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91.
Ramasubba Reddy Palem Ganesh D. Shimoga Zuzana Kronekova Monika Sláviková Petr Saha 《国际聚合物材料杂志》2018,67(1):1-10
Chitosan–silver nanocomposites (CS-HDA-AgNCs) was prepared using chitosan, biogenic silver nanocomposites, and crosslinker, hexamethylene 1,6-di(amino carboxysulfonate) (HDA). The film is flexible and transparent. Its physical, mechanical, thermal, hydrophilicity, and swelling properties were improved by HDA (2.5%). The antimicrobial activity of CS-HDA-AgNCs were not displayed any remarkable zone of inhibition but showed toxic effect in the presence of normal 3T3 fibroblasts and cancer HeLa cells. It decreases to ca. 5–7% for both cell lines. In conclusion, it can be mentioned that the CS-HDA-AgNCs, a kind of new functional biomaterial, could be useful for health-care applications. 相似文献
92.
The search for fresh or potable water remains a pressing concern throughout many regions of the world. Although most of the Earth's surface is covered by oceans, the effort to provide for the world's inhabitants with fresh or potable water seems to be insurmountable; at least one billion people do not have access to clean and fresh water. The World Health Organization (WHO) reported that about 41% of the Earth's population lives in water-stressed areas, and the number of people in the water scarce regions may climb to 3.5 billion by the year 2025. Thus, innovative and cost-effective desalination technologies for producing fresh water are needed to provide practical solutions. 相似文献
93.
Brajendra Singh Ashutosh Kumar Dubey Samayendra Kumar Naresh Saha Bikramjit Basu Rajeev Gupta 《Materials science & engineering. C, Materials for biological applications》2011,31(7):1320-1329
Herein, we report the effect of silver ions on the physical, antimicrobial and cytocompatibility properties of wet chemically synthesized silver doped Ca10?xAgx(PO4)6(OH)2 (0.0 ≤ x ≤ 0.5) hydroxyapatites (HAp). Silver ions containing HAp exhibit the comparable density, hardness and enhanced antimicrobial properties, in comparison to parent HAp. The optical absorption measurements confirm the presence of silver ions in the doped compositions, which are responsible for as increased antimicrobial property of doped HAp materials for x > 0.3. The cytotoxicity behavior of the doped HAp was evaluated using mouse fibroblast (L929) cell line. The important result has been that doped HAp (x > 0.3) exhibit statistically (significant) lower cell viability in comparison to undoped HAp. However, no difference in cellular functionality on doped HAp surfaces, in terms of cell adhesion and proliferation could be qualitatively observed in reference to undoped HAp. In order to explain the observed antimicrobial and cell viability properties, the in vitro release of Ag+ ions has been quantified using Inductively Coupled Plasma-Atomic Emission Spectroscopy (ICP-AES) and solubility was measured by weight loss in acetate buffer solution. 相似文献
94.
Chinmoy Saha Siva Ponnupandian Francis R. Costa Gert Heinrich Nikhil K. Singha 《Polymer Engineering and Science》2021,61(12):3163-3169
This investigation reports the synthesis of a new class of polyurethane (PU) based on bis(hydroxyalkyl) polydimethylsiloxane (PDMS) as diol and isophorone diisocyanate as diisocyanate followed by the preparation of PU/layered double hydroxide (PU/LDH) nanocomposite via ex-situ technique. Nuclear magnetic resonance and Fourier-transform infrared spectroscopy studies confirm the formation of PU and incorporation of PDMS into the PU backbone. Thermogravimetry analysis revealed that thermal stability of the composite improves significantly with incorporation of LDH into the PU matrix. This may be accredited to the barrier effect rendered by the LDH layers. Differential scanning calorimetry study reveals that with the incorporation of LDH, glass transition temperature (Tg) of the composite increases for an optimum level of loading beyond which it remains constant. 相似文献
95.
This paper presents a review of studies on natural convection heat transfer in the triangular enclosure namely, in attic-shaped space. Much research activity has been devoted to this topic over the last three decades with a view to providing thermal comfort to the occupants in attic-shaped buildings and to minimising the energy costs associated with heating and air-conditioning. Two basic thermal boundary conditions of attic are considered to represent hot and cold climates or day and night time. This paper also reports on a significant number of studies which have been performed recently on other topics related to the attic space, for example, attics subject to localized heating and attics filled with porous media. 相似文献
96.
Sourabh K. Saha S.K. Choudhury 《International Journal of Machine Tools and Manufacture》2009,49(3-4):297-308
Dry electric discharge machining (EDM) is an environment-friendly modification of the oil EDM process in which liquid dielectric is replaced by a gaseous medium. In the current work, parametric analysis of the process has been performed with tubular copper tool electrode and mild steel workpiece. Experiments have been conducted using air as the dielectric medium to study the effect of gap voltage, discharge current, pulse-on time, duty factor, air pressure and spindle speed on material removal rate (MRR), surface roughness (Ra) and tool wear rate (TWR). First, a set of exploratory experiments has been performed to identify the optimum tool design and to select input parameters and their levels for later stage experiments. Empirical models for MRR, Ra and TWR have then been developed by performing a designed experiment based on the central composite design of experiments. Response surface analysis has been done using the developed models. Analysis of variance (ANOVA) tests were performed to identify the significant parameters. Current, duty factor, air pressure and spindle speed were found to have significant effects on MRR and Ra. However, TWR was found to be very small and independent of the input parameters. 相似文献
97.
Badal C Saha Michael A Cotta 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2007,82(10):913-919
BACKGROUND: The objective of this work is to develop an efficient pretreatment method that can help enzymes break down the complex carbohydrates present in wheat straw to sugars, and to then ferment of all these sugars to ethanol. RESULTS: The yield of sugars from wheat straw (8.6%, w/v) by lime pretreatment (100 mg g?1 straw, 121 °C, 1 h) and enzymatic hydrolysis (45 °C, pH 5.0, 120 h) using a cocktail of three commercial enzyme preparations (cellulase, β‐glucosidase, and xylanase) at the dose level of 0.15 mL of each enzyme preparation g?1 straw was 568 ± 13 mg g?1 (82% yield). The concentration of ethanol from lime pretreated enzyme saccharified wheat straw (78 g) hydrolyzate by recombinant Escherichia coli strain FBR5 at pH 6.5 and 35 °C in 24 h was 22.5 ± 0.6 g L?1 with a yield of 0.50 g g?1 available sugars (0.29 g g?1 straw). The ethanol concentration was 20.6 ± 0.4 g L?1 with a yield of 0.26 g g?1 straw in the case of simultaneous saccharification and fermentation by the E. coli strain at pH 6.0 and 35 °C in 72 h. CONCLUSION: The results are important in choosing a suitable pretreatment option for developing bioprocess technologies for conversion of wheat straw to fuel ethanol. Copyright © 2007 Society of Chemical Industry 相似文献
98.
The spi gene of Streptococcus pneumoniae was cloned and its nucleotide sequence was determined. It encodes a protein of 204 amino acids that is homologous to bacterial signal peptidase I proteins. The S. pneumoniae protein contains all of the conserved amino acid sequence motifs previously identified in this enzyme from both prokaryotic and eukaryotic sources. Sequence comparisons revealed several additional motifs characteristic of the enzyme. The cloned S. pneumoniae gene complemented an Escherichia coli mutant defective in its leader peptidase gene. Expression of the spi gene in S. pneumoniae appeared to be essential for viability. The cloned gene was shown to produce a polypeptide of approximately 20 kDa. Overproduction of the S. pneumoniae spi gene in an E. coli expression system gave a native protein product, soluble in the presence of a non-ionic detergent, which should be amenable to structural determination. 相似文献
99.
HD Kalter M Hossain G Burnham NZ Khan SK Saha MA Ali RE Black 《Canadian Metallurgical Quarterly》1999,13(1):99-113
The objective of this study was to validate retrospective caregiver interviews for diagnosing major causes of severe neonatal illness and death. A convenience sample of 149 infants aged < 28 days with one or more suspected diagnoses of interest (low birthweight/severe malnutrition, preterm birth, birth asphyxia, birth trauma, neonatal tetanus, pneumonia, meningitis, septicaemia, diarrhoea, congenital malformation or injury) was taken from patients admitted to two hospitals in Dhaka, Bangladesh. Study paediatricians performed a standardised history and physical examination and ordered laboratory and radiographic tests according to study criteria. With a median interval of 64.5 days after death or hospital discharge, caregivers of 118 (79%) infants were interviewed about their child's illness. Using reference diagnoses based on predefined clinical and laboratory criteria, the sensitivity and specificity of particular combinations of signs (algorithms) reported by the caregivers were ascertained. Sufficient numbers of children with five reference standard diagnoses were studied to validate caregiver reports. Algorithms with sensitivity and specificity > 80% were identified for neonatal tetanus, low birthweight/severe malnutrition and preterm delivery. Algorithms with specificities > 80% for birth asphyxia and pneumonia had sensitivities < 70%, or alternatively had high sensitivity with lower specificity. In settings with limited access to medical care, retrospective caregiver interviews provide a valid means of diagnosing several of the most common causes of severe neonatal illness and death. 相似文献
100.
Kasztenny B. Rosolowski E. Saha M.M. Hillstrom B. 《Power Delivery, IEEE Transactions on》1997,12(3):1119-1127
In the paper the fuzzy logic based multi-criteria protective relay for a three-phase power transformer is presented. Twelve criteria used to stabilize the relay are introduced and integrated by means of multi-objective decision-making methods. The introduced protection scheme contains several internal functions and coefficients which are subject to off-line pre-installation self-setting. Three unique procedures are delivered for self-adjusting the relay, and thus, making it self-organized. The results of testing show significant gains in both sensitivity and selectivity of the self-organized relay compared with traditional approaches 相似文献