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21.
Different modes of activation are described for a postgrafting reaction of acrylic acid on poly(p-phenylene terephthalamid) (PPTA)mitrogen plasma or electron-beam irradiation. Both lead to surface radical formation, and these species are able to initiate grafting. The Functionalization through amino group attachment is characteristic of plasma treatment. Degradation initiated by UV-visible emission of plasma is noticed, leading to the amide clivage. The surface grafting is more important when the PPTA is irradiated with a cold plasma and if water is used as the solvent. The polymer crystallinity degree reduces the grafting of the electron beam-irradiated PPTA even with a high radical concentration. © 1994 John Wiley & Sons, Inc. 相似文献
22.
Sandra Aparecida de Assis Pedro Fernandes Bruno Sommer Ferreira Joaquim MS Cabral Olga Maria Mascarenhas Faria Oliveira 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2004,79(3):277-280
A partially purified extract of pectinmethylesterase (PME) from acerola fruit was immobilized on various supports: glass, celite, chrysotile, agarose, concanavalin A Sepharose 4B, egg shell, polyacrylamide and gelatin. In addition, reticulation with glutaraldehyde was assessed, as well as the use of gelatin in the presence of celite, glass and silica. The highest immobilization yields were obtained when the pectinmethylesterase was immobilized in concanavalin A Sepharose 4B (81.7%) and in gelatin‐water (78.0%). Copyright © 2004 Society of Chemical Industry 相似文献
23.
24.
Bruno Buchmayr 《国际钢铁研究》1992,63(10):446-446
25.
Schilling D.L. Milstein L.B. Pickholtz R.L. Bruno F. Kanterakis E. Kullback M. Erceg V. Biederman W. Fishman D. Salerno D. 《Communications Magazine, IEEE》1991,29(11):86-93
Multipath propagation in a broadband CDMA environment is described. A propagation model for broadband spread-spectrum signals is presented. Experimental results relating to the sharing of the band by fixed service microwave users and mobile personal communications network (PCN) users are discussed. Field tests indicate that PCN systems can provide high-quality communications when sharing the spectrum with fixed-service microwave systems in suburban and urban areas 相似文献
26.
A model for building integrated photovoltaic systems has been developed and implemented in a dynamic simulation tool. This tool takes into account the thermal interactions between the PV collector and the building. The influence of the type of integration upon the PV collector efficiency has been evaluated and hybrid PV/air collectors have been studied. An overall efficiency is defined, including the production of electricity and heat. A case study has been performed on two different typical buildings. In the case of a multi-crystalline silicon PV collector integrated on the roof of a single family house located in Paris, the efficiency of unventilated PV modules fixed on the roof is 14%. If the PV collector is used to preheat the ventilation air, the efficiency reaches 20%. A proper building integration also improves the environmental balance of PV technologies over their life cycle. 相似文献
27.
We deal with a complex game between Alice and Bob where each contender’s probability of victory grows monotonically by unknown amounts with the resources employed. For a fixed effort on Alice’s part, Bob increases his resources on the basis of the results for each round (victory, tie or defeat) with the aim of reducing the probability of defeat to below a given threshold. We read this goal in terms of computing a confidence interval for the probability of losing and realize that the moves in some contests may bring in an indeterminacy trap: in certain games Bob cannot simultaneously have both a low probability-of-defeat measure and a narrow confidence interval. We use the inferential mechanism called twisting argument to compute the above interval on the basis of two joint statistics. Careful use of such statistics allows us to avoid indeterminacy. 相似文献
28.
Despite the common use of tapping-mode atomic force microscopy to image composites or polymer blends, very few studies have focused on the measurement of the interdiffusion at an interface between two polymers in contact. In this study, we show how to assess the interphase between two polymers with two methods. First, stable and robust tapping conditions are established, and the problem of the phase contrast is discussed. Second, a contact-resonance method is presented: the tip in contact with the sample is electrostatically excited at its resonance frequency by a self-controlled oscillator. The gain and frequency images allow us to measure the interdiffusion width. Both methods (using high and weak mechanical solicitation) give the same assessment of the interdiffusion width. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献
29.
Thin layers of silver and titanium were deposited onto commercial Ti–48Al particles by magnetron sputtering prior to their consolidation by hot isostatic pressing and subsequent heat treatment.
Based on picnometry and electron probe microanalysis results, average values of 1.5 and 2.5 at.%, respectively, were obtained
for the silver and titanium contents in the coated particles. The surface modified Ti–48Al particles exhibited improved sintering ability than the unmodified ones. The consolidated samples have duplex microstructures
formed by γ-TiAl and γ-TiAl + α2-Ti3Al grains. Ag-rich nanoprecipitates were detected in the microstructure of the compacted Ti-48Al + Ag sample. The coatings are no longer visible at the grains boundaries after a subsequent homogenization heat treatment
at 1200°C. The highest values of hardness and Young’s modulus were obtained for the Ti–48Al + Ag sample, associated with a higher density and a lower percentage of pores. 相似文献
30.
J. Mller-Kemsa Bruno Lange Gmbh 《European Journal of Lipid Science and Technology》1992,94(11):439-440
Colour Measuring Instruments for Transparent Liquids Safeguard the Quality in the Chemical Industry – Quality Control of Transparent Liquids In many areas of the chemical industry a complete product specification comprises – besides various other parameters – the colour characteristics as well. The colour of transparent liquids is still frequently determined by visual comparison of the product with e.g. iodine, Hazen- or Gardner colour standard solutions or appropriate colourfilter discs. In 1989 a new DIN 53995 standard for instrumental colour assessment of transparent liquids was introduced to replace the error-prone, subjective methods of visual comparisons. Dr. Lange GmbH, Düsseldorf, has developed the LICO 200 spectrophotometer under consideration of the new DIN 53995 for objective colour assessment in compliance with the iodine, Hazen and Gardner colour scales. 相似文献