全文获取类型
收费全文 | 1013篇 |
免费 | 47篇 |
国内免费 | 7篇 |
专业分类
电工技术 | 21篇 |
综合类 | 9篇 |
化学工业 | 225篇 |
金属工艺 | 10篇 |
机械仪表 | 21篇 |
建筑科学 | 35篇 |
矿业工程 | 12篇 |
能源动力 | 32篇 |
轻工业 | 116篇 |
水利工程 | 6篇 |
石油天然气 | 2篇 |
无线电 | 71篇 |
一般工业技术 | 175篇 |
冶金工业 | 135篇 |
原子能技术 | 5篇 |
自动化技术 | 192篇 |
出版年
2024年 | 3篇 |
2023年 | 16篇 |
2022年 | 22篇 |
2021年 | 37篇 |
2020年 | 22篇 |
2019年 | 32篇 |
2018年 | 21篇 |
2017年 | 24篇 |
2016年 | 28篇 |
2015年 | 27篇 |
2014年 | 42篇 |
2013年 | 51篇 |
2012年 | 42篇 |
2011年 | 69篇 |
2010年 | 59篇 |
2009年 | 35篇 |
2008年 | 50篇 |
2007年 | 44篇 |
2006年 | 37篇 |
2005年 | 22篇 |
2004年 | 20篇 |
2003年 | 21篇 |
2002年 | 26篇 |
2001年 | 19篇 |
2000年 | 13篇 |
1999年 | 15篇 |
1998年 | 28篇 |
1997年 | 27篇 |
1996年 | 17篇 |
1995年 | 13篇 |
1994年 | 11篇 |
1993年 | 17篇 |
1992年 | 15篇 |
1991年 | 14篇 |
1990年 | 11篇 |
1989年 | 14篇 |
1988年 | 9篇 |
1987年 | 11篇 |
1986年 | 4篇 |
1985年 | 3篇 |
1984年 | 3篇 |
1983年 | 11篇 |
1982年 | 4篇 |
1981年 | 6篇 |
1980年 | 4篇 |
1978年 | 4篇 |
1977年 | 5篇 |
1976年 | 11篇 |
1974年 | 7篇 |
1964年 | 4篇 |
排序方式: 共有1067条查询结果,搜索用时 15 毫秒
11.
Naoufal Bahlawane Edgar Fischer Rivera Katharina Kohse-Hinghaus Armin Brechling Ulf Kleineberg 《Applied catalysis. B, Environmental》2004,53(4):245-255
The chemical vapor deposition method was used to deposit thin films of cobalt oxide starting with cobalt (II) acetylacetonate and oxygen. The deposition process was investigated and the obtained films were identified as a cubic spinel-type polycrystalline Co3O4 with a crystallite size of 30–40 nm. The coating was carbon-free and the surface oxygen concentration was measured to be 66 at.% with AES analysis. Smooth and highly uniform thin films were deposited on planar stainless steel substrates and subjected to TPR and catalysis tests that show positive correlation. The apparent activation energy of Co3O4 reduction to CoO was measured to be (33±5) kJ/mol. The catalytic activity of Co3O4 was investigated toward the conversion of both propane and ethanol to carbon dioxide. Though the catalytic action was registered at the same temperature, the deactivation process was seen to be different. The catalytic conversion of ethanol induces a fast deactivation process, which was linked to its high ability to reduce Co3O4. 相似文献
12.
A pump suitable for use with gas electrodes, in which recirculation of the gas is necessary, is described. The system to which the cell with the gas electrode and the pump are connected does not change its volume when the pump is in operation. The pump works as follows: an embolus, consisting of a Tefloncoated magnetic stirring bar, placed inside a glass tube having an internal diameter slightly larger than the diameter of the bar, is moved from the outside with a permanent magnet, which in turn is moved horizontally along the tube by means of a mechanical assembly driven by an electric motor. The motion of the embolus is accompanied by the closing and opening of glass valves which allow the gas to circulate in the desired direction. The pump, used in conjunction with a vacuum line, operates from pressures as low as 60 Torr to above atmospheric pressure. The operation of the pump is unaffected by organic gases and most inorganic gases. 相似文献
13.
Armin Mosandl und Ursula Palm 《Zeitschrift für Lebensmitteluntersuchung und -Forschung A》1991,193(2):109-114
Zusammenfassung Die Synthese von acht verschiedenen 2-Alkoxy-5-alkyl-tetrahydrofuranen und ihren Stereoisomeren wird vorgestellt, sieben von ihnen sind als Aromastoffe der Wassermelone bekannt. Alle Stereoisomeren werden, ausgehend von optisch reinen-Nonalacton-Enantiomeren, synthetisiert und mit Diisobutylaluminiumhydrid selektiv zu den entsprechenden Lactolen reduziert. Die Lactole werden mit den gewünschten Alkoholen in schwach saurer Lösung zucis/trans-Diastereomeren umgesetzt und durch Flüssigchromatographie in optisch reine Stereoisomere getrennt. Die sensorische Charakteristik aller Stereoisomeren der sieben Verbindungen wird aufgezeigt. Die Trennung dercis/trans-Diastereomeren an DB-210 wird vorgestellt und die chirospezifische Differenzierung der acht Verbindungen diskutiert.
Stereoisomeric flavour compounds L. Optically pure 2-alkoxy-5-alkyl-tetrahydrofurans — structures and properties
Summary The synthesis of eight different 2-alkoxy-5-alkyltetrahydrofurans and their stereoisomers is presented, seven of which are known to be flavour compounds of water melons. All stereoisomers were synthesized from optically pure-lactone enantiomers, which were selectively reduced by diisobutylaluminium hydride to the corresponding lactols. The lactols were treated with the desired alcohol component in weakly acidic media to yield thecis/trans diastereoisomers, which were separated into optically pure stereoisomers by liquid chromatography. The sensory characteristics of all four stereoisomers of the seven compounds are given. The Stereodifferentiation of thesecis/trans diastereoisomers on DB-210 is demonstrated and the direct chirospecific differentiation of all eight compounds discussed.相似文献
14.
Pre-existing discontinuities change the mechanical properties of rock masses,and further influence failure behavior around an underground opening.In present study,the failure behavior in both Inner and Outer zones around a circular opening in a non-persistently jointed rock mass under biaxial compression was investigated through numerical simulations.First,the micro parameters of the PFC3D model were carefully calibrated using the macro mechanical properties determined in physical experiments implemented on jointed rock models.Then,a parametrical study was undertaken of the effect of stress condition,joint dip angle and joint persistency.Under low initial stress,the confining stress improves the mechanical behavior of the surrounding rock masses;while under high initial stress,the surrounding rock mass failed immediately following excavation.At small dip angles the cracks around the circular opening developed generally outwards in a step-path failure pattern;whereas,at high dip angles the surrounding rock mass failed in an instantaneous intact rock failure pattern.Moreover,the stability of the rock mass around the circular opening deteriorated significantly with increasing joint persistency. 相似文献
15.
Tröger Armin Svensson Glenn P. Galbrecht Hans-Martin Twele Robert Patt Joseph M. Bartram Stefan Zarbin Paulo H. G. Segraves Kari A. Althoff David M. von Reuss Stephan Raguso Robert A. Francke Wittko 《Journal of chemical ecology》2021,47(12):1025-1041
Journal of Chemical Ecology - The obligate pollination mutualism between Yucca and yucca moths is a classical example of coevolution. Oviposition and active pollination by female yucca moths occur... 相似文献
16.
Chaudry Oliver Friedberger Andreas Grimm Alexandra Uder Michael Nagel Armin Michael Kemmler Wolfgang Engelke Klaus 《Magma (New York, N.Y.)》2021,34(3):367-376
Magnetic Resonance Materials in Physics, Biology and Medicine - To develop a precise semi-automated segmentation of the fascia lata (FL) of the thigh to quantify IMAT volume in T1w MR images and... 相似文献
17.
Mischa Schmidt Jan Seedorf Stefano Napolitano Rosario G. Garroppo Andrea Cavaliere Thilo Ewald Armin Jahanpanah Zbigniew Kopertowski Marcin Pilarski Pawel Grochocki 《Peer-to-Peer Networking and Applications》2013,6(2):134-154
Application Layer Traffic Optimization (ALTO) has recently gained attention in the research and standardisation community as a way for a network operator to guide the peer selection process of distributed applications by providing network layer topology information. In particular P2P applications are expected to gain from ALTO, due to the many connections peers form among each other, often without taking network layer topology information into account. In this paper, we present results of an extensive intra-ISP trial with an ALTO-enhanced P2P filesharing software. In summary, our results show that—depending on the concrete setting and on the distribution of upload capacity in the network—ALTO enables an ISP to save operational costs significantly while not degrading application layer performance noticeably. In addition, based on our experience we are able to give advice to operators on how to save costs with ALTO while not sacrificing application layer performance at all. 相似文献
18.
19.
20.
A case study validation of a knowledge-based approach for the selection of requirements engineering techniques 总被引:2,自引:1,他引:1
Requirements engineering (RE) is a critical phase in the software engineering process and plays a vital role in ensuring the
overall quality of a software product. Recent research has shown that industry increasingly recognizes the importance of good
RE practices and the use of appropriate RE techniques. However, due to the large number of RE techniques, requirements engineers
find it challenging to select suitable techniques for a particular project. Unfortunately, technique selection based on personal
experience has limitations with regards to the scope, effectiveness and suitability of the RE techniques for the project at
hand. In this paper, a Knowledge-based Approach for the Selection of Requirements Engineering Techniques (KASRET) is proposed
that helps during RE techniques selection. This approach has three major features. First, a library of requirements techniques
was developed which includes detailed knowledge about RE techniques. Second, KASRET integrates advantages of different knowledge
representation schemata and reasoning mechanisms. Thus, KASRET provides mechanisms for the management of knowledge about requirements
techniques and support for RE process development. Third, as a major decision support mechanism, an objective function evaluates
the overall ability and cost of RE techniques, which is helpful for the selection of RE techniques. This paper makes not only
a contribution to RE but also to research and application of knowledge management and decision support in process development.
A case study using an industrial project shows the support of KASRET for RE techniques selection.
相似文献
Behrouz H. FarEmail: |