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21.
Hybrid coatings of hyperbranched polyurethane‐urea (HBPUU) containing ZnO nanoparticles were prepared by mixing the hyperbranched polyurethane with the nanoparticles. The films were stored at room temperature and laboratory humidity conditions for one week to yield completely cured hybrid films. The ZnO nanoparticles were found to be well dispersed in the polymer up to 3 wt%. The structure–property relationship of various HBPUU–ZnO hybrid coatings was analysed using a Fourier transform infrared peak deconvolution technique with a Gaussian curve‐fitting procedure, while their viscoelastic, thermomechanical and surface morphology were studied using X‐ray diffraction, dynamic mechanical thermal analysis, thermogravimetric analysis, a universal testing machine, scanning electron microscopy, atomic force microscopy and contact angle instruments. The thermal stability and mechanical properties of the hybrid composite films improved with increasing ZnO content, which was believed to be due to thermal insulation in the presence of nanoparticles. Water contact angle data suggested that the hydrophobic character of the hybrid composites increased with increasing nanoparticle concentration. The antimicrobial property of the HBPUU–ZnO hybrid coatings was studied using the disc diffusion method. HBPUU–ZnO hybrid coatings showed good antimicrobial properties compared to HBPUU. Copyright © 2012 Society of Chemical Industry 相似文献
22.
Lipid carriers for delivery of celecoxib: In vitro,in vivo assessment of nanomedicine in rheumatoid arthritis
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Kunal Biswas Awdhesh Kumar Mishra Pradipta Ranjan Rauta Abdullah G. Al-Sehemi Mehboobali Pannipara Avik Sett Amra Bratovcic Satya Kumar Avula Tapan Kumar Mohanta Muthupandian Saravanan Yugal Kishore Mohanta 《International journal of molecular sciences》2022,23(2)
At present, the potential role of the AgNPs/endo-fullerene molecule metal nano-composite has been evaluated over the biosystems in-vitro. The intra-atomic configuration of the fullerene molecule (C60) has been studied in-vitro for the anti-proliferative activity of human breast adenocarcinoma (MDA-MB-231) cell lines and antimicrobial activity against a few human pathogens that have been augmented with the pristine surface plasmonic electrons and antibiotic activity of AgNPs. Furthermore, FTIR revealed the basic vibrational signatures at ~3300 cm−1, 1023 cm−1, 1400 cm−1 for O-H, C-O, and C-H groups, respectively, for the carbon and oxygen atoms of the C60 molecule. NMR studies exhibited the different footprints and magnetic moments at ~7.285 ppm, explaining the unique underlying electrochemical attributes of the fullerene molecule. Such unique electronic and physico-chemical properties of the caged carbon structure raise hope for applications into the drug delivery domain. The in-vitro dose-dependent application of C60 elicits a toxic response against both the breast adenocarcinoma cell lines and pathogenic microbes. That enables the use of AgNPs decorated C60 endo fullerene molecules to design an effective anti-cancerous drug delivery and antimicrobial agent in the future, bringing a revolutionary change in the perspective of a treatment regime. 相似文献
25.
Vidya Kishore Christine Ajinjeru Ahmed A. Hassen John Lindahl Vlastimil Kunc Chad Duty 《Polymer Engineering and Science》2020,60(5):1066-1075
To develop new materials for extrusion additive manufacturing (AM) systems, a fundamental understanding of rheological properties is essential to correlate the effect of processing on material structure and its properties. In this work, the rheological properties of five different grades of neat and carbon fiber (CF)-reinforced poly(ether ketone ketone) are reported. Rheological properties are essential to understand the effect of reinforcing fibers and AM process parameters such as time, temperature, environment, and shear rate on flow behavior during processing. Small-amplitude oscillatory shear tests and steady shear tests indicated neat grades to exhibit less increase in viscosity over time when processed in air than the CF-filled grades. The filled grades showed greater shear thinning and lower sensitivity to temperature. Overall, this rheological analysis provides a broad framework for determining appropriate processing conditions for extrusion deposition AM of such high-temperature polymer systems. 相似文献
26.
V. R. Pai Verneker K. Kishore C. B. V. Subhas 《Propellants, Explosives, Pyrotechnics》1979,4(4):83-86
Thermal decomposition studies on double-base propellants have been carried out in air and vacuum using differential scanning calorimetric, thermogravimetric and mass spectrometric techniques. Low temperature (90 °C–170 °C) decomposition seems to involve diffusion controlled process, the mechanism in air and vacuum being different. High temperature (170 °–205 °C) decomposition involves bond breakage. 相似文献
27.
Effects of the confining wall or blockage on the heat transfer phenomena of spheroid particles were numerically investigated. The heated spheroid particles were maintained at constant temperature and allowed to sediment in cylindrical tubes filled with Newtonian liquids. In this flow configuration, the heat transfer took place from the heated spheroid particles to the surrounding Newtonian liquid. The governing conservation equations of the mass, momentum, and energy together with appropriate boundary conditions were numerically solved using commercial software based on computational fluid dynamics. A simple correlation for the average Nusselt number of the confined spheroid particles was developed which can be applied in new applications. 相似文献
28.
Salleh Emee Marina Zuhailawati Hussain Ramakrishnan Sivakumar Dhindaw Brij Kumar 《Metallurgical and Materials Transactions A》2017,48(5):2519-2528
Metallurgical and Materials Transactions A - Magnesium (Mg) and its alloys have shown potential for use in the biomedical industry due to their excellent biological performance and biodegradability... 相似文献
29.
Ravi Kishore Ivaturi 《电子与电脑》2009,(3):32-34
低价位新车打入印度汽车市场,印度的汽车总数将于2012年超过4000万辆。空气质量已成为印度政府关注的首要课题,而针对省油引擎管理系统的重要性, 相似文献
30.
Sachin Nalawade M. Sundararaman J. B. Singh Amit Verma R. Kishore 《Transactions of the Indian Institute of Metals》2010,63(1):35-41
Alloy 718 samples under two initial microstructural conditions, viz., solution annealed to form only γ phase (ST) and aged
to precipitate only δ particles (DELTA), were deformed in tension till fracture in the temperatures range from 200°C–700°C.
From the comparison of the evolved microstructure of deformed and undeformed specimens that have been subjected to similar
thermal history, deformation induced precipitation could be identified. Deformation in the range of 550°C to 650°C promoted
the precipitation of γ′ and γ″ phases in both structures. In case of DELTA alloy, the γ′ precipitation was found to precede
the γ′ phase precipitation while no such preference for precipitation could be identified in ST specimens. This difference
in the precipitation behaviour and the sequence of precipitation has been explained on the basis of the relative concentration
of solutes in the matrix of the starting microstructures of ST and DELTA specimens. 相似文献