微球TiO2光催化剂的制备

采用溶胶凝胶-喷雾干燥法制备微球TiO2,其粒径为0．5～3μm,平均沉淀速度为5mm／s,为晶体粒径为8．3nm的锐钛型纳米TiO2的聚合体,比表面积较大。具有与纳米TiO2相似的催化活性,较好地解决了催化剂活性和分离之间的矛盾。     

非均相复合驱油体系驱替特征研究

针对聚合物驱后油藏缺乏有效提高采收率接替技术的问题,研发了新型非均相聚合物驱油剂PPG产品。通过长岩芯驱替实验考察了PPG产品的运移能力;利用微观物理模型对比了聚合物驱后油藏条件下二元驱与PPG驱的驱油效果。结果表明,聚合物驱后再用PPG驱波及能力最强,聚合物驱后再用二元驱的洗油效率高。将两种体系叠加,配制PPG与聚合物及表面活性剂形成的非均相复合驱油体系,在聚合物驱后再用非均相复合驱油体系驱可进一步提高采收率达10％以上。     

Synthesis and Tribological Behaviour of 1,3,4-Thiadiazole Schiff Base Derivatives as Multifunctional Lubricant Additives

Six new 1,3,4-thiadiazole Schiff base derivatives were synthesized and characterized by IR spectroscopy and ~1H NMR spectrometry, and their anti-corrosion properties and thermal stability were investigated via thermogravimetric analysis(TGA) and copper strip corrosion test. The tribological behavior of the said Schiff base derivatives was evaluated on an Optimol SRV~?4 oscillating reciprocating friction and wear tester. The worn surfaces of the steel discs were investigated using a scanning electron microscope(SEM) and energy dispersive X-ray spectrometer(EDS). The test results indicated that these thiadiazole Schiff base derivatives possessed favourable thermal stability, corrosion inhibiting ability and the capability of improving the tribological characteristic of the base oil effectively. It is assumed that the adsorbed additives probably reacted with the steel surfaces during the friction process, resulting in the formation of a protective film composed of sulphates, sulphides and organic nitrogen compounds.     

稠油降粘剂复配及降粘效果研究

研究了温度、单一降粘剂和复配降粘剂体系对河南某油田稠油的降粘效果,结果表明,稠油粘度随着温度上升而下降,当温度高于60℃时,粘度随温度升高下降缓慢并逐渐趋于稳定。等量等温试验条件下选取的5种降粘剂中AES的降粘效果最好,确定的降粘剂复配体系最佳复配条件为：AES用量0．2％,温度80℃,OP-10用量0．2％,十二烷基磺酸钠用量0．4％,此时降粘率达到97．50％以上。     

关于上海市闵行区新农村生活污水处理试点工程的技术探讨

随着上海城市水环境污染治理力度的不断加大,市郊农村生活污水的处理将是改善水环境质量重要环节之一,为研究适合农村生活污水处理的方法.对农村生活污水的排放特征和处理技术进行了探索,建立了"土壤渗滤+地表湿地"处理结合的组合技术,并进行了示范工程研究,水质监测结果表明"土壤渗滤+地表湿地"相结合的生活污水处理技术具有除磷脱氮效率较高,投资和运行费用低,维护管理方便等特点.同时农村污水处理工程必须根据当地排放特征和生态环境,提高污水处理效率.     

三峡船闸下游引航道防渗工程施工质量监理

华东勘测设计研究院监理中心在三峡工程通航建筑物下游引航道防渗工程施工阶段狠抓质量监理。监理工程师在开工申请，试验，工序控制，质量缺陷处理和竣工验收等方面严格起来，总结了一套理工程师在现场管理模式。     

Hierarchical Magnetic Network Constructed by CoFe Nanoparticles Suspended Within “Tubes on Rods” Matrix Toward Enhanced Microwave Absorption

Hierarchical magnetic-dielectric composites are promising functional materials with prospective applications in microwave absorption(MA)field.Herein,a three-dimension hierarchical“nanotubes on microrods,”core–shell magnetic metal–carbon composite is rationally constructed for the first time via a fast metal–organic frameworksbased ligand exchange strategy followed by a carbonization treatment with melamine.Abundant magnetic CoFe nanoparticles are embedded within one-dimensional graphitized carbon/carbon nanotubes supported on micro-scale Mo2N rod(Mo2N@CoFe@C/CNT),constructing a special multi-dimension hierarchical MA material.Ligand exchange reaction is found to determine the formation of hierarchical magnetic-dielectric composite,which is assembled by dielectric Mo2N as core and spatially dispersed CoFe nanoparticles within C/CNTs as shell.Mo2N@CoFe@C/CNT composites exhibit superior MA performance with maximum reflection loss of−53.5 dB at 2 mm thickness and show a broad effective absorption bandwidth of 5.0 GHz.The Mo2N@CoFe@C/CNT composites hold the following advantages:(1)hierarchical core–shell structure offers plentiful of heterojunction interfaces and triggers interfacial polarization,(2)unique electronic migration/hop paths in the graphitized C/CNTs and Mo2N rod facilitate conductive loss,(3)highly dispersed magnetic CoFe nanoparticles within“tubes on rods”matrix build multi-scale magnetic coupling network and reinforce magnetic response capability,confirmed by the off-axis electron holography.     

Solvent‐Assisted Low‐Temperature Crystallization of SnO2 Electron‐Transfer Layer for High‐Efficiency Planar Perovskite Solar Cells

A high‐quality polycrystalline SnO₂ electron‐transfer layer is synthesized through an in situ, low‐temperature, and unique butanol–water solvent‐assisted process. By choosing a mixture of butanol and water as a solvent, the crystallinity is enhanced and the crystallization temperature is lowered to 130 °C, making the process fully compatible with flexible plastic substrates. The best solar cells fabricated using these layers achieve an efficiency of 20.52% (average 19.02%) which is among the best in the class of planar n–i–p‐type perovskite (MAPbI₃) solar cells. The strongly reduced crystallization temperature of the materials allows their use on a flexible substrate, with a resulting device efficiency of 18%.     

Untraceable Analysis of Scalable RFID Security Protocols

Wireless Personal Communications - In order to support robust implementation of IoT, many schemes have been done to provide privacy, anonymity, scalability and customizability. Ray et al.’s...     

基于无线数据业务智能优化系统算法的研究与应用

针对业界GPRS/EDGE无线数据优化方法、算法不完善,工作效率低的问题,广西联通通过长期研究建立了一套优化经验方法和较适合现网的参数配置、算法,并将这套方法、算法应用到自主开发的无线数据业务智能优化系统中,使系统实现自动采集分析数据、自动提供优化方案、自动执行优化方案、自动生成优化报告功能,使无线数据业务优化工作朝着智能化方向迈进。