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81.
介绍用原子吸收分光光度法测定PE、PP氯含量。该方法采用氧气燃烧法处理样品,用Ag~+沉淀Cl~-,经分离后用原子吸收光谱测溶液中剩余Ag~+浓度,从而得到样品中氯含量。讨论了仪器参数、操作条件对测定结果的影响,结果表明,在分离前存放4~30分钟对测试结果无影响。火焰法的测定条件为波长328.1nm、灯电流7.5mA、狭缝宽度0.4nm、C_2H_2压力0.025MPa、空气压0.16MPa、燃烧器高度7.5mm。实验采用的离心转速2000r/min、时间5分钟、HNO_3浓度1%。该法灵敏度可达0.1μg/ml、相对标准误差<2%。 相似文献
82.
83.
Jun Rong Li Jun Wang Jia Rui Xu Ming Qiu Zhang Min Zhi Rong Qiang Zheng 《Composites Science and Technology》2006,66(16):3126-3131
The authors of this paper synthesized a series of amphiphilic triblock copolymers of polystyrene-b-poly(ethylene glycol)-b-polystyrene (PS-PEG-PS) having different PEG/PS ratios with nearly identical molecular weights of the entire copolymers. The interfacial interactions in the composites consisting of carbon black and the copolymers can thus be tailored. When these conducting composites are exposed to certain solvent vapors, their electrical resistances greatly increase, showing the gas sensitivity. The present work indicated that this switching behavior is controlled by the structural relaxation of the composites because matrix swelling acts as the main mechanism. The response time has been correlated with absolute temperature by Arrhenius equation, and the estimated activation energy reflects mobility of the fillers involved in the solvent induced expansion of the surrounding polymer. Therefore, by using the gas sensibility of the conductive composites, the structure evolution of the composite materials in solid state and the effect of filler/matrix interfacial interaction on the relaxation property of the matrix polymer has been inspected. It was found that lower activation energy represents stronger interfacial interaction in case good solvent of the matrix was used for the test. 相似文献
84.
用两亲聚合物制备大颗粒苯丙乳液 总被引:10,自引:0,他引:10
分别以两亲聚合物P(C9-AA)和P(DCPD-St-α-St-AA)作乳化荆,研究了制备大颗粒(约1μm)及具有一定稳定性的苯丙乳液的方法,讨论了乳化剂,温度及引发剂用量对乳液性能的影响。结果表明,以P(C9-AA)作乳化剂时,引发剂用量为单体质量的1.2%,90℃时可以合成性能良好的苯丙乳液;以P(DCPD-St-α-St-AA)作乳化荆时,引发剂用量为单体质量的1.2%,80℃时可以合成性能良好的苯丙乳液。 相似文献
85.
86.
SDI接口数字监视设备的设计与实现 总被引:2,自引:0,他引:2
介绍了一种对SDV(串行数字视频)信号进行解码的设备设计方案,提出了该系统的总体构架,并对该系统的硬件设计、软件设计进行了全面的论述。设计的产品具有较高的性能价格比,已进入了推广阶段。 相似文献
87.
The IEEE 802.11e medium access control (MAC) layer protocol is an emerging standard to support quality of service (QoS) in
802.11 wireless networks. Some recent work shows that the 802.11e hybrid coordination function (HCF) can improve significantly
the QoS support in 802.11 networks. A simple HCF referenced scheduler has been proposed in the 802.11e which takes into account
the QoS requirements of flows and allocates time to stations on the basis of the mean sending rate. As we show in this paper,
this HCF referenced scheduling algorithm is only efficient and works well for flows with strict constant bit rate (CBR) characteristics.
However, a lot of real-time applications, such as videoconferencing, have some variations in their packet sizes, sending rates
or even have variable bit rate (VBR) characteristics. In this paper we propose FHCF, a simple and efficient scheduling algorithm
for 802.11e that aims to be fair for both CBR and VBR flows. FHCF uses queue length estimations to tune its time allocation
to mobile stations. We present analytical model evaluations and a set of simulations results, and provide performance comparisons
with the 802.11e HCF referenced scheduler. Our performance study indicates that FHCF provides good fairness while supporting
bandwidth and delay requirements for a large range of network loads.
Pierre Ansel received a multidisciplinary in-depth scientific training in different fields such as Pure and Applied Mathematics, Physics,
Mechanics, Computer Science and Economics from the Ecole Polytechnique, Palaiseau, France. Then, he joined the Ecole Nationale
Superieure des Telecommunications, Paris, France in 2005 where he went further into electronics, databases, computer network
security and high speed networks. He received a multidisciplinary master of sciences degree and an additional master of sciences
degree in telecommunications in 2005. He did a summer internship in 2003 in INRIA, Sophia Antipolis, France where he worked
on the Quality of Service in 802.11 networks at Planete Group, France. Then in 2004, he joined France Telecom R&D, Issy-les-Moulineaux,
France to work on Intranet Security issues. He designed a WiFi security supervision architecture based on WiFi Intrusion Detection
Sensors. He is currently a French civil servant and belongs to the French Telecommunications Corps.
Qiang Ni received the B.Eng., M.Sc. and Ph.D. degrees from Hua Zhong University of Science and Technology (HUST), Wuhan City, China
in 1993, 1996 and 1999 respectively. He is currently a faculty member in the Electronic and Computer Engineering Division,School
of Engineering and Design, Brunel University, West London, U.K. Between 2004 and 2005 he was a Senior Researcher at the Hamilton
Institute, National University of Ireland, Maynooth. From 1999 to 2001, he was a post-doctoral research fellow in the multimedia
and wireless communication laboratory, HUST, China. He visited and conducted research at the wireless and networking group
of Microsoft Research Asia Lab during the year of 2000. From Sept. 2001 until may 2004, he was a research staff member at
the Planète group of INRIA Sophia Antipolis France. Since 2002, he has been active as a voting member at the IEEE 802.11 wireless
LAN standard working group. His current research interests include communication protocol design and performance analysis
for wireless networks, cross-layer optimizations, vertical handover and mobility management in mobile wireless networks, and
adaptive multimedia transmission over hybrid wired/wireless networks. He has authored /co-authored over 40 international journal/conference
papers, book chapters, and standard drafts in this field. He is a member of IEEE. E-mail: Qiang.Ni@ieee.org
Thierry Turletti received the M.S. (1990) and the Ph.D. (1995) degrees in computer science both from the University of Nice – Sophia Antipolis,
France. He has done his PhD studies in the RODEO group at INRIA Sophia Antipolis. During the year 1995–96, he was a postdoctoral
fellow in the Telemedia, Networks and Systems group at LCS, MIT. He is currently a research scientist at the Planete group
at INRIA Sophia Antipolis. His research interests include multimedia applications, congestion control and wireless networking.
Dr. Turletti currently serves on the Editorial Board of Wireless Communications and Mobile Computing. 相似文献
88.
89.
The intelligent controlling and data process of pitch error measurement is proposed. The whole system takes C++ as the development tool and takes advantages of object-oriented and visualization, having the advantages of easy operation and humanistic interface. In the meanwhile, the system can be complemented and improved according to the demand of user, having certain independence. The research of the system provides an efficient and reliable way to measure and analyze the gear pitch, which can be referenced in the future research. 相似文献
90.
绿色理念的内涵拓展与绿色图书馆建设 总被引:1,自引:0,他引:1
绿色图书馆是图书馆学的一个新的研究方向和发展趋势.文章首先深刻挖掘绿色内涵的本质,阐述正确理解绿色图书馆的含义,接着探讨了绿色图书馆建设的要素取向,从而明确了现阶段发展绿色图书馆的必要性. 相似文献