HVEM study of crack-tip dislocations in Si crystals prepared by FIB and twin-blade cutting method

Crack-tip dislocations in silicon crystals have been examined by using high-voltage electron microscopy. Cracks were introduced by the Vickers indentation method at room temperature and the indented specimens were annealed at high temperatures to induce dislocations around crack tips under the presence of residual stress due to the indentation. A selected area around a crack tip was thinned by a focused ion beam (FIB) technique. Specimens were thinned in advance by a twin-blade cutting (TBC) method, which is a simple cutting process for saving FIB machine time. A combination of FIB and TBC can be a useful thinning procedure for the efficient preparation of transmission electron microscopy specimens. Characteristic dislocation structures were observed around the tip of a crack, aiding the elucidation of dislocation processes, which is essential to increase the fracture toughness of materials.     

Polynucleotides. XLV Synthesis and properties of poly(2'-azido-2'-deoxyinosinic acid)

Poly (2'-azido-2'-deoxyinosinic acid), [poly (Iz)], was synthesized from 2'-azido-2'-deoxyinosine diphosphate by the action of polynucleotide phosphorylase. Poly (Iz) has UV absorption properties similar to poly (I) and hypochromicity of 11% at 0.15M Na+ and neutrality. In solutions of high Na+ ion concentration, poly (Iz) forms a multi-stranded complex and its Tm at 1.0M Na+ ion concentration was 43 degrees. Upon mixing with poly (C), poly (Iz) forms a 1:1 complex having a Tm lower than that of poly (I)-poly (C) complex in the same conditions. The effect of substitution at the 2'-position of the poly (I) strand was discussed in relation to the interferon-inducing activity.     

EACLE : Energy-Aware Clustering Scheme with Transmission Power Control for Sensor Networks

In this paper, we propose a new energy efficient clustering scheme with transmission power control named “EACLE” (Energy-Aware CLustering scheme with transmission power control for sEnsor networks) for wireless sensor networks, which are composed of the following three components; “EACLE clustering” is a distributed clustering method by means of transmission power control, “EACLE routing” builds a tree rooted at a sink node and sets the paths from sensor nodes taking energy saving into consideration, and “EACLE transmission timing control” changes the transmission timing with different levels of transmission power to avoid packet collisions and facilitates packet binding. With an indoor wireless channel model which we obtained from channel measurement campaigns in rooms and corridors and an energy consumption model which we obtained from a measurement of a chipset, we performed computer simulations to investigate the performance of EACLE in a realistic environment. Our simulation results indicate that EACLE outperforms a conventional scheme such as EAD (Energy-Aware Data-centric routing) in terms of communication success rate and energy consumption. Furthermore, we fully discuss the impact of transmission power and timing control on the performance of EACLE.     

Dynamic flying characteristics of an air bearing slider over a disk with grooves and distribution of material properties

Bit-patterned media (BPM) consisting of land parts for read/writing and grooves, which are almost filled with non-magnetic materials to prevent magnetic interference between recording bits, are considered to be promising media for achieving ultrahigh density recording. A flying head slider flying over a BPM disk suffers from variations in both the spacing and van der Waals (vdW) attractive forces, which induce slider vibrations and spacing fluctuations. In the present study, we considered that BPM disks not only have a groove depth distribution, but that they also have a distribution of material properties (e.g., refractive index), which gives rise to a distribution in the vdW force. In the dynamic responses of sliders with small groove depths and a small variation in the refractive index, spacing fluctuations are found to be a superposition of fluctuations due to slider behaviors (1) over a disk with transverse grooves in a uniform material with a uniform refractive index (Case 1) and (2) over a flat disk with a refractive index distribution (Case 2). When the effects of Cases 1 and 2 cancel each other, the spacing fluctuations for the two cases cancel each other, reducing the total spacing fluctuation.     

Near-net-shape forming of Al-Al3Ni functionally graded material over eutectic melting temperature

A possibility to make near-net-shape functionally graded material (FGM) products has been examined. The FGM billets having a graded volume fraction of Al₃Ni in thickness direction were machined from an Al-Al₃Ni FGM thick-walled tube manufactured by a vacuum centrifugal method. Billets, which were set in the container for the backward extruding, were heated to 650 °C to 680 °C, at which temperature the FGM becomes a mixture of molten aluminum eutectic and solid intermetallics. Then, billets were extruded successfully to FGM cups by a semisolid forming, except at 650 °C. Residual bulky Al₃Ni particles are found at higher temperature. Thus, an optimum operation temperature is found to be around 660 °C, because bulky Al₃Ni particles transform to fine spheroidal or fibrous shape after the forming. The volume fraction of intermetallics at the bottom region of the cup was condensed more than 60 vol pct in a proper billet setting.     

Development of multianode photomultiplier tube

We have developed a multianode photomultiplier tube (MAPMT) which has a sensitive cathode diameter of 36 mm and an anode with 88 segments. The position sensitivity of the tube was studied by using light from a LED and scintillation light from a scintillation-fiber bundle. We observed particle tracks for the first time by using a single photomultiplier tube.     

Large-Scale Shake Table Experiment and Numerical Simulation on the Nonlinear Behavior of Pile-Groups Subjected to Large-Scale Earthquakes

This paper describes the results of large-scale shake-table experiments involving a 3×3 pile-group. The pile-group was embedded in dry sand and subjected to sinusoidal waves and an earthquake motion recorded from the 1995 Hyogo-ken Nanbu (Kobe) earthquake. The load transfer between soil and pile was derived and the group effect was captured. Numerical simulations were also performed using a Beam-on-Nonlinear-Winkler-Foundation approach with a new hysteretic p-y curve. A comparison of the experimental and numerical results revealed that the numerical simulation is capable of accounting for the soil-pile interaction observed in the experiment.     

Development of fabrication process for Ag/polydiacetylene (core/shell) hybridized nanocrystals

Core/shell hybridized nanocrystals composed of Ag nanoparticle core and polydiacetylene shell were fabricated successfully by means of “co-reprecipitation/microwave irradiation method”. The hybridized nanocrystals were characterized using transmission electron microscopy (TEM) observation and UV–vis absorption spectroscopy. UV–vis spectral measurements revealed that polydiacetylene shell was the red phase while π-conjugated backbone is distorted. Detailed mechanism of formation of the red phase was discussed.     

Millimeter-Wave Radiometer for the Measurement of Stratospheric ClO Using a Superconductive (SIS) Receiver Installed in the Southern Hemisphere

A new sensitive radiometer for atmospheric minor constituents has been developed by Nagoya University and the National Institute for Environmental Studies (NIES). The instrument equipped low-noise superconducting (SIS) mixer with a system noise temperature of ≈200K (SSB) at 204GHz. The SIS mixer is operated in a single side band mode with a side band ratio grater than 10dB by adjusting the two tunable backshorts of the mixer. Since any additional SSB filters are not necessary, we can simplify the quasi-optical system and reduce the standing waves which makes difficult to achieve a flat spectral baseline. We installed the observation system at Las Campanas Observatory, Chile in December 1999, and started the test observation from 2000 October. We have detected significant ClO emission at 204.3 GHz with an actual observation time of only 4 hours. This is the first detection of the ClO at 40km altitude from the mid-latitude region of the southern hemisphere. The Nagoya-NIES system has enabled continuous monitoring of ClO in the stratosphere with a time resolution of 4 or 5 hours.