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51.
52.
Gang Li Dan I. Enache Jennifer Edwards Albert F. Carley David W. Knight Graham J. Hutchings 《Catalysis Letters》2006,110(1-2):7-13
The oxidation of benzyl alcohol to benzaldehyde has been investigated in the absence of solvent using zeolite-supported Au
and Au–Pd catalysts. Three zeolites were investigated, ZSM-5, zeolite β and zeolite Y, and these were contrasted with the
titanoslicalite TS-1 and TiO2 as supports. For the Au catalysts the best results are obtained with zeolite β as the support and the conversions were comparable
or better than those observed with TiO2 in terms of turn over frequencies. However, the selectivities observed with the acidic zeolites were lower than the non-acidic
TS-1 and TiO2. This is due to the subsequent reaction of benzaldehyde via acid catalysed reactions to give benzyl benzoate and its dibenzyl
acetal, and, in some cases dibenzylether. Initial catalysts were evaluated with a gold loading of 2 wt% and increasing this
to 4 wt% showed the expected increase in activity, indicating that there is scope to improve the performance of these catalysts.
The most active catalysts were prepared by impregnation and catalysts prepared by deposition precipitation were considerably
less active. Introduction of Pd into the catalyst improved the activity without significantly affecting the selectivity. 相似文献
53.
纳米碳酸钙在涂料中的应用研究 总被引:3,自引:0,他引:3
探究纳米碳酸钙先在溶剂中分散再与树脂进行调配的方法。利用正交设计法对其中高速搅拌法进行优惠条件实验,发现搅拌时间并非越长越好,优惠条件下涂料中纳米碳酸钙分散到原始粒径,涂料质量有较大提高。 相似文献
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反相微乳液法制备高溶度ZrO2陶瓷墨水(Ⅰ) 总被引:7,自引:0,他引:7
尝试采用新颖的反相微乳液法制备陶瓷墨水,为了获得高溶度陶瓷墨水,对反相微乳液体系优选进行研究,着重就Triton x-100/醇/烷/水体系,采用目测法,分光光度法,电导率法和离心分离法,分别考察了不同醇,烷配伍时体系的稳定性和相关物理性质,根据这些性质是否突变以确定体系是否发生相变,给出了体系拟三元相图。实验表明,在20℃时Triton x-100/正己醇/环己烷/水反相微乳液体系表现优异,当Triton x-100与正醇的质量比为3:2时达到最大范围的反相微乳液区,最大溶水量时的最佳组成为Triton x-100:正己醇:环己烷:水=19.1%:12.8%:23.7%:44.4%(质量比)。 相似文献
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In manufacturing industries, the quality of a product depends on the combined effect of multiple input variables working singly or together and therefore attention has been given on process capability indices to shift from single to multivariate domain. In case of multivariable domain the capability to incorporate uncertainties at the time of decision making becomes necessary. Fuzzy system is introduced to take care of this requirement. In this article the process parameters of soap manufacturing industries have been analyzed. The process capability is determined using Fuzzy Inference System rule editor based on a set of justified if then statements as applicable for the process. The data has been collected in linguistic form to derive its process capability, using a set of justified rules and the effect of each factor has been determined using Design of Experiments (DoE) and analysis of variance technique (ANOVA) for improving the soap quality from perspective of its softness. This article ventures to propose a new methodology by integrating Fuzzy with DoE providing better result followed by DoE and Fuzzy Inference system in isolation. 相似文献
59.
Recent progress in road and lane detection: a survey 总被引:2,自引:0,他引:2
The problem of road or lane perception is a crucial enabler for advanced driver assistance systems. As such, it has been an active field of research for the past two decades with considerable progress made in the past few years. The problem was confronted under various scenarios, with different task definitions, leading to usage of diverse sensing modalities and approaches. In this paper we survey the approaches and the algorithmic techniques devised for the various modalities over the last 5 years. We present a generic break down of the problem into its functional building blocks and elaborate the wide range of proposed methods within this scheme. For each functional block, we describe the possible implementations suggested and analyze their underlying assumptions. While impressive advancements were demonstrated at limited scenarios, inspection into the needs of next generation systems reveals significant gaps. We identify these gaps and suggest research directions that may bridge them. 相似文献
60.
耐药大肠杆菌的致病性与免疫原性 总被引:1,自引:0,他引:1
目的了解大肠杆菌耐药株的致病性与免疫原性。方法临床分离耐药大肠杆菌,经适宜条件培养后接种小鼠,观察耐药菌株对小鼠的致病性;并选择已知血清型的不同耐药谱和不同耐药水平的菌,分别培养至对数生长期,经甲醛灭活后免疫小鼠,2周后分别用致死剂量的原菌株和同期分离菌株进行攻毒,考察耐药菌株免疫原性。结果24株耐药菌普通肉汤培养物分别感染小鼠,在接种后18h,存活率仅为4%。只有2株菌在1周内仍不能将小鼠全部致死,经小鼠体内传3代后,可在18h内致死小鼠。耐药谱广的菌株感染的小鼠,心肌发生颗粒变性、局灶性出血、坏死;肝脏糖元溶解,脂肪变性;脾脏轻度淤血,淋巴细胞减少;肾脏出血,肾小球肾炎,上皮细胞颗粒变性,水泡变性。而耐药种类少的菌株与对照敏感菌株感染的小鼠主要特征为脾脏出血、淤血,坏死,脾小体消失;肠上皮细胞坏死、脱落、卡他性肠炎。免疫小鼠以免疫用菌株攻毒,均可得较高的保护率,最低为75%,最高为100%。免疫小鼠用非免疫菌株攻毒,小鼠感染后症状出现较缓慢,在18h后出现死亡高峰。耐药种类少的菌株免疫小鼠,对同期分离的非免疫用的致病性大肠杆菌攻击的保护率偏低,而对受试的11种抗生素耐受7种以上的菌株免疫小鼠后,对致病大肠杆菌攻击的保护率显著提高,多数达到75%以上,经统计学分析差异显著。结论耐药大肠杆菌具有较强致病性,且耐药特性与其免疫保护效果相关,多重耐药株对当前流行菌株具有更好的免疫保护作用。 相似文献