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Cellulose dissolved in ionic liquid (1‐(carboxymethyl)pyridinium chloride)/water (60/40 w/w) mixture is regenerated in various non‐solvents, namely water, ethanol, methanol and acetone, to gain more insight into the contribution of non‐solvent medium to the morphology of regenerated cellulose. To this end, the initial and regenerated celluloses were characterized with respect to crystallinity, thermal stability, chemical structure and surface morphology using wide‐angle X‐ray diffraction, thermogravimetric analysis, Fourier transform infrared spectroscopy and scanning electron microscopy. According to the results, regardless of non‐solvent type, all regenerated samples have the same chemical structure and lower crystallinity in comparison to the initial cellulose, making them a promising candidate for efficient biofuel production based on enzymatic hydrolysis of cellulose. The reduction in crystallinity of regenerated samples is explained based on the potential of the non‐solvent to break the hydrogen bonds between cellulose chains and ionic liquid molecules as well as the affinity of water and non‐solvent which can be evaluated based on Hansen solubility parameter. The latter also determines the phase‐separation mechanism during the regeneration process, which in turn affects surface morphology of the regenerated cellulose. The pivotal effect of regenerated cellulose crystallinity on its thermal stability is also demonstrated. Regenerated cellulose with lower crystallinity is more susceptible to molecular rearrangement during heating and hence exhibits enhanced thermal stability. © 2019 Society of Chemical Industry 相似文献
14.
Porkar Rezaeiye Payam Sharifi Arash Rahmani Amir Masoud Dehghan Mehdi 《The Journal of supercomputing》2021,77(12):14207-14229
The Journal of Supercomputing - With the expansion in the use of IoT, increasing the efficiency of these networks has become even more significant. Objects need reliable communications at suitable... 相似文献
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As we approach 100 nm technology the interconnect issues are becoming one of the main concerns in the testing of gigahertz system-on-chips. Voltage distortion (noise) and delay violations (skew) contribute to the signal integrity loss and ultimately functional error, performance degradation and reliability problems. In this paper, we first define a model for integrity faults on the high-speed interconnects. Then, we present a BIST-based test methodology that includes two special cells to detect and measure noise and skew occurring on the interconnects of the gigahertz system-on-chips. Using an inexpensive test architecture the integrity information accumulated by these special cells can be scanned out for final test and reliability analysis. 相似文献
16.
Ahmadreza Momeni Amir G. Aghdam 《International Journal of Adaptive Control and Signal Processing》2007,21(10):885-910
Most of the existing switching control techniques are developed specifically for finite-dimensional linear time-invariant (LTI) systems. In many practical applications, however, it is essential to take time delay into consideration in the modelling as the control system can be highly sensitive to delay. In this paper, a multi-model switching control algorithm is proposed for retarded time-delay systems. It is assumed that the plant is represented by a family of known multi-input multi-output, observable, LTI models with multiple delays in the states, and that corresponding to each model in the known family, there exists a high-performance finite-dimensional LTI controller. In addition, it is supposed that a bound on the magnitude of the external inputs and disturbances is available. It is then shown that the proposed switching controller can stabilize the uncertain system, and that under some mild conditions, output tracking can be achieved in the given problem setting. Copyright © 2007 John Wiley & Sons, Ltd. 相似文献
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The thermal and hydraulic performance of a modified two-stage evaporative cooler is evaluated. Variables considered are the mode of operation, packing thickness, mass flow rate of the water flowing to the precooler, and the mass flux of water flowing over the packing media. The effectiveness of the system increased with the increase of the mass flow rate of water flowing to the precooler, decreasing the mass flux of water flowing to the packing, and with the increase of the packing thickness. The effectiveness of the system with structured packing was higher than that with sheathy leaf base or natural fiber packing.The air-side pressure drop per unit length in the direction of air flow was nearly constant when the structured packing was used. For the sheathy leaf and natural fiber packings, the air pressure drop increased at a uniform rate as the mass flux of water flowing over the packing increased. The air pressure drop was lowest for the setup with the structured packing. 相似文献
18.
This paper considers the application of the method of boundary penalty terms (SAT) to the numerical solution of the wave equation
on complex shapes with Dirichlet boundary conditions. A theory is developed, in a semi-discrete setting, that allows the use
of a Cartesian grid on complex geometries, yet maintains the order of accuracy with only a linear temporal error-bound. A
numerical example, involving the solution of Maxwell’s equations inside a 2-D circular wave-guide demonstrates the efficacy
of this method in comparison to others (e.g., the staggered Yee scheme)—we achieve a decrease of two orders of magnitude in the level of the L2-error. 相似文献
19.
Makarand Hastak Amir Mirmiran Richard Miller Ronak Shah Reid Castrodale 《Canadian Metallurgical Quarterly》2003,8(5):267-272
Precast bridges are often constructed as single span for dead load, but continuous for live load. A diaphragm connection is provided for negative moment continuity. However, the connection may also be subjected to positive moments due to time-dependent effects. Because these moments may be large enough to damage the diaphragm or even the girders, a positive moment connection is often provided. This paper reports on a study to determine the types of positive moment connections used across the country and to identify potential problems with these types of connections. A questionnaire survey was conducted to assess the state of practice for precast prestressed concrete bridges made continuous. The survey provides valuable information on this type of bridge and updates a previous survey on this subject. 相似文献
20.
I Varsano B Volovitz Z Horev J Robinson Y Laks I Rosenbaum A Cohen N Eilam L Jaber C Fuchs J Amir 《Canadian Metallurgical Quarterly》1997,156(11):858-863
Two hundred and fifteen children aged 4 months 6 years with acute otitis media (AOM) were randomized to be treated either by a single i.m. injection of ceftriaxone, 50 mg/kg, with a second dose in the event of unsatisfactory response after 48 h or a history of recurrent AOM (109 patients) or amoxicillin clavulanate 12.5 mg tid (106 patients). The failure rate was similar in children treated by ceftriaxone and amoxicillin clavulanate, 4.6% and 4.7%, respectively (standard error for intergroup difference -2.87%, 95% confidence interval -5.62% to 5.87%). No significant differences between the groups were found in the dynamics of the resolution of the acute symptomatology, otoscopy findings, relapse rate at 30 days or tympanographic evidence of middle ear effusion at the scheduled visits on days 30, 60 and 90. Recurrence of AOM between days 31 and 90 was observed significantly in more children treated with amoxicillin clavulanate than with ceftriaxone--25 out of 84 (29.4%) versus 11 out of 81 (13.6%) (P = 0.012). Conclusion: Ceftriaxone injection(s) is as efficient at least as 10-day oral amoxicillin clavulanate for treatment of acute otitis media in children. Although not recommended as routine, ceftriaxone can be considered in the management of acute otitis media under special circumstances, particularly in cases when the ability to tolerate or absorb oral drugs is compromised, in children refusing or unable to take oral therapy or when the compliance is questionable. 相似文献