碳纤维增强氮化物基复合材料的制备及其性能表征

合成了全氢聚硅氮烷和硼氮烷的混杂先驱体并对其结构进行了表征；以混杂先驱体和3D碳纤维编制体为原料，采用先驱体浸渍-裂解（PIP）工艺制得了碳纤维增强氮化硼．氮化硅混杂基体的复合材料，并对复合材料的力学性能和抗烧蚀性能进行了研究。结果表明，混杂先驱体中含有B—N，B—H，Si—N，Si—H，N—H等结构，无其它杂质出现；随着PIP工艺循环次数的增加，复合材料的密度随之提高：当进行4个循环时基本致密，密度达到1．50g／cm^3，弯曲强度达到156．4MPa；轨道模拟实验显示复合材料具有优异的抗烧蚀性能。     

保温条件下过共晶Al-Si合金半固态浆料的组织演变

研究了保温时间和保温温度对电磁搅拌ZL117合金半固态浆料稳定性的影响.试验结果表明：半固态浆料中初生Si的颗粒直径随着保温时间的延长而逐渐增大,但在前15 min内增长速度比较缓慢,15 min后增长较快;随着保温温度的升高而缓慢增大;初生Si的形状系数随着保温时间的延长而变得越来越大,但也在前15 min内变化较为缓慢,15 min后变大速度突然加快;初生Si的形状系数在620 ℃下保温时最小,在610～620 ℃之间随着保温温度的升高而缓慢变小;在620～650 ℃之间随着保温温度的升高而逐渐增加.     

倾斜板角度对亚共晶高铬铸铁半固态组织的影响

采用倾斜板冷却体法对亚共晶高铬铸铁进行半固态成形,研究了倾斜板角度对亚共晶高铬铸铁半固态组织的影响规律。结果表明:倾斜板角度过大或过小都将使得组织中的初生奥氏体较粗大、圆整度较小。当倾斜板角度较小时,金属液的流速相对较慢,枝晶与枝晶和枝晶与金属液间的冲刷、碰撞、剪切作用较小,晶粒易于长大,导致枝晶状初生奥氏体比较多。当倾斜板角度较大时,金属液流速相对较快,金属液在倾斜板上流动的时间相对较短,枝晶间以及枝晶与金属液间的冲刷、碰撞、剪切作用时间相对较短,导致枝晶状初生奥氏体也比较多。当倾斜板角度为45°时,制备的亚共晶高铬铸铁初生奥氏体的尺寸最小,圆整度最高。     

大型薄壁组焊椭圆封头尺寸及变形的控制工艺

叙述了在压力容器制造中,当简体组装、封头分片压制后,焊接大型薄壁椭圆封头,其尺寸和角变形量的控制工艺。     

面向问题的小组课题工作--一种以学生为中心的教学模式

在欧美的大学中 ,课题工作是普遍采用的一种教学方法。为顺应科学技术的发展以及社会经济的变革 ,70年代初成立的丹麦罗斯基勒大学在传统的课题工作模式基础上 ,创造了一种以学生为中心的教学模式———面向问题的小组课题工作。这是一种开展于学生和教师之间 ,两者互相影响而由学生主导的实践性教学活动。一些传统的教学手段和方法受到了冲击。这一模式的实际操作步骤是程式化的。这一模式与建构主义的学习理论存在着较明显的联系。国内的大学教学模式的改革可以从中获得启示和借鉴。     

国外超细金丝的生产技术

介绍超细金丝的生产及其对生产环境和原料的要求,金丝的品种类型和化学成分,金丝的力学性能及其与键合特性的关联.着重介绍两种主要的生产方法和技术特点,讨论金丝代用材料的研制情况.     

Comparative study of bis-piperidiniummethyl-urea and mono-piperidiniummethyl-urea as volatile corrosion inhibitors for mild steel

Bis-piperidiniummethyl-urea (BPMU) and mono-piperidiniummethyl-urea (MPMU) were developed as novel volatile corrosion inhibitors (VCIs). Their vapor corrosion inhibition property was evaluated by volatile inhibiting sieve test (VIS) and vapor inhibiting ability test (VIA). Volatile weight-loss test in a closed space was used to compare their volatility. Electrochemical impedance spectroscopy of a volatile corrosion inhibitor monitor (VCIM) was applied to study the effect of BPMU and MPMU on the corrosion inhibition of mild steel in thin electrolyte layer. The results show that BPMU has the better protection effect compared with MPMU. Adsorption of BPMU and MPMU on steel surface was investigated by X-ray photoelectron spectroscopy (XPS). It was shown that one BPMU molecule has two N atoms to coordinate with one Fe atom, and that one MPMU molecule has one N atom to coordinate with one Fe atom. The quantum chemical parameters were obtained by PM3 semi-empirical method. BPMU has the smaller HOMO-LUMO energy gap and the smaller net positive charge intensities of 4N and 8N atoms in its molecule.     

一种新型振动下料机的PLC控制

在分析了新型振动下料机采用继电器－接触器控制方式存在不足的基础上，指出了对其进行PLC控制的必要性。分析了该振动下料机的基本构成及工作原理，建立了相应的液压系统。针对下料机正常工作对控制系统要求，确定了PLC的输入量及输出量，建立了PLC控制的硬件接线图，编制了相应的梯形图控制软件。大量实验验证了该控制方案的可行性和实用性。     

Microstructure and tensile properties of squeeze cast magnesium alloy AM50

High-pressure die cast magnesium alloy AM50 is currently used extensively in large and complex shaped thin-wall automotive components. For further expansion of the alloy usage in automobiles, novelmanufacturing processes need to be developed. In this study, squeeze casting of AM50 alloy with a relatively thick cross section was carried out using a hydraulic press with an applied pressure of 70 MPa. Microstructure and mechanical properties of the squeeze cast AM50 with a cross-section thickness of 10 mm were characterized in comparison with the die cast counterpart. The squeeze cast AM50 alloy exhibits virtually no porosity in the microstructure as evaluated by both optical microscopy and the density measurement technique. The results of tensile testing indicate the improved tensile properties, specifically ultimate tensile strength and elongation, for the squeeze cast samples over the conventional high-pressure die cast parts. The analysis of tensile behavior show that the strain-hardening rate during the plastic deformation of the squeeze cast specimens is constantly higher than that of the die cast specimens. The scanning electron microscopy fractography evidently reveals the ductile fracture features of the squeeze cast alloy AM50.     

中南大学学科布局及结构调整研究

学科结构及布局关系到高等学校整体功能的发挥和全局的发展 ,它直接影响人才培养的质量、规格、类型 ,关系到科研与创新能力和水平 ,最终影响到学校发展目标的实现。本文根据中南大学“综合性研究型大学”的发展目标 ,就中南大学学科布局和结构调整进行了研究。