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131.
Mansour N. Ben Djeridi W. Mir L. El 《Journal of Inorganic and Organometallic Polymers and Materials》2021,31(11):4360-4371
Journal of Inorganic and Organometallic Polymers and Materials - Nanoporous carbon matrix was prepared by the sol–gel process from pyrogallol-formaldehyde (PF) mixtures in water using picric... 相似文献
132.
V. Devadoss M. Noel K. Jayaraman C. Ahmed Basha 《Journal of Applied Electrochemistry》2003,33(3-4):319-323
The redox behaviour of Mn3+/Mn2+, Co3+/Co2+ and Ce4+/Ce3+ mediators commonly used in indirect oxidation of organic compounds were evaluated in methane sulfonic acid on a glassy carbon working electrode employing cyclic voltammetry. Manganic methanesulfonate exhibits higher instability in dilute methanesulfonic acid. The solid MnO2 formed during disproportionation on the glassy carbon electrode further affects the reproducibility. Cobaltic methanesulfonate formation occurs only at oxygen evolution region rendering the overall oxidation process less efficient. Ceric methane sulfonate formation is highly efficient over a wide acid concentration range. Ceric methanesulfonate can also be employed over a wide temperature range to oxidize different aromatic compounds. 相似文献
133.
A. H. M. Ahmed H. F. W. Taylor 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》1969,19(9):245-246
The stability relationships of xonotlite, foshagite and hillebrandite relative to kilchoanite and calcio-chondrodite have been studied under saturated steam pressures at 180° and 250°. Kilchoanite was unstable relative to xonotlite plus hillebrandite at 180°, or to foshagite plus hillebrandite at 250°; calcio-chondrodite was unstable relative to hillebrandite plus some more lime-rich phase, possibly Ca(OH)2, at both temperatures. Foshagite was stable relative to xonotlite plus hillebrandite at 250°, but unstable relative to these phases at 180°. 相似文献
134.
Smith Robert El. Wekstein David R. Sullivan Robert H. 《IEEE transactions on bio-medical engineering》1970,(2):151-156
A multiplexing, demodulating, and recording telemetry system designed to process multiple pulse-coded temperature channels is described. The system provides complete control of recording and multiplexing sequences and timing, and gives a single analog signal in response to each sample of pulse-coded data. It identifies all channels and indicates to a computer when a new data sample is to be processed. The system is self-calibrating to maintain accuracy over extended data collection periods, and is inexpensive. 相似文献
135.
The properties of styrene/butadiene copolymers obtained by conventional emulsion and miniemulsion polymerizations were studied. Thin layer chromatography with flame ionization detection was used to determine the gel fraction of the copolymer in the latex particles as a function of conversion. It was found that the gel formation began at a higher conversion in the miniemulsion polymerization when compared with that in the conventional process. Also, a lower glass transition temperature was noted at the lowest conversion sampled (~25%), implying a higher initial butadiene monomer concentration within the nucleated miniemulsion monomer droplets when compared with particles formed conventionally. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 4616–4622, 2006 相似文献
136.
A. H. Moinuddin Ahmed Lesley S. Dent Glasser 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》1973,23(6):457-463
α-BaO.Al2O3.4H2O has been synthesised and studied by infrared, X-ray and thermal analytical techniques. The compound of approximate formula BaO.Al2O3.0.5H2O, described in Part III, forms as a dehydration product, and appears to be identical with the compound β-BAH2 described by other workers. A possible explanation for the discrepancy in water content is discussed. 相似文献
137.
Styrene/hexadecane miniemulsions were polymerized at 50°C using a redox initiator. The miniemulsions and their corresponding latexes were characterized in terms of size, polymerization rate, and surface properties. The resulting data were analyzed to elucidate the miniemulsion stabilization and polymerization mechanisms. It was found that the free surfactant concentration exceeded the critical micelle concentration when large amounts of surfactant (60 mM sodium lauryl sulfate) were used, resulting in simultaneous micellar and droplet nucleation. Most surfactant was on the surface of the droplets (85%) or particles (95%). The fractional surface coverage was proportional to the surfactant concentration to the 0.55 power. Using a particle diameter equation, the number of particles was calculated to be proportional to the surfactant concentration to the 1.35 power. Through direct particle size measurements, a power of 1.38 was confirmed. The rate of polymerization was determined by reaction calorimetry to be proportional to the number of particles to the 0.59 power, in contrast to classical Smith–Ewart kinetics for conventional emulsions (1.0 power). The average number of radicals per particle was estimated from the rate and number data, and varied with the particle diameter to the 0.97 power. The observed kinetic dependencies were validated through an extension of Smith–Ewart theory. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 90: 3987–3993, 2003 相似文献
138.
Issam El Gmati Pierre Francois Calmon Ali Boukabache Patrick Pons Hatem Boussetta Mouhamed Adel Kallala Kamel Besbes 《Microsystem Technologies》2014,20(6):1085-1091
In this work, RF MEMS continuous reversible variable inductor has been fabricated by using microelectronic technology and lamination process. We review, evaluate and compare this variable inductor with other work. The proposed inductor is a dual circular coil and has an inductance of few nH. The fundamental idea is to place a liquid droplet between the metal turns of a coil in order to modify the capacitive/resistive coupling between metal tracks and hence to change the stored magnetic energy. The SU-8 resin was used to realize the microfluidic channels and Au as metallic tracks. To prove the reversibility of the inductor, two cases were studied: filling and emptying of channels. The tuning range of the inductance is approximately 107 % at 1.6 GHz, making these devices very suitable as building blocks in many RF applications. 相似文献
139.
Cotton and cotton/polyester fabrics were treated against microbial attack by applying a formulation based essentially on ZnO under high‐energy radiation and thermal curing. To achieve the homogeneity and the reactivity of the treating formulation, a binder (Impron MTP) and a dispersing agent (Setamol WS) were used with ZnO. The antimicrobial property of the fabrics was evaluated, in terms of mechanical properties, by a soil burial test. Moreover, the effect of antimicrobial finishing on the dyeing properties in terms of color strength was investigated. It was found that the best composition that affords the best antimicrobial protection to cotton fabrics contains 2% ZnO, 2% binder, and 1% dispersing agents. For the cotton/polyester blend, the best results were achieved at the same conditions except the ZnO was 1%. It was found that the treatment under the effect of electron‐beam irradiation is better than that of gamma irradiation and thermal curing. The results showed that when the finishing process was carried out before dyeing with a reactive dye, it affects the color strength rather than performing the finishing after the dyeing process. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 88: 1129–1137, 2003 相似文献
140.
Ghurmallah H. Al‐Ghamdi E. David Sudol Victoria L. Dimonie Mohamed S. El‐Aasser 《应用聚合物科学杂志》2006,101(6):4504-4516
Miniemulsification technology was used to encapsulate TiO2 particles inside a styrene/n‐butyl acrylate copolymer with high loading levels (11 to 70% PVC (pigment volume concentration)). In this approach, a St/BA copolymer dissolved in toluene in the presence of a costabilizer (hexadecane) was mixed with a dispersion of TiO2 particles in toluene and sonified, and then emulsified in an aqueous surfactant solution by sonification. The effect of sonification time on both the dispersibility of the TiO2 particles in the presence of the copolymer and hexadecane and on the encapsulated particle size was investigated. Particle size analysis by dynamic light scattering showed that these composite latexes are quite stable. It was also found that as the TiO2 loading increased from 11 to 43% PVC, the particle size of the TiO2 dispersion decreased while the polymer‐encapsulated TiO2 particle size increased. The effect of surfactant concentration (sodium lauryl sulfate, SLS) on the encapsulated particle size was investigated using four different SLS concentrations in the 11% PVC system. The results showed that as the SLS concentration increased the particle size decreased, as expected. Also it was found that the minimum surfactant concentration that gives stable encapsulated TiO2 particles is above 10 mM SLS. The role of HD in the recipe was studied for an artificial latex containing no TiO2 and one prepared at 11% PVC, in terms of particle size before and after solvent stripping, and its effect on the Tg. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 101: 4504–4516, 2006 相似文献