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81.
Wang Wenhai Tesio Alvaro Y. Olivares-Marín Mara Gómez Romero Pedro Tonti Dino 《Journal of Materials Science》2022,57(28):13403-13413
Journal of Materials Science - A simple route has been developed for the preparation of mesoporous graphitic carbons with embedded cobalt nanoparticles just using glycine as a nitrogen source,... 相似文献
82.
Cañizares P Carmona M Baraza O Delgado A Rodrigo MA 《Journal of hazardous materials》2006,131(1-3):243-248
In this work the adsorption of phenol solutions onto activated carbon Calgon F400 has been studied. The carbon was modified by acid treatment, using soxhlet extraction with hydrochloric acid 2N for 120 cycles. The treatment did not affect significantly the surface area of the activated carbon but affected significatively the different functional groups, and thus its adsorption properties. Tóth model reproduced satisfactorily the experimental isotherm data and an adsorption enthalpy of -17.9 kJ mol-1 was found, which indicates that the process is exothermic. The pH affected significatively to the adsorption process and an empirical polynomial equation was able to reproduce maximum capacity as a function of pH. The isotherms obtained at pH 3 and 7 are very similar and showed a higher adsorption capacity compared with that obtained at pH 13. The use of phosphate buffer solutions decreased the maximum phenol adsorption capacity, due to the competitive adsorption between the phenol and phosphates. Finally, it was demonstrated that the acid treatment introduced chloride ions into the carbon, giving it properties of ion exchanger. 相似文献
83.
Christof Huebner Rachel Cardell‐Oliver Stefan Hanelt Tino Wagenknecht Alvaro Monsalve 《Wireless Communications and Mobile Computing》2013,13(17):1499-1510
Wireless sensor networks for environmental monitoring and agricultural applications often face Long‐range requirements at low bit rates together with a large numbers of nodes. This paper presents the design and test of a novel wireless sensor network that combines a large radio range with very low power consumption and cost. Our asymmetric sensor network uses ultra‐low‐cost 40‐MHz transmitters and a sensitive software‐defined radio receiver with multi‐channel capability. Experimental radio range measurements in two different outdoor environments demonstrate a single‐hop range of up to 1.8 km. A theoretical model for radio propagation at 40 MHz in outdoor environments is proposed and validated with the experimental measurements. The reliability and fidelity of network communication over longer periods is evaluated with a deployment for distributed temperature measurements. Our results demonstrate the feasibility of the transmit‐only low‐frequency system design approach for future environmental sensor networks. Although there have been several papers proposing the theoretical benefits of this approach, to the best of our knowledge, this is the first paper to provide experimental validation of such claims. Copyright © 2011 John Wiley & Sons, Ltd. 相似文献
84.
This paper presents a discrete formulation of the nonlinear minimum weight design of welded connections, in which global throat stresses along every fillet are approximated by piecewise linear shape functions. With this formulation it is possible to find the set of throat thicknesses of a welded connection that gives the minimum amount of weld metal necessary to support an arbitrary set of external actions and a stress field in equilibrium with these actions and satisfying a strength criterion. The formulation adopted involves a linear form of objective function and equilibrium equations, which, together with the convex character of the nonlinear constraints, gives a full convex set of constraints and consequently a global optimum of the objective function. Moreover, the structure of the set of constraints makes it possible to demonstrate that stress and throat thickness values are unique at the optimum, which allows the optimum stress distributions to be simplified, to establish practical design recommendations. Realistic conditions can be imposed on the stress field. The problem is solved with a very accessible and well-known scientific library, which allows this method to be implemented by anyone involved in welding practice. The method proposed is developed for the case of a planar connection. Two practical applications using the strength criterion of Eurocode 3 are included, discussing the results obtained for two types of common arrangements and showing that numerical results are consistent and CPU times reasonably low. 相似文献
85.
86.
87.
S Aksoylar S Ak?it S Ca?layan I Yaprak R Bakiler F Cetin 《Canadian Metallurgical Quarterly》1997,39(2):215-217
A case of large fronto-temporo-parietal epidural hematoma associated with ipsilateral retrobulbar hematoma is reported. A 24-year-old man soon after a head injury due to a traffic accident became comatose with anisocoria and hemiplegia and developed exophthalmos, conjuctival chemosis, downward and lateral displacement of the eyeball. CT scan of the brain and the orbit showed the large epidural clot communicating with an ipsilateral retrobulbar hematoma through a sphenoid bone fracture. The patient underwent emergency surgery. Postoperatively, he improved and was discharged in good conditions. On follow-up one month later he was symptoms free. The available literature is reviewed: our case seems to be the fifth reported. 相似文献
88.
Verónica López Calvo Mónica Vicent Cabedo Emilie Bannier Eugeni Cañas Recacha Aldo R. Boccaccini Luis Cordero Arias Enrique Sánchez Vilches 《Journal of Materials Science》2014,49(23):7933-7942
45S5 bioactive glass powders with the composition of 45 SiO2, 6 P2O5, 24.5 CaO and 24.5 wt% Na2O were melted and quenched in water to obtain a frit. The frit was milled using two different routes: dry milling followed by sieving to obtain glass particles and wet milling followed by spray drying to obtain a powder comprising porous agglomerates. All feedstocks showed adequate characteristics that make them suitable to be deposited by atmospheric plasma spraying. The powders and coatings were characterised by field-emission gun environmental scanning electron microscope and X-ray diffraction. The roughness and the contact angle of the coatings were also determined. The bioactivity of the powders and coatings was assessed by immersion in simulated body fluid. It was found that bioactive glass prepared from bioglass frit by dry milling exhibited similar bioactivity as that of a commercial bioactive glass. All coatings produced showed good adhesion to the substrate as well as suitable surface properties to ensure efficient contact with body fluid. Regardless of the characteristics of the feedstocks or plasma spray conditions used, all coatings were exclusively made up of an amorphous phase. On the other hand, micrographs revealed that the characteristics of the feedstock strongly impact on the final coating microstructure. The most homogeneous microstructure was obtained when the feedstock was prepared by fine dry grinding of the frit. For this coating, the formation of a bioactive layer was also proved by Fourier transform infrared spectroscopy and X-ray diffraction. 相似文献
89.
90.
Maria?Elena?LeyvaEmail author Filiberto?González?Garcia Alvaro?Antonio?Alencar?de?Queiroz Demétrio?Artur?Werner?Soares 《Journal of Materials Science: Materials in Electronics》2011,22(4):376-383
The metallopolymer polyaniline-silver (PANI-Ag) was synthesized and used as conductive filler in crosslinked diglycidyl ether
of bisphenol A (DGEBA) epoxy network. The hybrid organic/inorganic PANI-Ag powders were successfully synthesized via in situ
chemical oxidation of polyaniline-emeraldine base (PANI-EB) by the capped Ag+ on the polyaniline-emeraldine base (PANI-EB) surface. The UV–Vis and FT-IR spectra confirmed the pernigraniline structure
(PN) of PANI in the hybrid PANI-Ag. The PANI-Ag dispersion in epoxidic matrix was analyzed by optical microscopy (OM). The
images analysis from OM showed that the particle agglomerate size of the metallopolymer increased with increasing PANI-Ag
concentration in the DGEBA composite, owing to the aggregation effect. The dc conductivity and impedance spectroscopy of the
DGEBA/PANI-Ag composite was measured at different PANI-Ag concentrations in the DGEBA network. The electrical dc conductivity
of the PANI-Ag was 35.1 S cm−1 and was dependent of the PANI-Ag concentration in DGEBA matrix. The real and imaginary part of impedance complex measurements
indicates a strong interfacial polarization at low frequency for both PANI-Ag and DGEBA/PANI-Ag, respectively. The imaginary
part of impedance complex Im(Z) data decrease with the PANI-Ag hybrid concentration in the frequencies range of 102–106 Hz. The dependence of the Im(Z) on the frequency exhibited a relaxation process in both, PANI-Ag and DGEBA/PANI-Ag composite with 10 phr of PANI-Ag powder. 相似文献