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11.
Paola Cristina Cajas Daza Rodrigo Arbey Muñoz Meneses Ana Candida Martins Rodrigues Cosme Roberto Moreira da Silva 《Ceramics International》2018,44(12):13699-13705
Doped CeGdO and codoped CeGdOSmO compositions were synthesized, giving rise to nanoparticulate powders. Ionic conductivities at bulk and grain boundaries of the sintered samples were determined, exhibiting increased conductivity in the samaria-codoped samples. Scanning electron microscopy (SEM) showed a significant reduction in the grain size of samaria-codoped electrolytes. This reduced grain size of the codoped samples caused a reduction in Schottky barrier height, increasing oxygen vacancy concentration in the space-charge layer of the grain boundary and culminating in greater ionic conductivity in the boundary region. For the gadolinium doped samples, high resolution transmission electron microscopy images at grains showed the presence of large cluster of defects (nanodomains), hindering the movement of charge carriers and reducing ionic conductivity. However, the samaria-codoped system displayed better homogeneity at atomic level, resulting in reduced oxygen vacancy ordering and, consequently, smaller nanodomains and higher bulk (grain) conductivity. The reduced grain sizes and smaller nanodomains caused by codoping favor the ionic conductivity of ceria-based ceramics, doped with gadolinia and codoped with samaria. 相似文献
12.
Marcia Cristina Kaezer Fran a Rosane Aguiar da Silva San Gil Jean-Guillaume Eon 《Catalysis Today》2003,78(1-4):105-115
γ-Al2O3 supported vanadium oxides were modified by tungsten and molybdenum oxides in order to improve dispersion and selectivity towards olefins in propane oxidative dehydrogenation (ODH). Both vanadium–tungsten and vanadium–molybdenum catalysts were obtained by adsorption of mixed isopolyanions (VW5O195−, V2W4O194−, VMo5O195− and V2Mo4O194−) from aqueous solutions. The isopolyanion solutions were characterized by UV-Vis and 51V NMR spectroscopy. Vanadium, vanadium–tungsten and vanadium–molybdenum precursors and catalysts were also characterized by UV-Vis (diffuse reflectance) and solid state 51V NMR spectroscopy. An improved selectivity to propene in the presence of tungsten and molybdenum in VOx/γ-Al2O3 was observed and attributed to dilution of vanadium by tungsten or molybdenum oxides on the γ-Al2O3 surface. 相似文献
13.
In this paper we describe, from a theoretical point of view, critical configurations for the projective reconstruction of
a set of points, for a single view, i.e. for calibration of a camera, in the case of projections from ℙk to ℙ2 for k ≥ 4. We give first a general result describing these critical loci in ℙk, which, if irreducible, are algebraic varieties of dimension k−2 and degree 3. If k=4 they can be either a smooth ruled surface or a cone and if k = 5 they can be a smooth three dimensional variety, ruled in planes, or a cone. If k≥ 6, the variety is always a cone, the
vertex of which has dimension at least k − 6. The reducible cases are studied in Appendix A.
These results are then applied to determine explicitly the critical loci for the projections from ℙk which arise from the dynamic scenes in ℙ3 considered in [13].
Marina Bertolini is currently Associate Professor of Geometry at the Department of Mathematics at the Università degli Studi di Milano, Italy.
Her main field of research is Complex Projective Algebraic Geometry, with particular interest for the classification of projective
varieties and for the geometry of Grassmann varieties. On these topics M. Bertolini has published more than twenty reviewed
papers on national and international journals. She has been for some years now interested also in applications of Algebraic
Geometry to Computer Vision problems.
Cristina Turrini is Associate Professor of Geometry at the Department of Mathematics of Università degli Studi di Milano, Italy. Her main
research interest is Complex Projective Algebraic Geometry: subvarieties of Grassmannians, special varieties, automorphisms,
classification. In the last two years she has started to work on applications of Algebraic Geometry to problems of Computer
Vision. She is author or co-author of about thirty reviewed papers. She is also involved in popularization of Mathematics,
and on this subject she is co-editor of some books. 相似文献
14.
The characterization of new synthesized chiral polymeric membranes, based in polysulfone polymer is here reported. Polysulfone was derivatized to chiral polysulfone, by bonding covalently the chiral carrier, N-dodecyl-4(R)-hydroxy-l-proline, to the polymer matrix. Two different chiral polysulfones, referred to as CPSA and CPSB, have been synthesized and used in the preparation of chiral polymeric membranes. However, as a consequence of the limited CPSB solubility, only CPSA resulted adequate to obtain useful membranes. Therefore, various chiral polysulfone membranes containing different amounts of CPSA in unmodified polysulfone (PS) were prepared and properly characterized by scanning electron microscopy (SEM) and by enantioselective transport experiments of racemic propranolol. Dialysis transport experiments allowed us to determine the influence of the carrier content in the membrane on the transport rate and on enantiomer separation. Membranes containing a CPSA/PS ratio of 1:3 showed an alpha value of 1.1 at 96 h of performance. Modelling of the propranolol transport rate is also performed. 相似文献
15.
Batch process industries are characterized by complex precedence relationships between operations, which renders the estimation
of an acceptable workload very difficult. A detailed schedule based model can be used for this purpose, but for large problems
this may require a prohibitive large amount of computation time. We propose a regression based model to estimate the makespan
of a set of jobs. We extend earlier work based on deterministic processing times by considering Erlang-distributed processing
times in our model. This regression-based model is used to support customer order acceptance. Three order acceptance policies
are compared by means of simulation experiments: a scheduling policy, a workload policy and a regression policy. The results
indicate that the performance of the regression policy can compete with the performance of the scheduling policy in situations
with high variety in the job mix and high uncertainty in the processing times.
Correspondence to: C.V. Ivanescu 相似文献
16.
When humans plan to execute a tool-use action, they can only specify the bodily movement parameters by taking into account the external target or goal of the tool-use action and the target-movement mapping implemented by the tool. In this study, the authors used the movement precuing method to investigate how people prepare for actions made with tools. More specifically, they asked whether people would be able to specify the spatial target and the target-movement mapping of the tool-use action independently of each other, and to what degree they would be able to prepare these components in advance. In 3 experiments, they precued either the target or the target-movement mapping of tool-use actions involving either a compatible or an incompatible target-movement mapping. Results indicate that participants benefit from partial advance information about the target-movement mapping, whereas no significant effects were found for precuing the spatial target of the action. These results occurred regardless of whether the target-movement mapping was compatible or incompatible and provide evidence for the notion that the target-movement mapping of a tool-use action is part of its cognitive representation. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
17.
Peter Eaton Andrea Ragusa Caroline Clavel Cristina T Rojas Paul Graham Raúl V Durán Soledad Penadés 《IEEE transactions on nanobioscience》2007,6(4):309-318
Glyconanoparticles which present carbohydrate and amino groups motifs at their surface were produced. These particles were highly stable and soluble in aqueous solutions. The presence of the carbohydrate groups also allowed the inclusion of more strongly binding groups, without affecting solubility. The binding of a model DNA, plasmid by these nanoparticles was studied by atomic force microscopy, transmission electron microscopy, and gel electrophoresis. Significant differences between the nanoparticles based on their affinities for the DNA were found, with implications for their potential use as nonviral gene delivery agents. 相似文献
18.
Simultaneous HPLC quantification of total cholesterol,tocopherols and β-carotene in Barrosã-PDO veal 总被引:1,自引:0,他引:1
José A. Mestre Prates Mário A. Gonçalves Quaresma Rui J. Branquinho Bessa Carlos M.G. Andrade Fontes Cristina M.P. Mateus Alfaia 《Food chemistry》2006
A simple, rapid and sensitive procedure for the simultaneous determination of total cholesterol, tocopherols and β-carotene in meat is described. The method involves a direct saponification of the meat, a single n-hexane extraction and the analysis of the extracted compounds by normal-phase HPLC, using fluorescence (tocopherols) and UV–Vis photodiode array (cholesterol and β-carotene) detections in tandem. Rates of recovery of spiked meat samples were 93% for cholesterol, 83–86% for (α-, β- and -γ) tocopherols and 89% for β-carotene. Repeatabilities were high (CV < 6%) for all determined compounds, except for δ-tocopherol. This tocopherol, which is not usually present in meat, showed a much lower recovery percentage (73%) and repeatability (12.8%). This methodology was applied for the quantification of total cholesterol, tocopherols and β-carotene in three muscles (longissimus thoracis, longissimus lumborum and semitendinosus) of the Portuguese traditional Barrosã-PDO veal, obtained from autochthonous calves fed extensively during summer (with the least abundant green pastures) and slaughtered in early autumn (October). Barrosã-PDO veal showed median contents of total cholesterol (0.50–0.56 mg/g) and, depending on the analysed muscle, moderate to high contents of α-tocopherol (3.3–3.9 μg/g) and β-carotene (0.07–0.09 μg/g), suggesting an high sensorial and hygienic quality. 相似文献
19.
Influence of electroosmotic treatment on the hydro-mechanical behaviour of clayey silts: preliminary experimental results 总被引:1,自引:0,他引:1
Laura Gabrieli Cristina Jommi Guido Musso Enrique Romero 《Journal of Applied Electrochemistry》2008,38(7):1043-1051
Preliminary results of an investigation focused on the influence of electrokinetic treatment on the mechanical and hydraulic
behaviour of clayey soils are presented. The experimental programme aims at providing a contribution to the sustainability
of contaminant extraction or containment via electroosmosis. Changes in the hydraulic and mechanical properties of two illitic
clayey soils, subjected to a DC electric field, were investigated. Samples of the two soils were subjected to electrokinetic
filtration, for different periods of time, and under different constant loads. Afterwards, they were tested under one-dimensional
compression to detect changes in stiffness and hydraulic conductivity due to the electrical treatment. After the application
of a DC field for a few hours, a small reversible increment in the average soil stiffness was observed, with respect to the
untreated soil, while the hydraulic conductivity was not affected substantially. Dramatic changes of the mechanical and hydraulic
soil properties, correlated to changes of the soil pH, were observed following non-conditioned electrokinetic treatment with
duration of the order of days. 相似文献
20.
R Centurioni P Leoni M Candela M Cristina Refe A Stella Strusi L Fabietti G Danieli 《Canadian Metallurgical Quarterly》1996,87(4):161-163
In absence of thrombocytosis, periodic bloodlettings represent the elective therapy of polycythemia vera. In the present study we tested if neocytoapheresis, a method able to remove large quantities of younger, and then bigger red cells could represent an alternative therapeutic choice in these patients. We found that the employment of neocytoapheresis produced a remarkable delay in the time of procedures with a mean interval of 100 +/- 55 days. The mean value of hematocrit before neocytopheresis is resulted statistically different in comparison with the hematocrit after the procedure (p = 0.0001). The reticulocyte count is resulted higher in apheresis product in comparison with the blood control measured before procedure (p = 0.0001). In the same way, the mean corpuscular volume in the collection bags was higher than the volume measured before neocytoapheresis (p = 0.0095). We did not find any variation about the mean values of white blood cells and platelets before and after neocytoapheresis in the patients examined. These preliminary data seem to underline a better withdrawal of big size cells by this technique suggesting the efficacy of neocytoapheresis in the treatment of polycythemia vera. 相似文献