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991.
992.
Y. Cohen K. Landskron N. Ttreault S. Fournier‐Bidoz B. Hatton G.A. Ozin 《Advanced functional materials》2005,15(4):593-602
The synthesis and characterization of a novel silicon–silica nanocomposite material are reported. A self‐assembly method allows the encapsulation of silicon nanoclusters within the channels of a periodic mesoporous silica thin film. The result is the formation of a silicon–silica nanocomposite film with bright, room‐temperature photoluminescence in the visible range, and a nanosecond luminescence lifetime. The properties of the nanocomposite material have been studied by several analytical techniques, which collectively show the existence within the channels of non‐diamondoid‐structure‐type silicon nanoclusters with various hydrogenated silicon sites. It is estimated that the silicon nanoclusters in the silica mesoporous films occupy up to 39 % of the accessible pore volume. The nanocomposite film shows improved resistance to air oxidation compared to crystalline silicon. The high loading and chemical stability to oxidation under ambient conditions are important advantages in terms of the development of silicon‐based light‐emitting diodes from this class of materials. 相似文献
993.
994.
适用于仿真工业控制系统的软件包 总被引:2,自引:0,他引:2
本文提出的仿真软件包具有丰富的数学运算功能、控制算法功能、逻辑运算功能及图形编辑能力.软件包结构上充分体现了模块化的设计思想,而在功能及组态方法上又十分类似于分散控制系统相应的功能。使用该软件包,可方便地对各种典型的工业控制系统特别是由微处理机组成的分散控制系统进行仿真研究。 相似文献
995.
Anthony L. Andrady Carlos M. Nunez Bor‐Sen Chiou Saad A. Khan 《Polymer Engineering and Science》2002,42(11):2065-2071
The solution rheology of different generations of hyperbranched polyesters in N‐methyl‐2‐pyrrolidinone (NMP) solvent was examined in this study. The solutions exhibited Newtonian behavior over a wide range of polyester concentrations. Also, the relative viscosities of poly(amidoamine) (PAMAM) dendrimers in ethylenediamine were compared with those of the hyperbranched polyesters in NMP. Both types of dendritic polymers have relative viscosities that are exponential functions of their molar fraction in solution. The slopes of these relative viscosity curves show a linear relationship with respect to the generation number. PAMAM dendrimers have the greater slopes for each generation, reflecting their relatively larger intrinsic viscosity values. 相似文献
996.
Summary Styrene polymerization was initiated by methylaluminoxane in the presence of haloalkane. The propagating species are shown by trapping experiments and electron paramagnetic resonance to be both radicals and cations. 相似文献
997.
It is shown that a superconductor cannot be simply treated as a low-loss conductor; rather, it should be treated as a negative dielectric material (with a negative dielectric constant). This approach is good only for vanishingly small field application with frequency significantly smaller than gap frequency and temperature not too close to the critical temperature of the superconductor. The electromagnetics of negative dielectric materials are discussed in terms of causality, perturbation technique, surface impedance, time-domain interpretation of current components, and computational electrodynamics 相似文献
998.
A modification to the time-domain finite-difference method (TDFDM) that uses a variable step size is investigated. The entire computational volume is divided into a coarse grid with a large step size. A fine grid with a small step size is introduced only around discontinuities. The corresponding time increments are related to the spatial increments with the same ratio in order to minimize the numerical dispersion. The fields within the coarse and fine grids are found using the TDFDM, while an interpolation in space and time is utilized to calculate the tangential electric field on the coarse-fine grid boundary. This subgridding decreases the required computer memory and therefore expands the capability of the TDFDM. The technique is shown to be numerically stable and does not entail any extra numerical error. The method is applied to the calculation of waveguides and microstrips 相似文献
999.
Summary Cyclic tris(ethylene terephthalate) (CTET) was separated from oligomeric extract of poly(ethylene terephthalate) by the conventional solvent separation method. The structure of CTET was characterized by differential scanning calorimetry, X-ray diffraction, and scanning electron microscopy. It is shown that the double melting behavior of meltcrystallized CTET is attributed to the morphological change created by heat-treatment. The effect of the morphological change on the crystal structure of CTET was also examined. 相似文献
1000.
Auguste Commeyras Hlne Collet Laurent Boiteau Jacques Taillades Odile Vandenabeele‐Trambouze Herv Cottet Jean‐Philippe Biron Raphaël Plasson Louis Mion Olivier Lagrille Herv Martin Franck Selsis Michel Dobrijevic 《Polymer International》2002,51(7):661-665
Addressing the still open question of the prebiotic origin of sequential macromolecules (peptides, nucleic acids) on the primitive Earth, we describe a molecular engine (the primary pump), which works at ambient temperature and continuously generates, elongates and complexifies sequential peptides. This new scenario is based on a cyclic reaction sequence, whose keystep is the activation of amino acids into their N‐carboxyanhydrides (NCA) through nitrosation by NOx. This process could have taken place on tidal beaches; it requires a buffered ocean, emerged land and a nitrosating atmosphere. With the help of geochemical studies and computer simulations of atmosphere photochemistry, we show that the primitive Earth during the Hadean may have satisfied all these requirements. © 2001 Society of Chemical Industry. 相似文献