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81.
82.
A number of production methods have been developed for high-performance fibers; however, most processes use toxic solvents or generate a lot of unwanted by-products. Our research resulted in the development of a new family of high-performance polypropylene (PP) fibers by utilizing a simple, ecologically friendly bath (ECOB). Various commodity polymers can be used with ECOB melt spinning system at high throughputs and performance benefits. Our treated as-spun PP fibers had a highly oriented, but not crystalline precursor morphology with f a up to 0.6 generating superior mechanical properties. After drawing at draw ratios of 1.49 at 120 °C, highly oriented crystalline and amorphous phases were achieved for the drawn fibers with f c and f a values of 0.95 and 0.87, respectively. This fine structure for ECOB-treated fibers resulted in tenacity close to 12 g/d, initial modulus higher than 150 g/d, and ultimate elongation at break of 20 %. The polymer melting point of the new fibrillar PP fibers increased by 9 °C. 相似文献
83.
High‐performance filaments by melt spinning low viscosity nylon 6 using horizontal isothermal bath process
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Several techniques and treatments have been developed for the production of high‐performance nylon‐6 fibers. The inherent problems of low productivity, high production cost, and high energy consumption, complexity of chemical reaction, mass transfer, and waste recovery systems make most of them inappropriate for industrial application. Horizontal isothermal bath (hIB) is an alternative ecofriendly simple treatment that can be used during melt spinning process for production of technical textile fibers. The efficacy of hIB in improving the mechanical properties of multifilament nylon‐6 yarn is studied in this research. The results showed that such treatment can increase the molecular orientation of the amorphous and crystalline functions up to 0.54 and 0.983, respectively, and raised both the amorphous isotropy and fiber birefringence by 67 and 45%, respectively. Hot drawing of the yarn at a very low draw ratio of 1.38, increased the tenacity and modulus up to 10 and 43.9 g/den, respectively, and decreased the elongation to 27%. POLYM. ENG. SCI., 55:2457–2464, 2015. © 2015 Society of Plastics Engineers 相似文献
84.
The aim of study was to investigate the effects of various curing protocols with quartz–tungsten halogen (QTH) or light‐emitting diode (LED) light‐curing units on the degree of conversion (% DC) of two dual‐cured core buildup resin composites. Two dual‐cured core buildup resin composites, Clearfil Dc Core Automix (CLF) and Grandio Core Dc (GR), were selected. Specimens were exposed to the polymerization protocols as follows: there was immediate photoactivation or photoactivation delayed by 2 or 5 min by a QTH or LED source, and one group was allowed to chemically polymerize and served as a control (n = 6). The % DC of the specimens was determined with attenuated total reflectance–Fourier transform infrared spectroscopy. The GR samples polymerized with QTH for the 5‐min‐delayed photoactivation had higher % DC values than those self‐cured, and the Clearfil Dc Core Automix (CLF) samples with immediate or delayed curing protocols with halogen yielded higher % DC values than the samples that were chemically polymerized. The comparison of the two resin composites polymerized with halogen showed a higher % DC for CLF than for GR in the 2‐min‐delayed photoactivation. On the other hand, when they were cured with LED, the % DC values of GR significantly increased after the 2‐min‐delayed photoactivation. In light of the results, it might be stated that CLF polymerized with QTH, could be the better option. GR provided adequate chemical polymerization; therefore, it might be useful in areas in which light curing is not possible. Clinicians should consider the polymerization characteristics of dual‐cured resin composites. The use of different composites may require the modification of the application procedures recommended by the manufacturer. © 2014 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2014 , 131, 40560. 相似文献
85.
Yasemin CaglarDilek Duygu Oral Mujdat CaglarSaliha Ilican M. Allan ThomasKeyue Wu Zhaoqi SunJingbiao Cui 《Thin solid films》2012,520(21):6642-6647
Mixed (CuO)x(ZnO)1 − x composite films have been prepared on glass substrates by a sol-gel spin coating method using copper acetate hydrate and zinc acetate dihydrate as precursors. The surface morphology and crystal structure of the films were investigated by field emission scanning electron microscopy and x-ray diffraction, respectively. It was observed that the crystal structure changed from wurtzite (ZnO) to monoclinic (CuO) as the Cu content increased from 0% to 100% in the films. UV-Vis absorption and photoluminescence measurements indicated that the optical properties can be tuned continuously from pure ZnO to pure CuO as the Cu content was increased, following the expected trends for a transition from ZnO to CuO. The resistivity of the films decreased by three orders of magnitude as Cu increased from 0% to 100%. These semiconducting composite oxides with tunable optical and electrical properties have potential applications in electronics and optoelectronics. 相似文献
86.
Kanat Burak Bozdogan Duygu Ozturk Ayhan Nuhoglu 《The Structural Design of Tall and Special Buildings》2009,18(1):1-12
In this study an approximate method based on the continuum approach and transfer matrix method for static and dynamic analyses of multi‐bay coupled shear walls is presented. The whole structure is idealized as a sandwich beam in this method. Initially the differential equation of this equivalent sandwich beam is written, then shape functions for each storey can be obtained by the solution of differential equations. By using boundary conditions and storey transfer matrices which are obtained by these shape functions, system modes and periods can be calculated. Reliability of the study is shown with a few examples. A computer program has been developed in MATLAB and numerical samples have been solved for demonstration of the reliability of this method. The results of the samples display the agreement between the present method and the other methods given in the literature. Copyright © 2007 John Wiley & Sons, Ltd. 相似文献
87.
Duygu Ağaoğulları Hasan Gökçe İsmail Duman M. Lütfi Öveçoğlu 《Journal of the European Ceramic Society》2012,32(7):1457-1462
In this study, AlB2 powders were synthesized by using a combined method of mechanical alloying (MA) and annealing of elemental aluminum (Al) and boron (B) powders. Milling was performed in a planetary ball-mill (Fritsch? Pulverisette 7 Premium Line) up to 15 h under argon (Ar) atmosphere. Annealing process was carried out in a tube furnace at 650 °C for 6 h under Ar atmosphere. The effects of MA durations on the annealing process and AlB2 formation were investigated. The conversion of Al and B powders to AlB2 starts after only MA for 3 h or after MA for 1 h and subsequent annealing. A slight formation of AlB12 occurs at 242 °C for as-blended powders and it shifts to about 272 °C for MA’d powders. Al–B powder blends MA’d for 9 h and annealed have AlB2 particles in size between 35 and 75 nm in the presence of Al13Fe4, Fe3B and Fe2B contaminations. 相似文献
88.
Esin Dogantekin Akif Dogantekin Derya Avci Levent Avci 《Digital Signal Processing》2010,20(4):1248-1255
In this study, an intelligent diagnosis system for diabetes on Linear Discriminant Analysis (LDA) and Adaptive Network Based Fuzzy Inference System (ANFIS): LDA-ANFIS is presented. The structure of this LDA-ANFIS intelligent system for diagnosis of diabetes is composed by two phases: The Linear Discriminant Analysis (LDA) phase and classificiation by using ANFIS classifier phase. In first phase, Linear Discriminant Analysis (LDA) is used to separate features variables between healthy and patient (diabetes) data. In second phase, the healthy and patient (diabetes) features obtained in first phase are given to inputs of ANFIS classifier. The correct diagnosis performance of the LDA-ANFIS intelligent system is calculated by using sensitivity and specificity analysis, classification accuracy and confusion matrix respectively. The classification accuracy of this LDA-ANFIS intelligent system was obtained about 84.61%. 相似文献
89.
Summary Novel phosphorus-containing acrylate/(di)methacrylate monomers based on 3-(acryloyloxy)-2-hydroxypropyl methacrylate (AHM) were prepared by two different methods. The first method involved reaction of AHM with diethylchlorophosphate to produce a phosphate-containing acrylate/methacrylate monomer followed by Michael addition of this monomer with dihexyl amine. In the second method, a hydroxyl-containing dimethacrylate monomer was prepared via Michael addition of hydroxyl amine to AHM followed by its reaction with diethylchlorophosphate. The photopolymerization kinetics of the synthesized monomers were investigated using a differential scanning calorimeter. It was shown that changing the monomer structure allows control of polymerization reactivity and new phosphorus-containing polymers can be obtained. 相似文献
90.
Bekir Özçelik Duygu Yazıcı Ahmet Ekicibil 《Journal of Superconductivity and Novel Magnetism》2013,26(5):1599-1605
This work is related to the structural and magnetic properties of the Co(PPh3)Cl2 metal complex for different sintering times. The structural and physical properties of the complex have been studied by using SEM, EDX, and magnetization techniques. SEM results clearly demonstrate that the grains of the complex are very well connected to each other and tightly packed. Magnetization measurements with respect to magnetic field and temperature show a paramagnetic behavior above 20 K for the all samples. Furthermore, the susceptibility (χ) as a function of temperature indicates a paramagnetic-antiferromagnetic phase transition with a negative value of the Curie–Weiss temperature, θ. In addition, increasing sintering time appears to also enhance the effective magnetic moment, μ eff. 相似文献