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31.
Yu‐Qing Cao Zhan Zhang Yan‐Xin Guo 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2008,83(10):1441-1444
A new efficient method for synthesising nitriles, important organic reagents, is reported in this paper. In an environmentally benign solvent‐free system, aryl carboxylic acids were converted into the corresponding nitriles via one‐pot reactions, by amidation with ethyl carbamate followed by dehydration with thionyl chloride, in excellent yields. The results showed that the method has the advantages of lower cost, higher yield, less pollution and greater ease of work‐up. Copyright © 2008 Society of Chemical Industry 相似文献
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王家沟流域属暖温带大陆性季风气候,冬季严寒少雪,春季干燥多风,夏季酷热多雨,秋季温凉适中,雨热同季,当地常见暴雨历时大多在2h以下,这种短历时、大强度的暴雨最易引起水土流失。分析了流域治理前后径流泥沙的来源情况,为同类型小流域综合治理提供科学依据。 相似文献
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35.
Sosnowchik B.D. Azevedo R.G. Cao A. Lin L. Pisano A.P. 《Advanced Packaging, IEEE Transactions on》2005,28(4):626-634
This paper presents the rapid, low-temperature bonding between silicon and steel using the rapid thermal annealing process. Three different thin-film adhesion layer systems including silver, gold, and nickel were utilized as the intermediate bonding material to assist the eutectic Pb/Sn bonding between silicon and steel. The bonding temperature was set at 220/spl deg/C for 20 s, with a 20-s ramp-up time. Five experiments were conducted to determine the strength of the bond, including static tensile and compressive four-point bend tests, axial extension tests, tensile bending fatigue tests, and corrosion resistance tests. The test results have shown that the gold adhesion layer is the most robust, demonstrating minimal creep during fatigue tests, no delamination during the tensile or compressive four-point bend tests, and acceptable strength during the axial extension tests. Additionally, all adhesion layers have withstood four months of submersion in various high-temperature solutions and lubricants without failure. Simulations of the axial stresses and strains that developed during the four-point bend and axial extension tests were performed and showed that the presence of the silicon die provides a local reinforcement of the bond as observed in the experimental tests. 相似文献
36.
Xue‐Bing Zhao Lei Wang De‐Hua Liu 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2008,83(6):950-956
Previous work has shown that the enzymatic hydrolysis of sugarcane bagasse could be greatly enhanced by peracetic acid (PAA) pretreatment. There are several factors affecting the enzymatic digestibility of the biomass, including lignin and hemicelluloses content, cellulose crystallinity, acetyl group content, accessible surface area and so on. The objective of this work is to analyze the mechanism of the enhancement of enzymatic digestibility caused by PAA pretreatment. Delignification resulted in an increase of the surface area and reduction of the irreversible absorption of cellulase, which helped to increase the enzymatic digestibility. The Fourier transform infrared (FTIR) spectrum showed that the absorption peaks of aromatic skeletal vibrations were weakened or disappeared after PAA pretreatment. However, the infrared crystallization index (N.O'KI) was increased. X‐ray diffraction (XRD) analysis indicated that the crystallinity of PAA‐treated samples was increased owing to the partial removal of amorphous lignin and hemicelluloses and probable physical change of cellulose. The effect of acetyl group content on enzymatic digestibility is negligible compared with the degree of delignification and crystallinity. The results indicate that enhancement of enzymatic digestibility of sugarcane bagasse by PAA pretreatment is achieved mainly by delignification and an increase in the surface area and exposure of cellulose fibers. Copyright © 2008 Society of Chemical Industry 相似文献
37.
A new torque estimator for switched reluctance motor (SRM) drives based on 2-D rotary regression analysis is presented in this paper. The proposed torque estimator is composed of a bicubic regressive polynomial as a function of rotor position and input current. The regressive coefficients can be computed offline or online from the torque characteristics acquired either experimentally or from numerical computation. Furthermore, a torque estimation method by taking mutual coupling into consideration is proposed. It can be seen that the estimated and experimentally obtained self-coupling and mutual-coupling torque characteristics are in good agreement with each other. In addition, the dynamic torque waveforms with and without the mutual coupling, estimated by the proposed estimator, are found to be virtually the same as those obtained from the bicubic spline interpolation for SRM drives with single-pulse voltage, hysteresis current chopping, as well as with voltage pulse width modulation control. The success of all the case studies being reported is a good validation of the usefulness and accuracy of the proposed real-time torque estimator that, as described in this paper, can be used to quickly estimate the instantaneous output torque of SRM drives. 相似文献
38.
3-D MCM封装技术及其应用 总被引:1,自引:0,他引:1
介绍了超大规模集成电路(VLSI)用的3-D MCM封装技术的最新发展,重点介绍了3-D MCM封装垂直互连工艺,分析了3-D MCM封装技术的硅效率、复杂程度、热处理、互连密度、系统功率与速度等问题,并对3-D MCM封装的应用作了简要说明。 相似文献
39.
40.
Jiayong Cao Yu Zhu Jinsong Wang Wensheng Yin Guanghong Duan 《IEEE transactions on magnetics》2004,40(6):3490-3494
This paper investigates three kinds of permanent-magnet arrays used in planar motors with polarity centers distributed in the lattices of a matrix. The magnetic field of every kind of magnet array is analyzed by analytical methods. First, we give a Laplace equation of magnetic scalar potential and a series of boundary conditions. Then, we derive the analytical expressions of magnet field strength and magnet flux density in the air gap of each kind of magnet array by the method of separation of variables. Finally, we compare the three types of magnet arrays on the basis of the analytical solutions. 相似文献