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21.
A new image analysis technique has been developed which allows maceral analysis of coal to be carried out. The technique is able to separate the liptinite component from the background resin by using two separate images of the surface captured with different camera exposure times. At normal exposure, the liptinite has a similar grey scale value to the surrounding resin, but at a higher exposure time, the resin remains black whilst the liptinite grey scale increases significantly enough to distinguish it from the resin. The method has been tested for repeatability and reproducibility and found to be within the ISO Standard requirements. 相似文献
22.
High-performance liquid chromatography of human milk triacylglycerols and gas chromatography of component fatty acids 总被引:1,自引:0,他引:1
Human milk triacylglycerols were separated by high-performance liquid chromatography. A 5-μ Supelcosil LC-18 column (Supelco,
Inc., Bellefonte, PA) was used with acetone/acetonitrile (64∶36, vol/vol) as mobile phase. Triacylglycerols were tentatively
identified based on theoretical carbon number and relative retention time. Despite changes resulting from dietary fat variation,
the major component triacylglycerols were those composed of palmitic, oleic and linoleic acids. Triacylglycerols with palmitic,
stearic and oleic acids were present as minor components. Fatty acids were quantified by gas chromatography relative to an
internal standard. Ratios of n−6/n−3 fatty acids were found to be high than previously reported.
Based on a paper presented at the Symposium on Milk Lipids held at the AOCS Annual Meeting, Baltimore, MD, April 1990. 相似文献
23.
The original Smoking Consequences Questionnaire (SCQ; T. H. Brandon & T. B. Baker, 1991) measured college students' outcome expectancies for cigarette smoking. A version (SCQ-Adult) was needed for assessing expectancies in more typical, older, nicotine-dependent smokers. Two separate versions of the SCQ were developed and compared. Tests of construct validity provided greater support for the version comprising probability items over the version comprising subjective expected utility items. As expected, principal components analyses revealed a greater number of factors than the original SCQ suggesting that expectancies become more specific with smoking experience. All scales showed good reliability. Over the course of smoking cessation treatment, expectancies became less positive, especially for abstaining participants. Other validity tests also tended to be consistent with research on alcohol expectancies and with contemporary models of drug outcome expectancies. (PsycINFO Database Record (c) 2011 APA, all rights reserved) 相似文献
24.
W. J. Reilly J. B. Schwartz E. S. Gahli Christopher T. Rhodes 《Drug development and industrial pharmacy》1994,20(8):1511-1515
Spherical dosage forms have been reported to be an efficient and effective method for delivering drugs into the body and controlling their dissolution rate. Substantial work has been conducted in these laboratories illustrating the advantages of microcrystalline cellulose-based spheres for these purposes. Through various methodologies, but most routinely the extrusion and marumerization technique, it has been determined by Funck, et al. that not more than 50% drug can be incorporated into a sphere formulation without the addition of other binders.
Because of the nature of the extrusion and marumerization manufacturing process, the type of drug being processed and the resultant particle size requirements of the spheres, the percent of spheres falling outside the desired particle size can range from between 3% and 20%. For this reason and the possibility of operator errors, our objective was to determine the parameters which needed monitoring when reprocessing was necessary. 相似文献
Because of the nature of the extrusion and marumerization manufacturing process, the type of drug being processed and the resultant particle size requirements of the spheres, the percent of spheres falling outside the desired particle size can range from between 3% and 20%. For this reason and the possibility of operator errors, our objective was to determine the parameters which needed monitoring when reprocessing was necessary. 相似文献
25.
Button Cathryn M.; Grant Malcolm J.; Hannah T. Edward; Ross Abraham S. 《Canadian Metallurgical Quarterly》1993,25(2):230
Two studies identified and labeled the dimensions that people use to judge others' attitudes. In the 1st study, 50 male and 50 female undergraduates viewed pairs of attitude statements drawn from 1 or 2 large sets. For each pair of statements, Ss judged whether or not a person who agreed with one statement in the pair would be likely to agree with the other. The dimensions of liberalism and traditional values were found to underlie perceived attitudes. Validity was confirmed in a 2nd study with 60 male and 60 female undergraduates who rated the characteristics of hypothetical people who agreed strongly with particular statements. Results suggest that there is a common structure to people's perceptions of others' attitudes. (French abstract) (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
26.
Qiwen Wang Xiaoyun Sun Bruce L. Golden Lenore Desilets Edward A. wasil Scott Luco Adam Peck 《Computers & Operations Research》1993,20(8)
A crucial step in manufacturing microcircuits is the wire bonding process in which a very thin gold wire must be formed to connect two surfaces in the microcircuit. The quality of the wire bond can be measured by visual inspection and a pull test—both of which are high-reliability, high-cost approaches to statistical process control. Westinghouse wanted to develop a high-reliability, low-cost quality assurance system. In this paper, we report on a year-long study to construct a neural network model that is capable of predicting the quality of wire bonds. The results of our modeling efforts reveal that neural networks are useful tools for statistical process control problems. 相似文献
27.
Roger Norman Rothon Christopher Mark Liauw Graham Clayton Lees Wayne Christopher Edward Schofield 《The Journal of Adhesion》2002,78(7):603-628
The interaction of ammonium stearate (AS) and γ-aminopropyltriethoxysilane (APS) treatments with a magnesium hydroxide flame retardant filler and their effects on its use in an ethylene vinyl acetate copolymer compound have been investigated. The work has shown clear evidence of changes in the structure of the surface layers formed on the filler as the amount of additive is increased and the levels at which these occur can be correlated with theoretical monolayer quantities. Infrared (IR) spectroscopy data suggest that the stearate coating changes from a half salt to a full salt as the coating level is increased and that the APS coating on the filler initially has a significant bicarbonate content, presumably due to reaction with atmospheric carbon dioxide. The effect of coating level on the melt flow rate, insoluble matrix content, crystallisation behaviour, tensile properties, limiting oxygen index, and ageing of the filled compound has been studied. Distinct trends have been observed, many of which can be correlated with the structure of the filler surface layers. Of particular importance is the observation that, unlike APS, excess stearate appears to promote detrimental ageing effects. 相似文献
28.
Jue Donald; Meador Kimford J.; Zamrini Edward Y.; Allen Martha E.; Feldman Daniel S.; Loring David W. 《Canadian Metallurgical Quarterly》1992,6(4):331
Studied memory for visuospatial arrays in 28 male and 34 female healthy dextral adults (aged 20–90 yrs). 10 abstract figures were presented in each hemispace over a series of learning trials, and then delayed free recall of figure placement was obtained. Figures were misplaced significantly downward and leftward in both hemispaces. Both vertical and horizontal absolute error increased significanty with age, but no age effects on directional errors were observed. The increase in absolute error over age is consistent with decreased anterograde memory and visuospatial skills in the elderly. The directional errors are believed to result from an attentional shift toward proximal peripersonal space, in combination with attentional shifts from differential left vs right cerebral activation. Gender effects were also observed. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
29.
Laura Akers Herbert H Severson Judy A Andrews Edward Lichtenstein 《Nicotine & tobacco research》2007,9(9):907-914
This study assessed the cost-effectiveness of two low-intensity programs for quitting smokeless tobacco, based on results of a randomized trial with 1,069 volunteer participants. Cost data were collected for two levels of intervention: manual only (a self-help manual) and assisted self-help (the manual plus a videotape and two supportive phone calls from tobacco cessation counselors). Incremental cost-effectiveness ratios were calculated for assisted self-help vs. quitting on one's own, using the manual-only quit rate and data from another study as alternative proxies for no intervention. A threshold analysis was conducted to determine the spontaneous quit rate at which the manual-only intervention becomes more cost-effective than assisted self-help. The cost to provide and receive the assisted self-help intervention averaged US $56 per participant vs. $20 for the manual-only intervention (societal perspective, Year 2000 dollars). Estimates for incremental cost per quit for the assisted self-help intervention ranged from $922 to $1,758, depending on the proxy used for no intervention. The manual-only intervention was more cost-effective than assisted self-help if quitting among motivated chewers who do not receive treatment does not exceed 3.4%. Support from a wife or partner added little cost to a quit attempt for male chewers ($3-$4). Providing a manual, video, and brief phone counseling to smokeless tobacco users who want to quit is a reasonable use of health care resources. The self-help quitting guide also may be a cost-effective treatment, but it remains to be demonstrated whether it is more effective than quitting on one's own. 相似文献
30.
Self-help cessation programs for smokeless tobacco users: long-term follow-up of a randomized trial.
Hebert H Severson Judy A Andrews Edward Lichtenstein Brian G Danaher Laura Akers 《Nicotine & tobacco research》2007,9(2):281-289
This paper presents long-term outcomes of the largest clinical trial of smokeless tobacco (SLT) cessation reported to date. SLT users in five northwestern states were recruited to call a toll-free number, and 1,069 users were randomized to one of two self-help conditions: either a manual-only condition or an assisted self-help condition, which included the manual, a targeted video, and two support phone calls. Significant between-group differences were not found for either the 12- or 18-month point-prevalence measure of abstinence from either SLT only or all tobacco products using outcomes based on either the responder or intention-to-treat outcomes. However, using a repeated point-prevalence measure across all three assessment points, we found that significantly more assisted self-help participants reported abstinence, compared with manual-only participants. Compared with manual-only participants, those in the assisted self-help condition were significantly more likely to use recommended cessation techniques. Results demonstrate that low-cost, minimal interventions delivered by mail and phone can help a sizable proportion of individuals quit using SLT. 相似文献