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21.
22.
M. Del C. Ruiz J. A. González J. B. Rivarola 《Metallurgical and Materials Transactions B》2004,35(3):439-448
The mechanism and kinetics of β-Ta2O5 chlorination, mixed with sucrose carbon, have been studied by a thermogravimetric technique. The investigated temperature
range was 500 °C to 850 °C. The reactants and reaction residues were analyzed by scanning electronic microscopy (SEM), X-ray
diffraction (XRD), and Brunauer-Emmett-Teller method for surface area (BET). The effect of various experimental parameters
was studied, such as carbon percentage, temperature, chlorine partial pressure, and flow, use of the multiple sample method,
and carbon previous oxidation. The carbon percentage and previous treatment have an effect on the system reactivity. The temperature
has a marked effect on the reaction rate. In the 500 °C to 600 °C temperature interval, the apparent activation energy is
144 kJ/mol of oxide, while at higher temperatures, the activation energy decreases. With high chorine partial pressures, the
order of reaction is near zero. The kinetic contractile plate model, X=kt, considering carbon oxidation as the controlling stage, is the one with the best fit to the experimental data. A probable
mechanism for the carbochlorination of β-Ta2O5 is proposed: (1) activation of chlorine on the carbon surface, (2) chlorination of Ta2O5, (3) oxidation of carbon, and (4) recrystallization of β-Ta2O5. 相似文献
23.
This paper proposes a low complexity joint space-time multiuser detection algorithm for asynchronous DS/CDMA antenna array systems. The proposed multiuser detector is composed of an adaptive antenna array, used as a linear beamformer, and a sliding window decorrelator. A QPSK modulation scheme is used in order to increase bandwidth efficiency. Numerical results are given in terms of Bit Error Rate (BER) under the assumption of a frequency-selective Rayleigh slow fading channel. In particular, the proposed receiver is shown to be near-far resistant, even in worst fading cases, and to exploit completely array introduction while maintaining acceptable computational complexity. The proposed architecture avoids linear filter realization of the decorrelator, which is impractical in the case of a large number of users, and operates with relatively short data frames instead of the complete information sequence. Finally, this receiver is very flexible to changes in timing configuration. 相似文献
24.
Fellers Gloria; McInnis Charles; Cappelli Mario; Cragg Susan; Vaillancourt Raymond 《Canadian Metallurgical Quarterly》1987,19(1):108
The WAIS-R Information subtest was combined with 21 potential substitute Canadian content items and group-administered to 119 high school students ranging in age from 16 to 19 years. Seven acceptable substitute items were identified. Mean scores on the American items for the 16-17 and 18-19 age groups suggested that Canadians of these ages are not penalized by American content with respect to either Verbal or Full Scale IQ. Nevertheless, the research identified eight Information items, four easier and four more difficult than the standard WAIS-R implies. Similar results were noted in two previous studies of the WAIS-R, and indicate the extreme caution required for the clinical interpretation of intra test scatter. There is also evidence that item difficulty within the Information subtest may vary with the age of the subject. These results were considered indicative of the necessity for Canadian content Information items and the development of Canadian norms for an adapted WAIS-R Information subtest. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
25.
Birnessites containing Na, K or Li in the interlayer have been prepared by oxidation of Mn(II) cations with H2O2 in a basic medium with different alkaline cation/Mn molar ratios. The solids prepared have been characterised by elemental chemical analysis, powder X-ray diffraction, thermal analyses (differential thermal analysis and thermogravimetric analysis), FT-IR spectroscopy and surface texture assessment by adsorption of N2 at –196°C. Crystalline birnessites are obtained for A/Mn ratios (A = K, Li) larger than 3.4, but MnO(OH) has been also identificed when such a ratio is smaller than 3.4. Ion exchange is topotactic, but is not complete for exchanging Na, K, or Mg for pre-existing Li. The solids are stable up to 400°C, and formation of spinels and solids with tunnel structures is observed at this temperature. Li-containing birnessites are transformed to LiMn2O4 spinel at 400°C, and co-crystallization of bixbyte (Mn2O3) is observed at higher temperatures. Bixbyte and cryptomelane are formed at 500°C for the K-containing birnessites. 相似文献
26.
27.
Reviews the book, Basic Processes in Reading Visual Word Recognition by Derek Besner and Glyn W. Humphreys (see record 1990-99017-000). While there has been an increase in the amount of work on many different aspects of reading, as Besner and Humphreys point out in the overview to their book, the vast majority of the research on the topic of reading in the past twenty years has been concerned with the processes involved in word recognition. For this reason, Besner and Humphreys have attempted to bring together studies on topics which are both relevant to current debates in the field of word recognition, and which are likely to be important for future developments in the field. They have compiled an edited volume consisting of their overview and eight additional chapters. The editors have attempted to span the continuum of processes involved in word recognition and thus have included chapters which cover topics ranging from the visual analysis of words, to those on the influence of semantic factors on word recognition. The authors of these chapters comprise an impressive list of researchers in the field of word recognition, with the majority of chapters being authored by leading researchers on the topic. Given the stature of the authors and the range of topics covered, in theory this volume should provide a very thorough overview of current theory and research on reading. There is no question that each of the chapters is interesting and important in its own right. However, in practice the volume as a whole fell somewhat short of my expectations. The different tacts taken by different authors has resulted in a very uneven coverage of the current debates in the field. Notwithstanding these criticisms, I am sure that the majority of researchers in this field will consider this volume to be an important contribution. The book would provide a very useful addition to graduate courses in cognitive sciences and as a supplemental text for an undergraduate course on the psychology of reading. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
28.
Whole cell voltage- and current-clamp recordings were obtained from mesencephalic trigeminal sensory (Mes 5) neurons identified visually in thin brain stem slices of neonatal rats with the use of infrared video microscopy. These cells exhibited accommodation in spike discharge responses to depolarizing current injection protocols whose duration differed as a function of holding potential (-50 vs. -65 mV). Several spikes were elicited before the membrane response accommodated from -50 mV, whereas from -65 mV only single action potentials were evoked. In response to similar protocols, application of the K+ channel blocker 4-aminopyridine (4-AP) (50 microM to 2 mM) caused sustained repetitive spiking whereas tetraethylammonium (TEA) (10-30 mM) did not cause repetitive spiking. In voltage clamp, 4-AP application (100 microM) revealed a sustained outward current (I4-AP) that was active between -60 and -30 mV. I4-AP was responsible for suppressing sustained repetitive spiking behavior, producing accommodation under normal circumstances. TEA application in voltage clamp revealed a sustained outward current evoked positive to -40 mV. Two transient outward currents (TOCs) were identified by prepulse protocols typically used to characterize A-type currents: a 4-AP-insensitive fast TOC, and a slow TOC (ITOC-S) sensitive to 4-AP (> 500 microM). A Ca(2+)-dependent outward current that activated positive to -30 mV was also characterized. A mathematical model of a Mes 5 neuron was assembled from our voltage-clamp records to simulate the dynamic interaction of outward currents during membrane excitation. We conclude that in Mes 5 neurons, the 4-AP-sensitive currents ITOC-S and I4-AP determine the duration of spike trains. In particular, the noninactivating I4-AP determines whether cells exhibit sustained repetitive discharge or accommodate in response to depolarizing current. Neurotransmitter modulation of this current or modulation of the resting membrane potential could modify the output properties of Mes 5 neurons, and therefore the properties of these currents must be incorporated into our current understanding of how these cells contribute to shaping oral-motor pattern generation. 相似文献
29.
To make exploring a locale's heritage a challenging and compelling experience, the Venice Game uses a handheld platform and educational software that leverages video game techniques. 相似文献
30.
Antonio J. Pérez-López José Manuel López-Nicolás Angel A. Carbonell-Barrachina 《European Food Research and Technology》2007,225(2):255-260
Consumers demand organic products because they believe that the organic products are more flavorful and respectful to the
environment and human health. The effects of organic farming on the minerals contents and aroma composition of Clemenules
mandarin juices were studied. Minerals (Fe, Cu, Mn, Zn, Ca, Mg, K, and Na) were quantified using atomic absorption-emission
spectroscopy, while volatile compounds were extracted using the dynamic headspace technique and were identified and quantified
by GC–MS. In general, organic farming produced a mandarin juice with a higher quality than that produced by conventional agricultural
practices. Higher concentrations of both minerals and positive volatile compounds were found in the organic juice, while the
formation of off-flavors was higher in the conventional juice, although threshold values were not reached. 相似文献