ADC Multi-Site Test Based on a Pre-test with Digital Input Stimulus

This paper describes two novel algorithms based on the time-modulo reconstruction method intended for detection of the parametric faults in analogue-to-digital converters (ADC). In both algorithms, a pulse signal, in its slightly adapted form to allow sufficient time for converter settling, is taken as the test stimulus relieving the burden placed on the accuracy requirement of the excitation source. Instead of calculating the accurate conventional dynamic and static parameters, a signature result is obtained through the analysis of the output data in the time domain. The basic concept of the algorithms is the evaluation on the performance of ADCs by the comparison of the similarity of the output waveforms. The multi-site test is expensive for traditional specification-based tests of ADCs, as high quality analogue data generators are required. Based on these two algorithms, this paper proposes a solution for this problem. The objective of the test scheme is not to completely replace traditional specification-based tests, but to provide a reliable method for early identification of excessive parameter variations in production test that allows quickly discarding of most of the faulty circuits before performing a conventional test. The efficiency of the methods is validated on an industrial 12-bit pipelined ADC both in simulations and in measurements.     

Design of an active-passive device for human ankle movement during functional magnetic resonance imaging analysis

Functional magnetic resonance imaging analysis has made major strides in recent years, both because of the development of new scanners and owing to magnetic resonance compatible systems that make it possible to stimulate parts of the human body during analysis. The significant gains in our knowledge of the brain that can thus be achieved justify efforts to construct machines with control circuits suitable for this purpose. This paper presents a magnetic resonance compatible mechatronic device with electropneumatic control that can be used to move one or both feet during functional magnetic resonance imaging analysis of the cerebral motor zones. The system is innovative and original. The results obtained at the end of the investigation were good, and demonstrated that the design is feasible.     

Preceramic polymer‐derived SiOC fibers by electrospinning

Silicon oxycarbide (SiOC) fibers with different chemical compositions were successfully fabricated by electrospinning a mixture of polyvinylpyrrolidone (PVP) and commercially available polymethylsilsesquioxane (MK) or polymethylphenylsilsesquioxane (H44) preceramic polymers, followed by cross‐linking and pyrolysis at 1000°C in Argon. The influence of the processing procedure (solvent selection, cross‐linking catalyst and additives) on the morphology of the produced fibers was investigated. For the MK/isopropanol system, the introduction of 20 vol% N,N‐dimethylformamide (DMF) enabled to decrease the diameter of the as‐spun fibers from 2.72 ± 0.12 μm to 1.65 ± 0.09 μm. For the H44/DMF systems, beads‐free fibers were obtained by adding 50 vol% choloroform. After pyrolysis, the resultant SiOC fibers derived from MK and H44 resins possessed uniform morphology, with an average diameter of 0.97 ± 0.07 μm and 1.07 ± 0.08 μm, respectively. Due to their different chemical compositions, the MK‐derived and H44‐derived SiOC ceramic fibers could find different potential applications. © 2013 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2014 , 131, 39836.     

Chloroplastic glycolipids fuel aldehyde biosynthesis in the marine diatom Thalassiosira rotula

Enzymatic preparations and specialized analytical tools have shown that chloroplast-derived glycolipids are the main substrates for the biosynthetic pathway that produces antiproliferative polyunsaturated aldehydes in broken cells of the marine diatom Thalassiosira rotula. This process, which is associated with the formation of free fatty acids and lyso compounds from polar lipids but not triglycerides, is largely dependent on glycolipid hydrolytic activity, rather than phospholipase A(2) as previously suggested. Preliminary characterization of lipolytic enzymes has revealed protein bands of 40-45 kDa. Under native conditions these proteins seem to be associated with soluble aggregates that have an apparent molecular weight of approximately 200 kDa. The biochemical process, which is similar to that described in the algal-bloom forming diatom Skeletonema costatum, suggests a mechanism based on decompartmentalization and mixing of preexisting enzymes and substrates.     

Morphological patterns of angiogenesis in ovarian follicle capillary networks. A scanning electron microscopy study of corrosion cast

To describe the morphological characteristics of the ovarian follicle (F) capillary neoformation and regression, the angiogenic figures were studied by means of scanning electron microscopy of corrosion casts in developing and mature F of rabbit, pig, and cow. Developing F showed gradual neoformation of thecal capillaries characterized by budding and then sprouting, likely from preexisting interstitial vessels. Postcapillary venules frequently showed vasoconstriction rings (sphincters). Vasodilation followed capillary elongation. Mature F, in addition to vessel elongation and dilation, also presented infolding of dilated capillary walls, followed by capillary duplication and sinusoidalization. Periovulatory F mainly showed functional changes, such as capillary dilation, signs of iperpermeabilization, and ischemia, the latter being limited to the apical follicular area. Vessel regression was characterized by thinning of capillaries and presence of avascular areas within the atretic F wall at any stage. This study showed two main types of angiogenic patterns. (a) longitudinal elongation (in series, sprouting angiogenesis) characterizing the initial phase of F development and (b) parallel duplication (in parallel, infolding or intussusceptive angiogenesis), ending in capillary lateral replication or splitting, secondary to functional microvascular changes. Indirect evidence of the establishment of postcapillary resistances contributing to capillary remodeling, was also shown. It is concluded that the sequence of capillary neoformation in mammalian ovarian F occurs in six steps: (1) budding, (2) sprouting (and elongation), (3) dilation, (4) infolding (intussusception), (5) duplication (splitting and elongation), and (6) sinusoidalization. Capillary regression hits F at any stage and characterizes F atresia.     

Quantitative comparison of energy-filtering transmission electron microscopy and atom probe tomography

Whereas transmission electron microscopy (TEM) is a well established method for the analysis of thin film structures down to the sub-nanometer scale, atom probe tomography (APT) is less known in the microscopy community. In the present work, local chemical analysis of sputtered Fe/Cr multilayer structures was performed with energy-filtering transmission electron microscopy (EFTEM) and APT. The single-layer thickness was varied from 1 to 6 nm in order to quantify spatial resolution and chemical sensitivity. While both the methods are able to resolve the layer structure, even at 2 nm thickness, it is demonstrated that the spatial resolution of the APT is about a factor of two, higher in comparison with the unprocessed EFTEM data. By calculating the influence of the instrumental parameters on EFTEM images of model structures, remaining interface roughness is indicated to be the most important factor that limits the practical resolution of analytical TEM.     

德国的屋面工程行业

本刊约请万德费尔特先生撰文简单介绍了德国屋面工程协会的性质、职能及其主要任务;重点介绍了德国的屋面铺设和屋面防水这两方面的专业工艺、技术规定及培训体制在欧洲屋面工程领域的领先地位;同时介绍了目前欧洲经济局势对德国屋面工程行业的影响以及屋面工程行业采取的应对措施。