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11.
An eXtended Finite Element Method (XFEM) is presented that can accurately predict the stress intensity factors (SIFs) for thermoelastic cracks. The method uses higher order terms of the thermoelastic asymptotic crack tip fields to enrich the approximation space of the temperature and displacement fields in the vicinity of crack tips—away from the crack tip the step function is used. It is shown that improved accuracy is obtained by using the higher order crack tip enrichments and that the benefit of including such terms is greater for thermoelastic problems than for either purely elastic or steady state heat transfer problems. The computation of SIFs directly from the XFEM degrees of freedom and using the interaction integral is studied. Directly computed SIFs are shown to be significantly less accurate than those computed using the interaction integral. Furthermore, the numerical examples suggest that the directly computed SIFs do not converge to the exact SIFs values, but converge roughly to values near the exact result. Numerical simulations of straight cracks show that with the higher order enrichment scheme, the energy norm converges monotonically with increasing number of asymptotic enrichment terms and with decreasing element size. For curved crack there is no further increase in accuracy when more than four asymptotic enrichment terms are used and the numerical simulations indicate that the SIFs obtained directly from the XFEM degrees of freedom are inaccurate, while those obtained using the interaction integral remain accurate for small integration domains. It is recommended in general that at least four higher order terms of the asymptotic solution be used to enrich the temperature and displacement fields near the crack tips and that the J- or interaction integral should always be used to compute the SIFs.  相似文献   
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The corrosiveness of bismuth telluride-based thermoelectric materials (n-type single-phase alloy and a nanocomposite with MoS2 nanoinclusions), in 0.1 molar solution of sodium chloride (NaCl), was investigated. The electrochemical impedance spectroscopy curves obtained after 1, 24, 48 and 72 h immersion time revealed the enhancement of the corrosion resistance of the nanocomposite specimen in a 0.1 molar NaCl solution in comparison with the single-phase bismuth telluride-based alloys, and the passivity increased by immersion time up to 72 h. The nanocomposite sample with submicron grains provided suitable nucleation sites for passive film nucleation that led to higher protective behavior.  相似文献   
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In many industrial applications, the quality of mixing between different materials is fundamental to guarantee the desired properties of products. However, properly modeling and understanding polymer mixing presents noticeable difficulties, because of the variety and complexity of the phenomena involved. This is also the case with the Cavity Transfer Mixer (CTM), an add‐on to be mounted downstream of existing extruders, to improve distributive mixing. The present work proposes a fully three‐dimensional model of the CTM: a finite element solver provides the transient velocity field, which is used in the mapping method implementation to compute the concentration field evolution and quantify mixing. Several simulations are run assessing the impact on mixing of geometrical and functioning parameters. In general, the number of cavities per row should be limited and the cavity size rather big to guarantee good mixing quality. © 2017 American Institute of Chemical Engineers AIChE J, 64: 1034–1048, 2018  相似文献   
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Oxovanadium(IV) Schiff base complex have been anchored onto the surface of purely siliceous MCM-41 and tested for its activity as catalyst for the oxidation of sulfides. This catalyst could alter this oxidation reaction extremity, exhibiting excellent yields with 100 % selectivity. The intercalation of the complex inside the silica matrix was supported by various characterization techniques like X-ray diffraction, differential thermogravimetric (TG-DTA), BET measurements, UV–Vis diffuse reflectance spectroscopy and Fourier transform infrared spectroscopy (FT-IR). The stability of the catalyst during the course of the reaction was confirmed from its post catalytic FT-IR and XRD analysis. The catalyst could be reused five times without notable loss of its catalytic activity and efficiency which indicates that the metal-Schiff base moiety is intact and the coordination environments are not altered during the reaction.  相似文献   
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Calcination of diatomite is an expensive process frequently resulting in products with unpredictable structure. Alternatively, calcination in swirling flow is an energy‐saving option. Computational fluid dynamics modeling of an experimental calcination process unit is presented. Experimental results and systematic collection of process data were used to define boundary condition for steady‐state and transient simulation runs. The comparison of experimental and simulation results shows the complexity of the calcination process. The results can be used for further process optimization.  相似文献   
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