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131.
Amphiphilic segmented polymer networks (SPNs) have been prepared by free radical copolymerization of methyl methacrylate with α,ω-bisacrylate terminated poly(2-methyl-2-oxazoline) and poly(2-ethyl-2-oxazoline). DSC and DMTA analysis demonstrated the influence of the copolymer composition, the molecular weight and nature of the poly(2-alkyl-2-oxazoline)s and the polymerization conditions on the final phase morphology of the networks. A comparative phase morphology study of the polymer blends and SPNs revealed the more compatible phase morphology of the networks. The compatibility could be further increased by UV-induced network formation. The investigation of the solvent uptake in different solvents clearly demonstrated the amphiphilic nature of the SPNs. 相似文献
132.
133.
Zengzeng Yao Mei Lin Jing Zhou Haitao Wang Wei Zhong Qiangguo Du 《Polymer Engineering and Science》2007,47(11):1943-1950
Polybutylene terephthalate (PBT)/acrylonitrile–butadiene–styrene (ABS) copolymer blends compatibilized by a mixture of styrene–acrylonitrile–maleic anhydride (ASMA) copolymers and epoxy resin (EP) were prepared through melt reactive extrusion. The morphological, rheological, and mechanical properties of these blends were studied. The epoxy functional groups of EP can react with anhydride groups of ASMA and the PBT terminal groups (? OH and ? COOH) simultaneously, leading to the formation of ASMA–EP–PBT graft copolymers. Because of the effective compatibilization of these copolymers at the interface, finer dispersed phase morphologies were obtained. Compared with PBT/ABS/ASMA blends, the addition of EP induced a more stable molten phase structure, with increases of storage moduli, loss moduli, and dynamic viscosities. Results indicated that 1.5 wt% of the EP in the blends was most suited for the compatibilization. Impact properties of these blends were also investigated. POLYM. ENG. SCI., 47:1943–1950, 2007. © 2007 Society of Plastics Engineers 相似文献
134.
一次低烧SrTiO3基晶界层电容器的研究 总被引:2,自引:0,他引:2
研究了以Li2CO3为助烧结剂、Sr(Li1/4Nb3/4)O3为施主掺杂剂、Bi2O3和SiO2为晶界绝缘剂的SrTiO3基晶界层电容器的一次低温烧成技术。初步探索了Ti/Sr比值、施主掺杂剂、绝缘剂对显微结构及介电性能的影响。在1150℃烧成温度下,获得了εapp〉3.5×10^4;p〉1.0×10^11Ω·cm;tgδ〈1.0%;ΔC/C〈±5.0%(-25 ̄+85℃)的SrTiO3基晶界层 相似文献
135.
Yong?An?Jung Du?Young?Choi Seung?Bum?Hong Kyung?Ho?RowEmail author 《Korean Journal of Chemical Engineering》2003,20(4):705-708
Reversed-phase high-performance liquid chromatography was successfully developed for the simultaneous and rapid separation for the main whey proteins, α-Lactalbumin and β-Lactoglobulin. This method consisted of a linear gradient of the two mobile phases of 0.1% trifluoroacetic acid in water and 0.1% trifluoroacetic acid in acetonitrile. The total run time for this separation was approximately 30 min, and α-Lactalbumin was eluted followed byβ- Lactoglobulin. The injection volume was fixed at 20 μl and the flow rate was 1 ml 1/min. The optimum mobile phase composition and gradient conditions to separate α-Lactalbumin and β-Lactoglobulin (A+B) were experimentally obtained at the 15 μm particle with a pore size of 300 Å on the linear-gradient mode. 相似文献
136.
L. T. Guan F. G. Du G. Z. Wang Y. K. Chen M. Xiao S. J. Wang Y. Z. Meng 《Journal of Polymer Research》2007,14(3):245-251
Completely biodegradable foams of poly(propylene carbonate) (PPC) derived from carbon dioxide and propylene oxide were fabricated
using N, N′-dinitroso pentamethylene tetramine (DPT) as chemical blowing agent, and urea as the activator to lower the decomposition
temperature of DPT. Thermal decomposition behavior and gas evolution behavior of the DPT composite with various urea to DPT
ratios were investigated to optimize the composition of the blowing agent. The formulation of blowing agent mixture and foaming
condition, the foam morphologies, the molecular weight change, as well as the mechanical properties of produced PPC foams
were studied extensively. The experimental results demonstrated that the greatest blowing ratio of 14.8 can be afforded in
case 12 phr blowing agent was used at 170 °C for 30 min. Gel permeation chromatography (GPC) and thermal analysis revealed
that DPT acted as both chain-extension agent and blowing agent for PPC matrix. The molecular weight of PPC subjected to foaming
increased by 76%. The foamed PPC exhibited superior mechanical properties and can be used as packaging material for many practical
applications. 相似文献
137.
138.
Chaoite-like carbon was prepared by quenching the pyrolysate of acetylene gas at 873 K and ambient pressure. Its morphology is carbon macrotubes (CMTs) with 20–60 μm in diameter and up to 8 mm in length. Microstructure analysis revealed that sp-bonded carbon (SPBC) chains in CMTs are kinked and the crystal orientation is anisotropic along the length and circumference directions of CMTs. A SPBC belt scrolling model was proposed for explaining the formation process of CMTs. 相似文献
139.
In this paper, we propose a discriminative multi-task objects tracking method with active feature selection and drift correction. The developed method formulates object tracking in a particle filter framework as multi-Task discriminative tracking. As opposed to generative methods that handle particles separately, the proposed method learns the representation of all the particles jointly and the corresponding coefficients are similar. The tracking algorithm starts from the active feature selection scheme, which adaptively chooses suitable number of discriminative features from the tracked target and background in the dynamic environment. Based on the selected feature space, the discriminative dictionary is constructed and updated dynamically. Only a few of them are used to represent all the particles at each frame. In other words, all the particles share the same dictionary templates and their representations are obtained jointly by discriminative multi-task learning. The particle that has the highest similarity with the dictionary templates is selected as the next tracked target state. This jointly sparsity and discriminative learning can exploit the relationship between particles and improve tracking performance. To alleviate the visual drift problem encountered in object tracking, a two-stage particle filtering algorithm is proposed to complete drift correction and exploit both the ground truth information of the first frame and observations obtained online from the current frame. Experimental evaluations on challenging sequences demonstrate the effectiveness, accuracy and robustness of the proposed tracker in comparison with state-of-the-art algorithms. 相似文献
140.
For hyperspectral target detection, it is usually the case that only part of the targets pixels can be used as target signatures, so can we use them to construct the most proper background subspace for detecting all the probable targets? In this paper, a dynamic subspace detection (DSD) method which establishes a multiple detection framework is proposed. In each detection procedure, blocks of pixels are calculated by the random selection and the succeeding detection performance distribution analysis. Manifold analysis is further used to eliminate the probable anomalous pixels and purify the subspace datasets, and the remaining pixels construct the subspace for each detection procedure. The final detection results are then enhanced by the fusion of target occurrence frequencies in all the detection procedures. Experiments with both synthetic and real hyperspectral images (HSI) evaluate the validation of our proposed DSD method by using several different state-of-the-art methods as the basic detectors. With several other single detectors and multiple detection methods as comparable methods, improved receiver operating characteristic curves and better separability between targets and backgrounds by the DSD methods are illustrated. The DSD methods also perform well with the covariance-based detectors, showing their efficiency in selecting covariance information for detection. 相似文献