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排序方式: 共有651条查询结果,搜索用时 15 毫秒
91.
92.
Bernard W. Ikua Hisataka Tanaka Fumio Obata Satoshi Sakamoto Takeyasu Kishi Tatsuo Ishii 《Precision Engineering》2002,26(1):821
This paper presents the results of a series of experiments performed to examine the validity of a theoretical model for evaluation of cutting forces and machining error in ball end milling of curved surfaces. The experiments are carried out at various cutting conditions, for both contouring and ramping of convex and concave surfaces. A high precision machining center is used in the cutting tests. In contouring, the machining error is measured with an electric micrometer, while in ramping it is measured on a 3-coordinate measuring machine. The results show that in contouring, the cutting force component that influences the machining error decreases with an increase in milling position angle, while in ramping, the two force components that influence the machining error are hardly affected by the milling position angle. Moreover, in contouring, high machining accuracy is achieved in “Up cross-feed, Up cut” and “Down cross-feed, Down cut” modes, while in ramping, high machining accuracy is achieved in “Left cross-feed, Downward cut” and “Right cross-feed, Upward cut” modes. The theoretical and experimental results show reasonably good agreement. 相似文献
93.
94.
The pervaporation behaviors of methanol–water by poly(γ-methyl L -glutamate) (PMLG) membrane at non-steady- and steady-state permeation were investigated. The values of t1/2 (time required to reach a half value of steady-state permeation flux) for methanol and water changed and did not change with the component in feed, respectively. Both of the average diffusion coefficients for methanol–and water–PMLG from the mixture changed exponentially with the sorption amount of methanol by the synergetic effect on diffusion. The difference in behavior of non-steady and steady state diffusion was explained by whether Do (diffusion coefficient at zero penetrant concentration) was influenced by the concentration distribution of penetrant in PMLG membrane. 相似文献
95.
Ichikuni Nobuyuki Sato Fumio Shimazu Shogo Uematsu Takayoshi 《Topics in Catalysis》2002,18(1-2):101-104
SiO2-supported NbC catalysts were prepared by using temperature-programmed reactions (TPR). XAFS analysis confirmed that Nb2O5 was reduced to NbO2 in the first TPR stage and converted into NbC in the second TPR stage. Nb particles grew only in the second TPR stage. Formation of highly dispersed NbC particles on SiO2 surfaces was achieved. 相似文献
96.
Radiation-vulcanization of natural rubber latex (NRL) with n-butyl acrylate gives a higher tensile strength for films obtained after casting. The ageing properties of radiation-vulcanized natural rubber in the presence of various antioxidants have been investigated. In order to find out suitable antioxidants for radiation-vulcanized natural rubber latex (RVNRL) films, extraction of the gel fraction was carried out in xylene with 1 wt.-% antioxidant and air bubbling. Antioxidants which give less reduction in gel fraction due to oxidative degradation during extraction are effective for ageing tests of RVNRL films. It was found that tris(nonylated phenyl) phosphite (Nonflex TNP) and 2,5-di-tert-amylhydroquinone (Antage DAH), among 12 different antioxidants tested, were the most effective antioxidants for RVNRL films. 相似文献
97.
Yelim Song Fumio Kawamura Takashi Taniguchi Kiyoshi Shimamura Naoki Ohashi 《Journal of the American Ceramic Society》2018,101(11):4876-4879
In this study, we investigated the Al–Sn flux system and its growth conditions to obtain AlN single crystals. AlN single crystals of a size of 50 μm were successfully grown using an Al–Sn melt under nitrogen gas pressure. The growable region of the AlN crystals was established using a pressure‐temperature diagram. The required nitrogen gas pressure for the growth of the AlN crystals was found to decrease with increasing temperature, and AlN was grown at 0.1 MPa nitrogen pressure above 1300°C. By investigating the AlN yield with various Al concentrations, we confirmed that the Al component in the Al–Sn melt facilitated nitrogen dissolution. Finally, scanning electron microscopy analysis showed that the obtained AlN particles showed good morphology. 相似文献
98.
A reagent for the determination of phosphorus in sea water which contains Mo(VI) plus Mo(V) may be easily prepared by the reduction of Mo(VI) with metallic zinc in acid medium. This reagent is stable in the air for several months, and the development of the molybdenum blue colour is complete in 20 min at about 100°C; the colour is stable for at least a few months. The salt error is approximately 5 per cent with sea water of chlorinity 19 per milli. The interference due to either arsenate or silicate at their concentrations in sea water is negligible. 相似文献
99.
Henares TG Takaishi M Yoshida N Terabe S Mizutani F Sekizawa R Hisamoto H 《Analytical chemistry》2007,79(3):908-915
A general and simple implementation of simultaneous multiparametric sensing in a single microchip is presented by using a capillary-assembled microchip (CAs-CHIP) integrated with the plural different reagent-release capillaries (RRCs), acting as various biochemical sensors. A novel "drop-and-sip" technique of fluid handling is performed with a microliter droplet of a model sample solution containing proteases (trypsin, chymotrypsin, thrombin, elastase) and divalent cations (Ca2+, Zn2+, Mg2+) that passes through the microchannel with the aid of a micropipette as a vacuum pump, concurrently filling each RRC via capillary force. To avert the evaporation of the nanoliter sample volume in each capillary, PDMS oil is dropped on the outlet hole of the CAs-CHIP exploiting the capillary force that results in spontaneous sealing of all the RRCs. In addition, this high-speed sample introduction alleviates the possibility of protein adsorption and capillary cross-contamination, allowing a reliable and multianalyte determination of a sample containing many different proteases and divalent cations by using the fluorescence image analysis. Presented results suggested the possible application of this microchip in the field of drug discovery and systems biology. 相似文献
100.
Radiation crosslinking of carboxymethylcellulose (CMC) with a degree of substitution (DS) from 0.7 to 2.2 was the subject of the current investigation. CMC was irradiated in solid‐state and aqueous solutions at various irradiation doses. The DS and the concentration of the aqueous solution had a remarkable affect on the crosslinking of CMC. Irradiation of CMC, even with a high DS, 2.2 in solid state, and a low DS, 0.7 in 10% aqueous solution, resulted in degradation. However, it was found that irradiation of CMC with a relatively high DS, 1.32, led to crosslinking in a 5% aqueous solution, and 20% CMC gave the highest gel fraction. CMC with a DS of 2.2 induced higher crosslinking than that with a DS of 1.32 at lower doses with the same concentration. Hence, it was apparent that a high DS and a high concentration in an aqueous solution were favorable for high crosslinking of CMC. It is assumed that high radiation crosslinking of CMC was induced by the increased mobility of its molecules in water and by the formation of CMC radicals from the abstraction of H atoms from macromolecules in the intermediate products of water radiolysis. A preliminary biodegradation study confirmed that crosslinked CMC hydrogel can be digested by a cellulase enzyme. © 2000 John Wiley & Sons, Inc. J Appl Polym Sci 78: 278–283, 2000 相似文献