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51.
Phase-transfer catalysis (PTC) has been widely used for the synthesis of organic compounds for more than three decades. The scope and mechanistic features of PTC have been the aim of numerous studies. This review focuses on the application of phase transfer catalysis in synthesis of phosphorus compounds. 相似文献
52.
Gheorghe Juncu 《International Journal of Heat and Mass Transfer》2008,51(3-4):920-928
Numerical methods are used to investigate the transient heat transfer from an elliptic cylinder to a steady stream of viscous, incompressible fluid. The temperature of the cylinder is considered spatially uniform but not constant in time. The momentum and heat balance equations were solved numerically in elliptic coordinate system. The solutions span the parameter ranges 5 ? Re ? 40, 1 ? Pr ? 100 and axis ratio ε, 0.1 ? ε ? 0.75. The computations were focused on the influence of the axis ratio and volume heat capacity ratio on the heat transfer rate. 相似文献
53.
Effect of short carbon fibers and MWCNTs on microwave absorbing properties of polyester composites containing nickel-coated carbon fibers 总被引:1,自引:0,他引:1
Igor Maria De Rosa Adrian Dinescu Fabrizio Sarasini Maria Sabrina Sarto Alessio Tamburrano 《Composites Science and Technology》2010
Multiphase composite materials filled with multiwall carbon nanotubes (MWCNTs), short nickel-coated carbon fibers and millimeter-long carbon fibers with various weight fractions and compositions are developed and used for the design of wide-band thin radar-absorbing screens. The effective complex permittivity of several composite samples is measured in the frequency range from 8 GHz to 18 GHz. The obtained results show that the addition of the MWCNTs into the mixture allows tuning the EM properties of the composite filled with the short nickel-coated fibers. Numerical simulations are also performed in order to design new radar-absorbing shields. Single-layer and bi-layer thin dielectric Salisbury screens are designed to exhibit minimum reflection coefficient at 10 GHz and at 15 GHz, and maximum bandwidth at −10 dB. It results that the total thickness of the screen can be reduced below 2 mm by using a lossy sheet made with the composite filled with MWCNTs and nickel-coated carbon fibers, whereas the bandwidth at −10 dB can exceed 6 GHz in a bi-layer structure. 相似文献
54.
Alina C Ion Ion Ion Alina Culetu Dragos Gherase Carmen A. Moldovan Rodica Iosub Adrian Dinescu 《Materials science & engineering. C, Materials for biological applications》2010,30(6):817-821
A sensitive biosensor for chloropyrifos (CPF), an organophosphorus pesticide, was developed by immobilizing acetylcholinesterase (AChE) through covalent bonding to an oxidized exfoliated graphite nanoplatelet (xGnPs)–chitosan cross-linked composite. Because of the increased surface area and the conductive properties of the nanomaterial, AChE developed a high affinity for acetylthiocholine (ATCI) and formed thiocholine with a fast response. The response of the sensor was a linear function of ATCI concentration in two segments, one from 0.005 to 0.039 mM and the second from 0.064 mM to 0.258 mM. The corresponding equation for the first range was ip(A) = 2.26 × 10? 5c + 4.39 × 10? 7 (R2 = 0.992) and the equation for the second was ip(A) = 6.80 × 10? 6c + 1.30 × 10? 6 (R2 = 1.000), with a detection limit of 1.58 × 10? 10 M. The fabrication of the sensor was simple, the response was fast and the stability acceptable. This sensor has many potential applications, the foremost being in organophosphorus pesticides. 相似文献
55.
Petre Badica Dan Batalu Mihail Burdusel Mihai A. Grigoroscuta Gheorghe V. Aldica Monica Enculescu Raluca A. Gabor Zhiyong Wang Ruoxuan Huang Peifeng Li 《Ceramics International》2018,44(9):10181-10191
Pristine and (SiC+Te)-added MgB2 powders, green and spark plasma sintered (SPS) compacts were investigated from the viewpoint of quasi-static and dynamic (Split-Hopkinson Pressure Bar, SHPB) compressive mechanical properties The amount of the additive (SiC+Te) was selected to be the optimum one for maximization of the superconducting functional parameters. Pristine and added MgB2 show very similar compressive parameters (tan δ, fracture strength, Vickers hardness, others) and fragment size in the SHPB test. However, for the bulk SPSed samples the ratio of intergranular to transgranular fracturing changes, the first one being stronger in the added sample. This is reflected in the quasi-static KIC that is higher for the added sample. Despite this result, sintered samples are brittle and have roughly similar fragmentation behavior as for brittle engineering ceramics. In the fragmentation process, the composite nature of our samples should be considered with a special focus on MgB2 blocks (colonies) that show the major contribution to fracturing. The Glenn-Chudnovsky model of fracturing under dynamic load provides the closest values to our experimental fragment size data. 相似文献
56.
G. Stanciu L. Gheorghe F. Voicu S. Hau C. Gheorghe G. Croitoru M. Enculescu R.P. Yavetskiy 《Ceramics International》2019,45(3):3217-3222
(Y0.87-xLa0.1Zr0.03Ybx)2O3 (x?=?0.02, 0.04, 0.05) transparent ceramics were obtained by solid-state reaction and combined sintering procedures with La2O3 and ZrO2 as sintering additives. A method based on two-step intermediate sintering in air followed by vacuum sintering was applied in order to control the densification and grain growth of the samples during the final sintering process. The results indicate that La2O3 and ZrO2 co-additives can improve the microstructure and optical properties of Yb:Y2O3 ceramics at relatively low sintering temperature. On the other hand, the addition of Zr4+ ions leads to the formation of dispersed scattering volumes in the ceramic bodies. Transmittance of 78.8% was measured for the 2.0?at% Yb:Y2O3 ceramic sample at the wavelength of 1100?nm. The spectroscopic properties of Yb:Y2O3 ceramics were investigated at room temperature. The obtained results show that the absorption cross-section at 978?nm is in the range of 2.08?×?10–20 to 2.36?×?10–20 cm2, whereas the emission cross-section at 1032?nm is ~1.0?×?10–20 cm2. 相似文献
57.
58.
Andrei Victor Sandu Alexandra Ciomaga Gheorghe Nemtoi Costica Bejinariu Ion Sandu 《Microscopy research and technique》2012,75(12):1711-1716
This article presents the SEM‐EDX and microFTIR study and the corrosion behavior of new five types of phosphated coatings obtained by coprecipitation in acid aqueous medium of some metal cations, pursuing the influence of the addition of other cations and a moderator of precipitation, on the uniformity and compactness of the layers and on the morphology of dendritic structure of Zn(II) and Fe(II) phosphates. Microsc. Res. Tech. 2012. © 2012 Wiley Periodicals, Inc. 相似文献
59.
This paper presents a new method in order to appreciate the roughness of elliptical or spherical small bodies by using ultrasound. This thing is possible by knowing about 2-4 acoustic resonance frequencies. The maximum diameter and medium roughness of the bodies are evaluated. Small bodies such as tumors can be detected, when other medical devices like ultrasound or tomography computerized cannot evaluate the surface shape because of limited spatial resolution. The method is intended to be used in oncological medicine for early non-invasive diagnostic for cancer, because tumor tissue has outer surface more or less rough, depending on whether or not it is malignant. 相似文献
60.
Gheorghe Juncu 《International Journal of Heat and Mass Transfer》2011,54(1-3):669-677
Numerical methods are used to investigate the transient mass transfer from a binary gas bubble to an incompressible liquid. The bubble has two components: A – soluble and B – insoluble in the surrounding fluid. The concentration of A inside the bubble is considered spatially uniform but not constant in time. The maximum value of the initial volumetric fraction of A is 0.3. The mathematical model equations were solved numerically in spherical coordinates system. Creeping flow, moderate Re number flow, 10 ? Re ? 100, and potential flow around the bubble were assumed. The computations focused on the influence of the initial fraction of A and Henry number on the mass transfer rate for Pe ? 104. 相似文献