过氧化甲乙酮合成研究

研究了在酸性催化剂存在下，以邻苯二甲酸二丁酯作溶剂，由双氧水和甲乙酮作用制取过氧化甲乙酮溶液的工艺，并得到最佳工艺条件。结果表明，产品性能优良。     

整定管理软件系统在继电保护故障分析中的应用探析

结合实际工作经验,讨论了整定计算软件在新型继电保护系统中应用的必要性,评定和探究了整定管理在继电保护故障分析中的运用,并总结了整定管理在整套系统中的实际应用。     

Preparation and protein adsorption of hydrogel polysucrose microspheres

A series of novel hydrogel polysucrose microspheres with the mean size ranging from 200 to 500 μm were prepared via two‐step method. First, soluble polysucrose was synthesized by solution polymerization between sucrose and epichlorohydrin; second, a reversed phase suspension crosslinking reaction was performed to prepare polysucrose microspheres. The SEM images indicated that these spherical beads had smooth surface and hydrogel interior structure. FTIR was used to characterize the chemical structure of the beads. The hydrated and dry densities, equilibrium water content, and hydroxyl content of polysucrose microspheres were also investigated. The characteristic of high hydroxyl content (15.48–19.04 mmol/g) make these microspheres suitable for protein adsorption. Meanwhile, bovine serum albumin was used to examine the adsorption capacity of the microspheres. These microspheres had a capacity as high as 49.28 mg/g. The adsorption kinetics and recycling of the beads were also investigated. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 5934–5940, 2006     

数字签名技术的应用

数字签名技术建立在公钥加密系统基础之上,可以检验数据传输过程中是否被篡改以及数据的真实性和完整性。利用其提供的安全保障机制,在某市自建的横向联网系统中实现了对交易报文在传递过程中的安全加密,从软件架构上进一步完善了系统的安全体系。     

推光漆应唤回推光漆精神

推光漆是中国漆文化的重要组成部分。历史地看 ,推光漆注重人的德性培养、技气培养、美善培养和物化质量。推光漆的前人名之为“推光漆精神。”这种精神沿续甚久。在改革开放初期依然存在。失落推光漆精神始于二十世纪九十年代之初 ,企业承包 ,实行厂长 (经理 )责任制 ,抓经济放在了首位。抓经济 ,没有错 ,要富国强民 ,非走这条路子别无选择。问题是有些顾此失彼。其所失 ,那就是党的领导大大削弱 ,工会成了“喝凉水搭筷子” ,“职工之家”的牌子也摘了。几乎放弃了政治思想建设 ,放弃了爱岗敬业教育 ,放弃了推光漆精神。说是推光漆 ,若不说…     

光交联对HDPE凝胶量的影响

用安息香二甲醚和三(丙烯酰氧乙基)异氰尿酸酯(TAEIC)作为PE的光敏剂和助交联剂,研究了它们的用量、光照时间、交联温度,紫外光光强对PE交联度的影响。结果表明,安息香二甲醚是一种有效的光敏剂,引发效率较高;助交联剂可以提高交联效率;光照时间、紫外光光强和交联温度等对PE的交联度均有明显的影响。     

Stabilization And Tracking Of Underactuated Surface Vessels In Random Waves With Fin Based On Adaptive Hierarchical Sliding Mode Technique

Trajectory tracking and roll stabilization are both vital practices in ship motion control. Trajectory tracking is a kind of low‐frequency control, while roll stabilization by means of fins is a kind of high‐frequency control. However, they have been studied separately previously; most tracking control of underactuated surface vessels in the previous studies do not account for roll stabilization by means of fins. In reality, however, they are an integral system. In this paper, a simple control strategy is proposed to achieve trajectory tracking and fin roll stabilization simultaneously. Four degrees of freedom derived from a six degrees of freedom mathematical model of a surface vessel is considered, including surge, sway, roll and yaw. Surge force, roll moment and yaw moment are considered as control inputs, while position, yaw angle and roll angle are controlled. The number of control inputs is fewer than the outputs to be controlled. Therefore, we are dealing with an underactuated problem. An adaptive hierarchical sliding mode control technique is employed to deal with the underactuation. Stabilization of underactuated surface vessels is studied as a special case. Random waves are applied to test the robustness of the designed controllers. Lyapunov stability theory is used to show the stability of closed‐loop system. The simulation results verify the effectiveness of the proposed strategy.     

混合物MH-81状态方程的研究——从无限稀释活度系数预测混合物汽液平衡

本文由无限稀释活度系数求取混合物MH-81状态方程的二元相互作用参数,预测了二元混合物的汽液平衡,获得了较满意的结果。     

Structural topology optimization with constraints on multi-fastener joint loads

This paper addresses an important problem of design constraints on fastener joint loads that are well recognized in the design of assembled aircraft structures. To avoid the failure of fastener joints, standard topology optimization is extended not only to minimize the structural compliance but also to control shear loads intensities over fasteners. It is shown that the underlying design scheme is to ameliorate the stiffness distribution over the structure in accordance with the control of load distributions over fastener joints. Typical examples are studied by means of topology optimization with joint load constraints and the standard compliance design. The effects of joint load constraints are highlighted by comparing numerical optimization results obtained by both methods. Meanwhile, resin models of optimized designs are fabricated by rapid prototyping process for loading test experiments to make sure the effectiveness of the proposed method.     

Damping of vinyl acetate–n‐butyl acrylate copolymers

A photopolymerization process at room temperature was devised to copolymerize vinyl acetate (VAc) and n‐butyl acrylate (BA) mainly to prepare rubber‐like damping sheet bearing pressure‐sensitive adhesive property in this study. The investigations using both the differential scanning calorimeter and rheometric dynamic analysis show the existence of two glass transition temperatures for each copolymer. The scanning electron microscopic pictures reveal that the degree of microphase separation increases with increasing annealing time at 70°C. It was suggested that the rubbery domain (formed by the PBA blocks) disperses in the glassy domain (constituted by the PVAc blocks), making an effective damping entity. Excellent damping was observed for the copolymer samples, with the tanδ peak values as high as 1.76–1.80 at a certain temperature range and with tanδ> 0.3 at quite wide temperature ranges. In addition, the copolymers containing more VAc tend to have the higher damping. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 91: 1396–1403, 2004