard, implementation of the turbo decoder, especially for the mobile equipments, faces design decisions related to computational complexity, power efficiency, and memory requirements. In this paper we compare different approaches of low complexity implementation of the turbo decoder, with emphasis on the issues of signal scaling and quantization, the sliding window operation for memory size reduction and the iteration stopping algorithms. The demodulated signal at the output of the RAKE receiver may have a wide dynamic range and it may require many bits of precision. In order to overcome the numerical precision problem and to prevent Log Likelihood ratio (LLR) metric overflow, a scaling algorithm must be used. Our simulation results indicate that the Average Absolute (AA) algorithm using dynamic scaling outperforms other scaling schemes and it is less sensitive to the channel conditions. One of the major challenges in the implementation of a practical turbo decoder is optimization of memory requirements. In this paper we evaluate the performance of the sliding window algorithm using different main and guard window sizes. We show that the bit and block error rate performance of the sliding window scheme mainly depend on the guard window size rather than the main window size. The simulation results indicate that small guard window sizes can significantly decrease the iteration gain for large frames in fast fading channels. Iteration stopping algorithms reduce the power consumption and the latency of the decoder and help to dedicate more resources to other functions of the receiver. The block error distribution in the fading channels makes it even more essential to use an iteration stopping rule. Our simulations conclude that a rule called the minimum absolute value appears to be a very effective, low complexity and robust algorithm. Mohamadreza Marandian Hagh was born in Tabriz, Iran on January 1974. He received the B.S. and the M.S. degrees in electrical engineering from Tehran University with honors in 1996 and 1999, respectively. He is pursuing the Ph.D. degree in electrical engineering at Northeastern University, Boston. His research interests includes information theory, channel coding and iterative techniques for wireless communication systems. His current research is focused on low complexity designs for iterative receivers using Space-Time coding in time-dispersive channels. He is also interested in Exit-Chart analysis of iterative receivers. From 1996 to 1999, he was with Sana Pro Inc. as a system engineer, developing simulation tools for OFDM, WCDMA, CDMA2000. He is currently with Airvana Inc. in Chelmsford, MA and working on 1xEVDO wireless systems. Masoud Salehi received BS degree (Summa Cum Laude) from Tehran University and MS and Ph.D. degrees from Stanford University all in Electrical Engineering. Before joining Northeastern, he was with the Departments of Electrical and Computer Engineering, Isfahan University of Technology and Tehran University. From February 1988 to May 1989 Dr. Salehi was a visiting professor at the Information Theory Research Group, Department of Electrical Engineering, Eindhoven University of Technology, The Netherlands, where he did research in network information theory and coding for storage media.In 1989 Dr. Salehi joined Department of Electrical and Computer Engineering, Northeastern University. Professor Salehi is a member of the CDSP (Communication and Digital Signal Processing) Center. His main areas of research interest are network information theory, source-channel matching problems in single and multiple user systems, data compression, turbo coding, coding for fading channels, and digital watermarking. Professor Salehi’s research has been supported by research grants from the National Science Foundation (NSF), GTE, NUWC, CenSSIS, and Analog Devices. Professor Salehi has also done consulting to the industry including Teleco Oilfield Services and AT&T. Professor Salehi is currently a member of the Editorial Board of The International Journal of Electronics and Communications.Professor Salehi is the coauthor of the textbooks “Communication Systems Engineering”, Prentice-Hall 1994, 2002, “Contemporary Communication Systems Using MATLAB and Simulink” Thomson 1998, 2000, 2004, and “Fundamentals of Communication Systems”, Prentice-Hall 2005. Abhay Sharma received B.E. (Hons) Electrical and Electronics Engineering degree from Birla Institute of Technology and Science, Pilani, India in 1996 and M.S. Electrical Engineering degree from Ohio State University, Columbus in 2000. From 2000 to 2005 he was working with Analog Devices, RF and Wireless Systems Group, Wilmington, USA, where he was working on design and implementation of algorithms for the emerging cellular communication standards. Currently he is working with Allgo Embedded Systems, Bangalore, India, in the area of wireless networks and systems based on the emerging W-PAN wireless technologies. Zoran Zvonar received the Dipl. Ing. degree in 1986 and the M.S. degree in 1989, both from the Department of Electrical Engineering, University of Belgrade, Yugoslavia, and the Ph.D. degree in Electrical Engineering from the Northeastern University, Boston, in 1993.From 1986 to 1989 he was with the Department of Electrical Engineering, University of Belgrade, Belgrade, Yugoslavia, where he conducted research in the area of telecommunications. 1993 to 1994 he was a Post-Doctoral investigator at the Woods Hole Oceanographic Institution, Woods Hole, MA, anconducted research on multiple-access communications for underwater acoustic networks. Since 1994 he has been with the Analog Devices, Communications Division, Wilmington, USA. He is the Manager of the Systems Engineering Group focusing on the design of algorithms and architectures for wireless communications, with emphasis on integrated solutions and real-time software.He was a Guest Editor of the IEEE Transactions on Vehicular Technology, the International Journal of Wireless Information Networks and the ACM/Baltzer Wireless Networks, Associate Editor of the IEEE Communications Letters and a co-editor of the books GSM: Evolution Towards Third Generation Systems, Kluwer Academic Publishers, 1998, Wireless Multimedia Networks Technologies, Kluwer Academic Publishers, 1999 and Software Radio Technologies: Selected Reading, IEEE Press, 2001. Dr. Zvonar is currently Co-Editor of the Radio Communication Series in the IEEE Communications Magazine.     

Synthesis and characterization of Cu nanotubes and nanothreads by electrical arc evaporation

We report the formation and characterization of copper nanostructures, nanotubules and nanothreads, which were obtained by electrical arc evaporation of Cu electrodes under varied conditions of He ambience. Electrical arc evaporation was done with approximately 10 V and (approximately 50-100 A) DC current. The current was used in a pulse mode. The evaporated material was condensed on a formvar-coated Cu grid mounted on a liquid N2-cooled specimen holder. Transmission electron microscopy was employed to characterize the condensed materials. These investigations revealed that the condensed materials consisted of the mentioned nanostructures. Nanotubes and nanothreads are formed for a He pressure in the chamber corresponding to approximately 140 and approximately 500 torr, respectively. Extensive electron microscopic investigations showed that the diameter of the nanotubes varied from approximately 5 nm to approximately 50 nm and their length from 2 microns to 3 microns.     

A multi-sensor climatological view of double ITCZs over the Indian Ocean

We characterize the climatological features of the double inter-tropical convergence zones (DITCZs) over the western Indian Ocean during November–December by a synergistic analysis of the Hamburg Ocean Atmosphere Parameters and Fluxes from Satellite (HOAPS III) data (1988–2005) and the National Aeronautics and Space Administration's (NASA's) A-Train data (2002–2009). We investigate rainfall, freshwater flux and cloud liquid water, cloud fraction and relative humidity over the DITCZs. In addition, the daily rainfall data from the Global Precipitation Climatology Project (GPCP) are used to document the DITCZs during the El Niño southern oscillation (ENSO) events. An analysis of the GPCP data shows that the DITCZs are clearly discernible during strong ENSO events (1997, 2002 and 2006), in sharp contrast to the DITCZs in the eastern Pacific Ocean, where they are absent during ENSOs. Further, these convergence zones on either side of the equator are of short duration, approximately 3–6 pentads during November and December. All satellite sensor data sets consistently capture the major features of DITCZs. As an accurate simulation of DITCZs in coupled global climate models remains a challenge, the results from the present study would provide a platform for evaluating these models.     

Gold Nanoparticles and g‐C3N4‐Intercalated Graphene Oxide Membrane for Recyclable Surface Enhanced Raman Scattering

Toxic organic pollutants in the aquatic environment cause severe threats to both humans and the global environment. Thus, the development of robust strategies for detection and removal of these organic pollutants is essential. For this purpose, a multifunctional and recyclable membrane by intercalating gold nanoparticles and graphitic carbon nitride into graphene oxide (GNPs/g‐C₃N₄/GO) is fabricated. The membranes exhibit not only superior surface enhanced Raman scattering (SERS) activity attributed to high preconcentration ability to analytes through π–π and electrostatic interactions, but also excellent catalytic activity due to the enhanced electron–hole separation efficiency. These outstanding properties allow the membrane to be used for highly sensitive detection of rhodamine 6G with a limit of detection of 5.0 × 10^?14m and self‐cleaning by photocatalytic degradation of the adsorbed analytes into inorganic small molecules, thus achieving recyclable SERS application. Furthermore, the excellent SERS activity of the membrane is demonstrated by detection of 4‐chlorophenol at less than nanomolar level and no significant SERS or catalytic activity loss was observed when reusability is tested. These results suggest that the GNPs/g‐C₃N₄/GO membrane provides a new strategy for eliminating traditional, single‐use SERS substrates, and expands practical SERS application to simultaneous detection and removal of environmental pollutants.