Simultaneous spectrophotometric determination of copper(II), lead(II) and cadrnium(II)

The full spectrum technique in the fourier domain was studied for simultaneous determination of Cu(II), Pb(II) and Cd(II) with 4-(2-pyridylazo) resorcinol (PAR). A program called SPGRFSQ. was designed to perform the calculations. Seven error functions were calculated for deducing the number of factors. Data reduction was performed using principal component analysis (PCA) algorithm. Experimental results showed the method to be successful even where there was severe overlap of spectra.     

Reprint of “Suppressing propylene carbonate decomposition by coating graphite electrode foil with silver”

A method has been developed to suppress the decomposition of propylene carbonate (PC) by coating graphite electrode foil with a layer of silver. Results from electrochemical impedance measurements show that the Ag-coated graphite electrode presents lower charge transfer resistance and faster diffusion of lithium ions in comparison with the virginal one. Cyclic voltammograms and discharge-charge measurements suggest that the decomposition of propylene carbonate and co-intercalation of solvated lithium ions are prevented, and lithium ions can reversibly intercalate into and deintercalate from the Ag-coated graphite electrode. These results indicate that Ag-coating is a good way to improve the electrochemical performance of graphitic carbon in PC-based electrolyte solutions.     

A Performance Evaluation of Classic Convolutional Neural Networks for 2D and 3D Palmprint and Palm Vein Recognition

Palmprint recognition and palm vein recognition are two emerging biometrics technologies. In the past two decades, many traditional methods have been proposed for palmprint recognition and palm vein recognition, and have achieved impressive results. However, the research on deep learning-based palmprint recognition and palm vein recognition is still very preliminary. In this paper, in order to investigate the problem of deep learning based 2D and 3D palmprint recognition and palm vein recognition in-depth, we conduct performance evaluation of seventeen representative and classic convolutional neural networks (CNNs) on one 3D palmprint database, five 2D palmprint databases and two palm vein databases. A lot of experiments have been carried out in the conditions of different network structures, different learning rates, and different numbers of network layers. We have also conducted experiments on both separate data mode and mixed data mode. Experimental results show that these classic CNNs can achieve promising recognition results, and the recognition performance of recently proposed CNNs is better. Particularly, among classic CNNs, one of the recently proposed classic CNNs, i.e., EfficientNet achieves the best recognition accuracy. However, the recognition performance of classic CNNs is still slightly worse than that of some traditional recognition methods.

     

Reaction mechanism and microstructure evolution of reaction sintered <Emphasis Type="Italic">h</Emphasis>-BN

Hexagonal boron nitride ceramic (h-BN) based on the nitridation of B powders was obtained by reaction sintering method. The effects of sintering temperature on the mechanical properties and microstructure of the resultant products were investigated and the reaction mechanism was discussed. Results showed that the reaction between B and N₂ occurred vigorously at temperatures ranging from 1 000 °C to 1 300 °C, which resulted in the generation of t-BN. When the temperature exceeded 1 450 °C, transformation from t-BN to h-BN began to occur. As the sintering temperature increased, the spherical particles of t-BN gradually transformed into fine sheet particles of h-BN. These particles subsequently displayed a compact arrangement to achieve a more uniform microstructure, thereby increasing the strength.     

多视无人机影像环形拼接算法

由于多视无人机影像拼接时误差的传播和累计经常导致拼接图扭曲偏斜或者拼接的失败.针对这个问题提出了构建拼接环并以多级拼接作为辅助的拼接策略.首先将待拼接图像分为多组,每组中以环形方式进行拼接,然后利用SIFT进行匹配,RANSAC实现误匹配的去除,而后计算透视变换关系,最后通过平差方程将误差削弱.通过实拍无人机影像进行的拼接实验表明该方式可以有效减少累计误差的影响,提高拼接精度.该方法的提出可以作为影像拼接消除累计误差的有效方式之一.     

Mechanical analysis of double-layered circular graphene sheets as building material embedded in an elastic medium

Journal of Central South University - Possessing the unique and highly valuable properties, graphene sheets (GSs) have attracted increasing attention including that from the building engineer due...     

Modal Identification of Linear Time-varying Systems Using Continuous Wavelet Transform

A wavelet based identification method for linear time-varying systems is presented,and the ridge and skeleton of the continuous wavelet transform of free response is used to extract time-varying parameters. The stiffness and damping coefficients of single-degree-of—freedom systems,frequencies and damping ratios of multi-degree-of-freedom systems are estimated without any prior information of systems. The proposed method is applied to linear time-varying systems with both abrupt and smooth variation parameters. Gaussian white noise is added to the response to test the anti-noise performance of the algorithm. The simulation results show that the proposed method is capable of accurately tracking the variation of the systems.     

微小电偶腐蚀电流的准确测定

为了更多地获得电偶腐蚀的信息并揭示其本质规律，提出了电偶腐蚀试验实时监测模型。通过选用不同设备对试样的电偶腐蚀微小电流的测量，结果发现：选用现成设备测量试样的电偶腐蚀微小电流时，测量电流波动非常大，噪声明显超过实际信号输入——电偶腐蚀电流。经自行开发研制的MCD01电偶腐蚀计可以准确的测量腐蚀电流，特别是微小电偶腐蚀电流。     

利用金属络合物的电火花加工研究

在电火花加工的工作液中添加络合剂，使之与被蚀除的金属颗粒产生络合化学反应，生成可溶于工作液中的络合物。利用这种原理，可提高电火花加工性能，在小孔、深槽等加工应用中起到促进排屑的作用。     

用双层辉光等离子法在钛表面制备的Ti-Pd合金层性能研究

采用双层辉光等离子冶金技术在纯钛表面制备了Ti—Pd合金层。其深度大约为90μm，Pd含量呈梯度变化，并出现了TiPd3，TiPd2，Ti2Pd3，Ti3Pd5，TiPd，Ti4Pd等6种化合物相和Pd相。合金层在100℃的NaCl饱和溶液＋HCl溶液以及40℃的8．6％H2SO4溶液中的耐缝隙腐蚀性能优于Ti0．2Pd合金；在室温80％H2SO4的溶液中，腐蚀速率仅为0．682mm／a，是Ti0．2Pd合金的18．2％：在室温30％HCl的溶液中，表面Ti—Pd的腐蚀速率仅为0．004mm／a，是Ti0．2Pd合金的12．5％。