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91.
Artur Suchan Joanna Nackiewicz Zbigniew Hnatejko Witold Waclawek Stefan Lis 《Dyes and Pigments》2009,80(2):239-244
The association of zinc octacarboxyphthalocyanine, was studied using UV–vis absorption and fluorescence emission spectroscopy; the effects of dye concentration, pH and solvents on spectra were discussed. Calculations showed that the dye dimerized in aqueous solutions ranging from 5.0 × 10?7 to 5.0 × 10?5 mol/dm3, at 25 °C. The dimerization constant of 106 dm3/mol and the spectral Q band shift of 1185 cm?1 imparted by dimerization indicated strong π–π interactions between phthalocyanine molecules. Red S1 fluorescence of the dye monomer was observed in various solutions which was quenched owing to molecular association and other factors. The strong influence of pH on both aggregation and fluorescence was discussed. At pH < 5.0, only dye aggregates were present in solution; monomers appeared at pH ≥ 5.0 and, in alkaline solution, only the monomeric anions of phthalocyanine existed. The spectral absorption and emission data for the dye in binary solvents revealed that at concentrations ranging from 0.5 × 10?5 to 1.0 × 10?5 mol/dm3, the dye can be used in photosensitised oxidation reactions. 相似文献
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Dziedzic Krzysztof Górecka Danuta Szwengiel Artur Michniewicz Jan Drożdżyńska Agnieszka Walkowiak Jarosław 《Food science and biotechnology》2019,28(3):649-655
Food Science and Biotechnology - The tomato pomace obtained during processing as a residue of tomato processing from large industry. The interactions between tomato pomace and fecal bacteria, bile... 相似文献
94.
Kaczyński Łukasz K. Cais-Sokolińska Dorota Szwengiel Artur 《Food science and biotechnology》2019,28(5):1529-1534
Food Science and Biotechnology - The aim of this work was the analysis of galactooligosaccharides (GOS) formation in a model mixture of goat’s milk and its permeate from microfiltration and... 相似文献
95.
Joanna Mastalska‐Popawska Piotr Izak ukasz Wjcik Agata Stempkowska Zuzanna Gral Artur T. Krzyak Iwona Habina 《Polymer Engineering and Science》2019,59(6):1279-1287
Transparent and intumescent polymer‐silicate hydrogels were synthesized by free‐radical polymerization, in the presence of the redox initiators system (potassium persulphate/sodium thiosulphate) and cross‐linking monomer (N,N′‐methylenebisacrylamide). Hydrogels obtained in such a manner were rheologically tested and it was found that the same sample with a different sodium acrylate concentration polymerized faster when its content was lower. The spectroscopic and thermal analysis proved that the polymer combines with sodium silicate by hydrogen bonds and during thermal degradation only small polymer fragments and water molecules were released. NMR studies have shown that the content of water glass causes shorter relaxation times. Conducted fire tests showed that glass panes systems filled with the tested hydrogels meet the relevant construction standards and what is their big advantage, a thin 1 mm layer of polymer‐silicate gel is sufficient for this purpose. We believe that these results will contribute to the development of intumescent hydrogels with enhanced fire‐retardant properties. POLYM. ENG. SCI., 59:1279–1287 2019. © 2019 Society of Plastics Engineers 相似文献
96.
Evaluation of apple texture with contact acoustic emission detector: A study on performance of calibration models 总被引:1,自引:0,他引:1
Artur Zdunek Justyna CybulskaDorota Konopacka Krzysztof Rutkowski 《Journal of food engineering》2011,106(1):80-87
Performance of calibration models for evaluation of apples sensory texture with contact acoustic emission detector (CAED) was studied. For model evaluation and testing, 2500 apples of 19 cultivars were harvested over two seasons. Apples were stored at normal atmosphere (NA), controlled atmosphere (CA) for different periods or were treated with 1-methylcyclopropene (1-MCP) in order to obtain a high variability of texture and fruit maturity. Apples were tested simultaneously in two distinct laboratories. The models were created and validated on averaged values from 10 fruits using simple linear regression, multiple linear regression (MLR) and principal component regression (PCR). Performance statistics of the models were expressed in terms of determination coefficient (R2), root mean square errors of cross validation (RMSECV) or prediction (RMSEP) and ratio of prediction to deviation (RPD). Firmness and total acoustic emission counts were predictors of sensory texture in the models. MLR and PCR models show better performance for prediction of sensory data than simple linear regression models however PCR models show the best results among models tested in this study. Common PCR models for several cultivars allow for successful prediction of hardness (RPD > 2.0), crispness and overall texture (1.5 < RPD < 2.0). The single-cultivar PCR models, constructed on data sets containing 26-39 averaged values, reveal significantly better performance (RPD > 2.0 for most of the cases) than the common PCR models for many varieties. 相似文献
97.
Jeffrey F. Wheeldon Christopher E. Valdivia Alexandre W. Walker Gitanjali Kolhatkar Abdelatif Jaouad Artur Turala Bruno Riel Denis Masson Norbert Puetz Simon Fafard Richard Ars Vincent Aimez Trevor J. Hall Karin Hinzer 《Progress in Photovoltaics: Research and Applications》2011,19(4):442-452
Four tunnel junction (TJ) designs for multijunction (MJ) solar cells under high concentration are studied to determine the peak tunnelling current and resistance change as a function of the doping concentration. These four TJ designs are: AlGaAs/AlGaAs, GaAs/GaAs, AlGaAs/InGaP and AlGaAs/GaAs. Time‐dependent and time‐average methods are used to experimentally characterize the entire current–voltage profile of TJ mesa structures. Experimentally calibrated numerical models are used to determine the minimum doping concentration required for each TJ design to operate within a MJ solar cell up to 2000‐suns concentration. The AlGaAs/GaAs TJ design is found to require the least doping concentration to reach a resistance of <10−4 Ω cm2 followed by the GaAs/GaAs TJ and finally the AlGaAs/AlGaAs TJ. The AlGaAs/InGaP TJ is only able to obtain resistances of ≥5 × 10−4 Ω cm2 within the range of doping concentrations studied. Copyright © 2010 John Wiley & Sons, Ltd. 相似文献
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Mauro Zammarano John R. Shields Isaac Leventon Ickchan Kim Shonali Nazare Andre Thompson Rick D. Davis Artur Chernovsky Matthew Bundy 《火与材料》2021,45(1):114-126
Herein, we describe a reduced‐scale test (“Cube” test), measuring the fire performance of specimens including a fire barrier (FB) and a flammable core material, which acts as the main fuel load. The specimen is intended to reproduce a cross‐section of a composite product where heat/mass transfer occurs primarily in a direction perpendicular to the FB. The Cube test procedure and benefits are discussed in this work by adopting residential upholstery furniture as an exemplary study. One flexible polyurethane foam, one polypropylene cover fabric, and 10 commercially available FBs were selected. They were used to compare the fire performance of FBs, measured in terms of peak of heat release rate, in the ASTM E1474‐14 standard test and the newly developed Cube test. Edge effects severely affected the performance of FBs in the ASTM E1474‐14 standard test but not in the Cube test. Furthermore, appropriate test conditions were determined in the Cube test to measure the so‐called “wetting point,” that is, the time and value of heat release rate measured when flammable liquid products were first observed on the bottom of the specimen. The relevance of the “wetting point” in terms of full‐scale fire performance and failure mechanism of FBs is discussed. 相似文献