脂肪族超支化聚酯的端链结晶行为

以长链烷基酸为改性剂,对以三羟甲基丙烷为核、二羟甲基丙酸为支化单体合成的第三代端羟基超支化聚酯进行端基改性,采用羟值滴定和核磁共振氢谱(1H-NMR)表征超支化聚酯的改性程度,采用差示扫描量热分析(DSC)和广角X射线衍射(WAXD)研究了端烷烃链长度和端基改性程度对超支化聚酯相转变行为和结晶行为的影响。结果表明,超支化聚酯的结晶归因于长链端烷烃的有序排列,端烷烃链越长,端烷基超支化聚酯的冷结晶温度、热结晶温度和熔融温度均逐渐升高;端烷烃链越长或改性程度越高,衍射峰强度越大,晶粒尺寸变小。进一步用DSC研究了端十八烷基超支化聚酯的非等温结晶行为并用Ozawa法对其非等温结晶动力学进行了分析,发现其成核方式为异相成核,生长方式为针状晶体的一维生长。     

高线机组轧制急停控制系统的开发应用案例

介绍安钢高线机组生产急停控制系统的开发应用过程。     

基于ANSYS的可靠性分析

介绍了结构可靠性的基本原理和基本分析方法，利用ANSYS中的可靠性分析工具——Probabilistic DEesign，对框架结构的可靠性进行了分析，实例证明：该方法可得到比较精确的可靠度指标和失效概率，但是其效率不高，需要对其抽样方法进行改进。     

冰冻灾害及其他心理因素对脑出血发病的影响

目的探讨冰冻灾害及其他社会心理因素对脑出血患者发病的影响。方法应用自制一般情况量表、生活事件量表、社会支持量表、特质应对方式问卷、A型行为类型评定量表对60例脑出血患者及60例健康体检者进行病例对照研究。结果冰冻灾害、文化、职业、高血压病史、糖尿病病史、卒中家族史、正性事件刺激量、负性事件刺激量、事件刺激总量、主观支持、对支持的利用度、消极应对、积极应对,脑出血患者与健康体检者比较差异有统计学意义（P〈0.05或P〈0.01）。多元逐步Logistic回归分析发现：冰冻灾害、高血压病史、负性事件刺激量与脑出血呈正相关（P〈0.05或P〈0.01）,主观支持与脑出血呈负相关（P〈0.05）。结论冰冻灾害作为社会环境因素对脑出血患者发病有明显影响。     

钻孔灌注桩后注浆的分析和探讨

通过实测试验数据表明后注浆能够改善土层性质,提高单桩承载力,同等加荷下降低沉降值;但桩侧桩端联合注浆与仅桩端注浆对单桩承载力的提高幅度相当,桩侧注浆对侧摩阻力的影响离散性较大。后注浆桩的桩侧摩阻力极限值比未注浆的大,但在加荷过程中,多数土层仍会出现类似于未注浆土层的侧摩阻力软化现象。     

干熄焦锅炉炉管失效机理分析

通过对干熄焦锅炉炉管及腐蚀产物开展系统研究,提出炉管失效原因为氧化/硫腐蚀＋高温粉尘冲刷。长寿命炉管仅耐磨层发生了较为严重的氧化及硫腐蚀,而近基体层发生了轻微氧化及硫腐蚀,基体只发生了轻微氧化;短寿命炉管耐磨层、近基体层以及基体裂纹内均发生了较为严重的氧化及硫腐蚀,且存在珠光体球化、内表面产生全脱碳层等缺陷。推测短寿命炉管存在超温现象,而超温可加剧氧化及硫腐蚀反应。此外,短寿命炉管遭受了较为严重的高温粉尘冲刷,不仅可造成炉管减薄,还会导致炉管表面温度升高。因此,减少循环气体中粉尘量尤其是大颗粒,可有效减弱冲刷以及控制炉管表面温度,是提高炉管使用寿命的关键。     

Underwater Localization for Multiple AUVs Based on Bearing and Range Measurements

A novel underwater localization algorithm for autonomous underwater vehicle （AUVs） is proposed. Taking aim at the high cost of the traditional ＂leader-follower＂ positioning, a ＂parallel＂ model is adopted to describe the localization problem. Under an unknown-but-bounded assumption for sensor noise, bearing and range measurements can be modeled as linear constraints on the configuration space of the AUVs. Merged these constraints, a convex polyhedron representing the set of all configurations consistent with the sensor measurements can be induced. Estimates for the,uncertainty in the position of a single AUV or the relative positions of two or more AUVs can then be obtained by projecting this polyhedron into appropriate subspaces of the configuration space. The localization uncertain region for each AUV can be recovered by an approximation algorithm to realize underwater localization for multiple AUVs. The deduced theoretically and the simulated results show that it is an economical and practical localization method for the AUV swarm.     

茶叶多糖的研究进展

茶叶多糖是一种复合杂多糖，具有许多生物活性。作者系统地介绍了茶叶多糖的提取、分离、纯化、纯度鉴定及相对分子质量测定的方法，以及其含量和组成、理化性质、化学结构及空间构象、生物活性等方面的研究进展，并对上述方法及研究进展进行了分析和评述。     

苏氨酸锌的制备与表征

以苏氨酸和氧化锌为原料,在水溶液中反应合成了新型锌营养强化剂———苏氨酸锌螯合物。用EDTA络合滴定法、凯氏定氮法、IR、TG-DTA、ESI-MS等分析手段对制备的目的产物进行成分测定和结构表征,确定其化学式为C8H16N2O6Zn·2H2O。     

SENSITIVE AND RAPID DETECTION OF ENTEROBACTER SAKAZAKII IN INFANT FORMULA BY LOOP-MEDIATED ISOTHERMAL AMPLIFICATION METHOD

Enterobacter sakazakii is an emergent pathogen associated with ingestion of infant formula milk and was defined in category "A" of the hazard identification by FAO and WHO on microorganisms, which is based on the strength of evidence of a causal association between their presence in powdered infant formula and illness in infants. In this study, a loop-mediated isothermal amplification (LAMP) method has been developed for the detection of E. sakazakii in infant formula. The assay detected the species-specific DNA sequence of the 16S-23S rRNA internal transcribed spacer. The sensitivity of the detection is 1.2 cfu per 100 g infant formula with the selective enrichment. As the amplification is made under isothermal conditions, only a water bath or heating block is needed to maintain the required temperature. Thus, the method will be easily generalized and popularized in the future.

PRACTICAL APPLICATIONS

Enterobacter sakazakii is an emerging opportunistic pathogen associated with meningitis, bacteria and necrotizing enterocolitis in neonates. Powdered infant formulae have been implicated as the source of infection in neonatal meningitis. Thus, in order to minimize the hazard caused by E. sakazakii , it is of utmost importance to develop a rapid, sensitive and simple method for the early detection of this bacterium in infant formula.
In our study, the E. sakazakii was detected sensitively and rapidly in the infant formula by the loop-mediated isothermal amplification (LAMP) assay. LAMP is easy to perform once the appropriate primers are prepared. The LAMP method will be a simple and rapid method for the scene detection of E. sakazakii as only four primers, a Bst polymerase and a regular laboratory bath are needed.