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81.
Gian Luigi Angrisani Piriya Taptimthong Susanne Elisabeth Thürer Christian Klose Hans Jürgen Maier Marc Christopher Wurz Kai Möhwald 《Advanced Engineering Materials》2018,20(9)
82.
Mónica Giménez‐Marqués Elena Bellido Thomas Berthelot Teresa Simón‐Yarza Tania Hidalgo Rosana Simón‐Vázquez África González‐Fernández José Avila Maria Carmen Asensio Ruxandra Gref Patrick Couvreur Christian Serre Patricia Horcajada 《Small (Weinheim an der Bergstrasse, Germany)》2018,14(40)
Controlling the outer surface of nanometric metal–organic frameworks (nanoMOFs) and further understanding the in vivo effect of the coated material are crucial for the convenient biomedical applications of MOFs. However, in most studies, the surface modification protocol is often associated with significant toxicity and/or lack of selectivity. As an alternative, how the highly selective and general grafting GraftFast method leads, through a green and simple process, to the successful attachment of multifunctional biopolymers (polyethylene glycol (PEG) and hyaluronic acid) on the external surface of nanoMOFs is reported. In particular, effectively PEGylated iron trimesate MIL‐100(Fe) nanoparticles (NPs) exhibit suitable grafting stability and superior chemical and colloidal stability in different biofluids, while conserving full porosity and allowing the adsorption of bioactive molecules (cosmetic and antitumor agents). Furthermore, the nature of the MOF–PEG interaction is deeply investigated using high‐resolution soft X‐ray spectroscopy. Finally, a cell penetration study using the radio‐labeled antitumor agent gemcitabine monophosphate (3H‐GMP)‐loaded MIL‐100(Fe)@PEG NPs shows reduced macrophage phagocytosis, confirming a significant in vitro PEG furtiveness. 相似文献
83.
Kirsten Bobzin Christian Kalscheuer Parisa Hassanzadegan Aghdam 《Advanced Engineering Materials》2023,25(4):2201195
Crystalline α- and γ-Al2O3 exhibit in many applications high wear resistance, chemical resistance, and hot hardness, making them interesting materials for production engineering. To synthesize α-Al2O3 with high coating thickness of s ≥ 10 μm, chemical vapor deposition at temperatures T > 1000 °C is well established. However, there are almost no studies dealing with the synthesis of thick α-Al2O3 by physical vapor deposition (PVD) at high temperatures T > 700 °C. High-temperature deposition of thick coatings can be realized by means of the dense hollow cathode plasma, combined with the transport function of the plasma gas in high-speed (HS) PVD. Herein, crystalline α- and γ-Al2O3 films are deposited on cemented carbides at substrate temperatures T s ≈ 570 °C and T s ≈ 780 °C by HS-PVD. These coatings exhibit a thickness up to s = 20 μm. Moreover, phase analysis presents α-phases in coatings synthesized at substrate temperature of T s ≈ 780 °C with significant higher hardness than films by T s ≈ 570 °C. These release the potential of HS-PVD to synthesize α-Al2O3 coatings with high thickness. Thereby, a higher thickness of these coatings is beneficial for the wear protection of turning and die casting tools. 相似文献
84.
Sina Jafarzadeh Anders Christian Wulff Kurt Engelbrecht Christian Robert Haffenden Bahl 《Advanced Engineering Materials》2023,25(11):2201790
Obtaining a highly homogeneous magnetic field is desired for field-controlled applications. For example, the resolution of magnetic analysis methods can be improved by generating a stronger and more homogeneous field over the region of interest (ROI). A set of 3D-printed passive shims is fabricated using additive manufacturing to improve the magnetic field homogeneity of a Halbach magnet assembly. The feedstock is a custom acrylonitrile butadiene styrene (ABS)-hard magnet composite filament filled with 60% wt. isotropic NdFeB. Additionally, a method for investigating the remanence is developed and validated. The result reveals a good agreement between the new method and existing measurement techniques for the remanence of permanent magnets. It is also shown that the additive manufacturing procedure has negligible effects on the magnetic properties. Performing a parametric study over a rectangular ROI, an optimized shim configuration is achieved. In the optimized and 3D-printed configuration, the average norm of the magnetic flux density, Bnorm, is increased by 13% and, more importantly, a 43% increase in the magnetic uniformity is obtained. These results highlight the great potential of freeform manufacturing, namely, additive manufacturing, to tailor the properties of magnet structures. 相似文献
85.
Christoph Weigel Valeriya Cherkasova Mathias Holz Hai Binh Phi Christian Görner Tenorio Björn Wilbertz Leonard Voßgrag Thomas Fröhlich Steffen Strehle 《Advanced Engineering Materials》2023,25(9):2201873
Ultralow expansion (ULE) glasses are of special interest for temperature stabilized systems for example in precision metrology. Nowadays, ULE materials are mainly used in macroscopic and less in micromechanical systems. Reasons for this are a lack of technologies for parallel fabricating high-quality released microstructures with a high accuracy. As a result, there is a high demand in transferring these materials into miniaturized application examples, realistic system modeling, and the investigation of microscopic material properties. Herein, a technological base for fabricating released micromechanical structures and systems with a structure height above 100 μm in ULE 7972 glass is established. Herein, the main fabrication parameters that are important for the system design and contribute thus to the introduction of titanium silicate as material for glass-based micromechanical systems are discussed. To study the mechanical properties in combination with respective simulation models, microcantilevers are used as basic mechanical elements to evaluate technological parameters and other impact factors. The implemented models allow to predict the micromechanical system properties with a deviation of only ±5% and can thus effectively support the micromechanical system design in an early stage of development. 相似文献
86.
Christian Wolf Martin Prechtl René Bauer Michael Dinkel Fabian Beck Leopold Franz Viktor Neumeyer 《真空研究与实践》2023,35(1):35-39
To mark our anniversary, we are presenting articles that have been particularly appreciated by readers of our online edition once again in print. Here: 3D-Printing for High Vacuum Applications 3D printing technology has made the leap from a home-based private practice to industrial manufacturing. Due to the increasing reliability of printers and increasing material diversity, especially in the metal sector, double-digit percentage growth rates are possible in the coming years. This thesis deals with the manufacture of parts made by 3D printing for high vacuum application. Different components are printed and examined for their vacuum compatibility. As shown furthermore, conventionally made standard components can be vacuum sealed to printed parts, which enables cost-effective production of more complex components, such as e.g. a vacuum chamber allows. In addition, functional components can already be realized in the manufacturing process. The integration of a system of flow channels directly into the wall of a chamber is just one example. Thus, such a chamber can be heated during evacuation and effectively cool in later operation. 相似文献
87.
Jürgen R. Reichenbach Marco Essig E. Mark Haacke Benjamin C. Lee Christian Przetak Werner A. Kaiser Lothar R. Schad 《Magma (New York, N.Y.)》1998,6(1):62-69
The purpose of this study was to evaluate a non-flow related magnetic resonance imaging method to visualize small veins independent of arteries in the human brain. A long TE, high-resolution 3D gradient echo MR acquisition was used to highlight venous information. The method is based on the paramagnetic property of deoxyhemoglobin and the resulting phase difference between veins and brain parenchyma at long echo times. The MR magnitude images were masked with a phase mask filter to enhance small structure visibility.. Venous information down to sub-pixel vessel diameters of several hundred microns is visible. Venous data are displayed in an angiographic manner using a minimum intensity projection algorithm. Both superficial veins and deep white matter veins are visible. The method has been successfully applied in volunteers. Preliminary results in patients with cerebral arteriovenous malformations indicate its potential in clinical applications. The proposed method is easy to implement and does not require administration of a contrast agent or application of specially designed rf pulses to highlight the veins. Rather it exploits the intrinsic magnetic properties (BOLD-effect) and the prolonged T 2* of venous blood. The method may be of diagnostic potential in the assessment of arteriovenous malformations or other vascular venous lesions. © 1998 Elsevier Science B.V. All rights reserved. 相似文献
88.
We discuss the design of a complete, compact holographic storage demonstrator based on a combination of spatial and angular multiplexing and using acousto-optic deflectors for rapid nonmechanical access. We also describe the implementation of this design and preliminary results of both the analog storage and the retrieval of 20,000 holograms in twenty 1-mm-thick layers of a lithium niobate crystal and of the digital storage and error-free retrieval of color images by using error-correcting techniques. 相似文献
89.
Lei Tang Zhiwen Yu Xingshe Zhou Hanbo Wang Christian Becker 《Personal and Ubiquitous Computing》2011,15(3):253-269
Along with the improvement of the key technologies for pervasive computing, the design of applications itself has emerged
as a notable research area. A design should decide which features go into the application of supporting its context-awareness
and ascertaining how well those features add value for users with an acceptable user experience. This paper initially identifies
the challenges in designing and evaluating pervasive applications. It then presents a condensed survey of prototyping techniques
and existing toolkits with the aim of understanding how the design issues have been addressed by research prototypes. At the
end, we describe various open issues with suggestions of possible ways to extend the capabilities of current prototyping toolkits. 相似文献
90.
The IEEE standardized Property Specification Language, PSL for short, extends the well-known linear-time temporal logic LTL with so-called semi-extended regular expressions. PSL
and the closely related SystemVerilog Assertions, SVA for short, are increasingly used in many phases of the hardware design cycle, from specification to verification. In
this article, we extend the common core of these specification languages with past operators. We name this extension PPSL.
Although all ω-regular properties are expressible in PSL, SVA, and PPSL, past operators often allow one to specify properties more naturally
and concisely. In fact, we show that PPSL is exponentially more succinct than the cores of PSL and SVA. On the star-free properties,
PPSL is double exponentially more succinct than LTL. Furthermore, we present a translation of PPSL into language-equivalent
nondeterministic Büchi automata, which is based on novel constructions for 2-way alternating automata. The upper bound on
the size of the resulting nondeterministic Büchi automata obtained by our translation is almost the same as the upper bound
for the nondeterministic Büchi automata obtained from existing translations for PSL and SVA. Consequently, the satisfiability
problem and the model-checking problem for PPSL fall into the same complexity classes as the corresponding problems for PSL
and SVA. 相似文献