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51.
Polycrystalline Ag treated with O2 at pressures up to 1 bar and at temperatures up to 920 K was examined by TDS. It was found that the peak commonly observed at 595±25 K and assigned to adsorbed atomic oxygen (Oa) is shifted to higher desorption temperatures with rising dosing temperatures. Since saturation of the uptake was not possible either, this peak was identified as dissolved atomic oxygen (Od). The existence of a maximum for the O2 uptake after exposure at 820 K was found. Hence, under conditions of formaldehyde synthesis ( 920 K) the ability of the catalyst to dissolve oxygen is near its maximum. 相似文献
52.
A non-steady boundary layer model is developed for numerical simulation of combustion and gasification of a single shrinking char particle. The model considers mass and energy conservation coupled with heterogeneous char reactions producing CO and homogeneous oxidation of CO to CO2 in the boundary layer surrounding the char particle. Mass conservation includes accumulation, molecular diffusion, Stefan flow and generation by chemical reaction. Energy conservation includes radiation transfer at the particle surface and heat accumulation within the particle. Simulation results predict experimentally measured conversion and temperature profiles of a burning Spherocarb particle in a laminar flow reactor. Effects of bulk oxygen concentration and particle size on the combustion process are addressed. Predicted particle temperature is significantly affected by boundary layer combustion of CO to CO2. With increasing particle size, char gasification to char combustion ratio increases, resulting in decreasing particle temperature and increasing peak boundary layer temperature. 相似文献
53.
Marie-Laure Favier Pierre-Etienne Bost Christine Guittard Christian Demigné Christian Rémésy 《Lipids》1997,32(9):953-959
The effects of partially hydrolyzed, nonviscous, guar gum (PHGG) on cholesterol metabolism and digestive balance have been
compared with those of native guar gum (GUAR) in rats adapted to 0.4% cholesterol diets. Both types of guar gum elicited acidic
fermentations in the large intestine, but only GUAR effectively lowered plasma cholesterol (P<0.001), chiefly in the triglyceride-rich lipoprotein fraction. The biliary bile acid excretion was significantly enhanced
in rats fed GUAR (P<0.05), as well as the intestinal and cecal bile acid pool (P<0.001). In rats fed GUAR and to a lesser extent in those fed PHGG, the fecal excretion of bile acids and neutral sterol was
higher than in controls (P<0.01). The digestive balance (cholesterol intake-steroid excretion) was positive in control rats (+47 μmol/d), whereas it
was negative in rats fed GUAR (−20 μmol/d), which could involve a higher rate of endogenous cholesterol synthesis. In rats
fed PHGG, the steroid balance remained slightly positive. Liver 3-hydroxy-3-methylglutaryl-CoA (HMG-CoA) reductase activity
was very low (22 pmol/min/mg protein), owing to cholesterol supplementation, in control rats or in rats fed PHGG, whereas
it was markedly higher (+463%) in rats fed GUAR. In conclusion, even if PHGG does alter some parameters of the enterohepatic
cycle of cholesterol and bile acids, its effects are not sufficient to elicit a significant cholesterol-lowering effect. The
intestinal (ileal or cecal) reabsorption of bile acids was not reduced, but rather increased, by GUAR; nevertheless the intestinal
capacities of reabsorption were overwhelmed by the enlargement of the digestive pool of bile acids. In the present model,
induction of HMG-CoA reductase probably takes place in the presence of elevated portal bile acid concentrations. 相似文献
54.
A mathematical model to describe the protonation of weak acid ion-exchange resins with various acids has been developed. The charge profiles calculated using the theory are demonstrated by photographs. Interdiffusion coefficients in the resin phase have been determined and it is shown how they depend on the system parameters and on the properties of the resin. 相似文献
55.
Under the applied high reaction temperatures (900 K) the Ag surface is restructured and a tightly held oxygen species is formed on the surface (O) apart from O atoms dissolved in the bulk (O). Methanol oxidation to formaldehyde proceeds through this O species as demonstrated by application of a variety of spectroscopic techniques. 相似文献
56.
The rotational mobility of stable nitroxide radicals in PS, PMMA, PVC, PP and PE has been studied over a wide temperature range by the e.s.r. method. At temperatures T lower than Tg, spin probes act as kinetically independent particles, the rotational frequency of which is deter mined mainly by the micropore dimensions of the polymer and depends indirectly on the mobility of segments or side groups. 相似文献
57.
Summary Solid state 23Na- and 13C-NMR spectra of alkali cellulose are presented as a function of NaOH-concentration of the steeping lye, steeping temperature and amount of adhering lye (press factor). Results are discussed with regard to chemical binding of NaOH to the cellulose chain in the system cellulose/ NaOH/H2O.Presented at the 22nd Microsymposium, Characterization of Structure and Dynamics of Macromolecular Systems by NMR Methods, Prague, CSSR, July 20–23,1981 相似文献
58.
Parsing details like author names and titles out of bibliographic references of scientific publications is an important issue that has received considerable attention recently. However, most existing techniques are tailored to the highly standardized reference styles used in the last two to three decades. They do not perform well with the wide variety of reference styles used in older, historic publications. Thus, they are of limited use when creating comprehensive bibliographies covering both historic and contemporary scientific publications. This paper presents a generic approach to bibliographic reference parsing, named RefParse, which is independent of any specific reference style. Its core feature is an inference mechanism that exploits the regularities inherent in any list of references to deduce its format. In addition, our approach learns names of authors, journals, and publishers to increase the accuracy in scenarios where human users double check parsing results to increase data quality. Our evaluation shows that our approach performs comparably to existing ones with contemporary reference lists and also works well with older ones. 相似文献
59.
CMC samples obtained by gel filtration on a preparative scale were used to calibrate an agarose column. The relation between molecular weight and the peak elution volume for monodisperse samples were calculated as well as the relation between band broadening and the peak elution volume. In the calculations of the molecular weight distribution curves of the studied CMC samples, consideration was given to the variable band broadening by proper transformations of the experimental data, thus making it possible to obtain numerical solutions free from oscillations. The method admits a rapid determination of the molecular weight distribution of cellulose and related materials. 相似文献
60.
正一年前,东风标致3008正式上市,时隔一年后东风标致第二款小型SUV车型2008在4月17日正式上市。简单翻阅了一下车主论坛上对这款新车的态度,让人惊讶的是居然都是一片叫好的声音。对于标致的车个人一直不太感冒,而它在国内销售情况也并不太乐观,相信包括笔者在内的很多人对于以前标致老款的车型,都很难对其萌生喜爱的感觉。不合时宜的外观设计也许正是阻碍标致国内销售的元凶之一。我们看到的情况,标致又怎么会不了解,或许是为了突破这种尴尬情况,从3008开始 相似文献