CSAa黏弹性表面活性剂压裂液的研制

用化学试荆长链烷基季铵盐CSAa制备了两种VES压裂液并研究了相关性能，其组成（CSAa／水杨酸钠／氯化钾／正丁醇，以g／dL为单位）如下：1．0／0．3／1．0／0．2；2．0／0．6／0．5／0．1。在耐温性测定中，1．0g／dL CSAa压裂液的黏度由30℃时的75．0mPa·s降至50℃时的37．5mPa·s；2．0g／dL CSAa压裂液的黏度由40℃时的225mPa·s逐渐降至55℃时的110mPa·s，再降至60℃时的65．0mPa·s.在1701／s剪切2h后，剪切温度为42℃时1．0g／dL CSAa压裂液的黏度下降26％，剪切温度为53℃时2．0g／dL CSAa压裂液黏度下降9％。陶粒沉降速度测定结果表明，40℃、42℃时的1．0g／dL CSAa压裂液（黏度分别为60和54mPa·s）和50℃、53℃时的2．0g／dLCSAa压裂液（黏度分别为180和145mPa·s）携砂性能良好，而45℃、50℃时的1．0g／dLCSAa压裂液和55℃、60℃时的2．0g／dL CSAa压裂液，携砂性能则较差或很差。认为VES压裂液的携砂性能来源于棒状胶束网络，并不全由压裂液黏度决定。还考察了VES压裂液的破胶性能。图1表2参5。     

A segmentation-based fine-grained peer sharing technique for delivering large media files in content distribution networks

Delivering large media files over the Internet is a challenging task because it has some unique features that are different from delivering conventional Web documents. In this paper, we propose a fine-grained peer sharing technique for dealing with the problem in the context of content distribution networks. The key difference of the technique from conventional peer-to-peer systems is that the unit of peer sharing is not a complete media file, but at a finer granularity. By doing so, we improve the flexibility of replica servers for handling client requests. We analyze the storage requirement at replica servers and design a scheduling algorithm to coordinate the delivery process from multiple replica servers to a client. Our simulations show that the fine-grained peer sharing approach can reduce the initial latency of clients and the rejection rate of the system significantly over a simple peer sharing method.     

Y-Ba-Cu-O超导涂层的研制

用等离子喷涂工艺制备了 Y-Ba-Cu-O 高临界温度超导涂层,涂层的初始转变温度为101K、零电阻温度为86K。电阻率与磁化率的测量结果表明这种超导涂层具有与烧结超导块体相类似的性能,X 光衍射谱显示出涂层主要由 YBa_2Cu_3O_(?)单相化合物组成。     

基于GPRS网络传输的雨水情遥测传输系统设计

远程雨水情遥测是现代化水利工程系统中一个重要环节,特别是在山洪地质灾害预警系统中,能准确及时掌握雨水情数据,为预警预报、合理决策、指挥调度提供了可靠的依据。文章介绍了一种利用GPRS网络传输,以PIC16C74单片机为核心的雨水情遥测设备,并给出了相关的硬件接口电路连接以及软件实现方法。     

55t/h锅炉技术改造成功经验

介绍了35t／h锅炉扩容改造为55t／h非标锅炉的技术成功经验。从增加锅炉的容积、受热面面积、燃烧器喷嘴改造三个方面介绍了对锅炉本体的改造，改造后实现了锅炉的水位、汽温及燃烧自动调节，提高了锅炉的热效率为以后的锅炉扩容改造提供了实践经验。     

Formation of mushroom-like ZnO microcrystals through a solution calcination process

Mushroom-like ZnO microcrystals have been prepared via a solution calcination route, using Zn(NO₃)₂ as Zn source in the absence of any surfactants, templates or catalysts. This is the first example to prepare mushroom-like crystals as semiconductors, which are expected to show particular physical properties. The ZnO products were investigated by X-ray powder diffraction (XRD), scanning electron microscopy (SEM), Raman spectroscopy and photoluminescence (PL) spectrum measurements. A suitable concentration of Zn(NO₃)₂ solution was important for the growth of the mushroom-like products. The reported synthetic procedure is straightforward and inexpensive, and thus can be readily adopted to produce large quantities of mushroom-like ZnO microcrystals.     

Shape-control of nano-ZnO by changing the solvent

ZnO sub-micrometer sized disk using ethanol/water mixed solution as solvent is synthesized by solvent-thermal process without any additive, while ZnO nanorods are obtained when water is used as solvent. This formation of disk is discussed based on the reaction of Zn-terminated ZnO (0001) plane with ethanol molecule, which results in the passivation of ZnO (0001) planes and lowering the free surface energy of ZnO (0001).     

中碱值硫化烷基水杨酸钙的制备及性能研究

介绍了一种碱值达170mgKOH／g以上、硫含量大于3．0％、钙含量大于6．0％的硫化烷基水杨酸钙盐润滑油添加剂的制备过程及其性能。实验中重点考察了促进剂及硫磺加入量对产品碱值及硫含量的影响；通过冷冻蚀刻电镜法观察了含碳酸盐的胶体粒子结构及粒度分布情况；应用凸轮挺校、四球试验机等考察了硫化烷基水杨酸钙盐产品的极压抗磨性能。结果表明，硫化烷基水杨酸钙产品不但具有良好的高温洁净性、抗氧化安定性、胶体稳定性，而且具有突出的极压抗磨性及热稳定性。