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21.
We implement a filterless illumination scheme on a hyperspectral fluorescence microscope to achieve full-range spectral imaging. The microscope employs polarisation filtering, spatial filtering and spectral unmixing filtering to replace the role of traditional filters. Quantitative comparisons between full-spectrum and filter-based microscopy are provided in the context of signal dynamic range and accuracy of measured fluorophores' emission spectra. To show potential applications, a five-colour cell immunofluorescence imaging experiment is theoretically simulated. Simulation results indicate that the use of proposed full-spectrum imaging technique may result in three times improvement in signal dynamic range compared to that can be achieved in the filter-based imaging. 相似文献
22.
A. Manera U. Rohde H.-M. Prasser T.H.J.J. van der Hagen 《Nuclear Engineering and Design》2005,235(14):1517-1535
This paper reports on the modeling and simulation of flashing-induced instabilities in natural-circulation systems, with special emphasis on natural-circulation boiling water reactors (BWRs). For the modeling the 4-equation two-phase model FLOCAL [Rohde, U., 1986. Ein teoretisches Modell fur Zweiphasen-stromungen in wassergekulthen Kernreaktoren und seine Anwendung zur Analyse des Naturumlaufs im Heizreaktor AST-500. Ph.D. dissertation, Akademie der Wissenschaften der DDR, Dresden], developed at the Forschungszentrum Rossendorf (FZR, Germany), has been used. The model allows for the liquid and vapor to be in thermal non-equilibrium and, via drift-flux models, to have different velocities.The phenomenology of the instability has been studied and the dominating physical effects have been determined. The results of the simulations have been compared qualitatively and quantitatively with experiments [Manera, A., van der Hagen, T.H.J.J., 2003. Stability of natural-circulation-cooled boiling water reactor during start up: experimental results. Nuc. Technol., 143] that have been carried out within the framework of a European project (NACUSP) on the CIRCUS facility. The facility, built at the Delft University of Technology in The Netherlands, is a water/steam 1:1 height-scaled loop of a typical natural-circulation-cooled BWR. 相似文献
23.
Hagen Renner 《Journal of Modern Optics》2013,60(5):907-915
Abstract Simple general formulae for the coupling coefficients of the fundamental modes on well-separated parallel optical waveguides are derived. The calculation merely requires accurate knowledge of the propagation constants and core fields of the modes on the individual waveguides, while the far-from-core fields need not be known. Results for coupled circular fibres are identical with the asymptotic expansions of previously derived exact coupling coefficients. Analytical expressions for the coupling coefficients between the fundamental modes on identical weakly guiding channel waveguides are obtained. 相似文献
24.
Susan Walter Thomas Herzog Henning Heuer Hagen Bartzsch Daniel Gloess 《Microsystem Technologies》2012,18(7-8):1193-1199
We investigated the potential of the aluminum nitride films to excite ultrasonic waves at frequencies >50?MHz. The deposition process of the aluminum nitride thin film layers on silicon substrates was investigated and optimized regarding their piezoelectric behavior. Large single element transducers were deposited on silicon substrates with aluminum electrodes, under different parameters for the magnetron sputter process, like pressure and bias voltage. Special test setup and a measuring station were created to characterize the sensors. Acoustical measurements were carried out in pulse echo mode up to 500?MHz and the values of piezoelectric charge constant (d33) were determined. As a result, two parameter sets were found for the sputtering process to obtain an excellent piezoelectric charge constant of about 7.2?pC/N maximum. Then the sputtering process with these parameters was used to deposit sensors on various substrate materials and with different electrode sizes. 相似文献
25.
Carlos E.M. Guarido Deborah V. Cesar Mariana M.V.M. Souza Martin Schmal 《Catalysis Today》2009,142(3-4):252
Ethanol reforming and partial oxidation were studied on Cu/Nb2O5 and Ni/Al2O3 catalysts. Compared to the Ni/Al2O3 catalyst, the Cu/Nb2O5 catalyst presents conversion as high as Ni/Al2O3 catalyst, however, for the same level of formation of hydrogen it occurs at much lower temperature on the Cu/Nb2O5 catalyst, 200 °C lower than for the Ni/Al2O3 catalyst, with remarkable little formation of CO, which can be attributed to the strong interaction between copper and niobia. Temperature-programmed desorption (TPD-ethanol) and surface reactions (TPSR) of partial oxidation of ethanol showed formation of ethylene, acetaldehyde, ethane and mainly H2 and CO2 besides little methane. DRIFTS results are in accordance with TPD analysis and the formation of acetate species at room temperature suggests reactivity of the surface and its oxidative dehydrogenation capacity. The adsorption of ethanol gives rise to ethoxide species, which form acetate and acetaldehyde that can be oxidized to CO2 via carbonate. A comparison with reported results for Cu/Al2O3 this catalyst is promising, yielding high level of H2 with little CO production during reforming and partial oxidation reaction. The maximum H2 formation for the partial oxidation of ethanol was 41% at ratio (O2/Et) 0.8, increasing to 50% at ratio 1.5. The H2/CO is around 10 for the partial oxidation and 7 for steam reforming, which is excellent, compared to the Ni/Al2O3 catalyst with a factor 4–8 lower. 相似文献
26.
27.
Lukas Durdina Max B. Trueblood Elizabeth A. Black Steven Achterberg Donald E. Hagen 《Aerosol science and technology》2016,50(9):906-918
Soot is a climate forcer and a dangerous air pollutant that has been increasingly regulated. In aviation, regulatory measurements of soot mass concentration in the exhaust of aircraft turbine engines are to be based on measurements of black carbon (BC) calibrated to elemental carbon (EC) content of diffusion flame soot. The calibration soot must currently meet only one criterion: minimum EC to total carbon (TC) ratio of 0.8. However, not including soot properties other than the EC/TC ratio may potentially lead to discrepancies between different BC measurements. We studied the response of two instruments, the AVL Micro-Soot Sensor (MSS) and the Artium Laser-Induced Incandescence 300 (LII), to soot from two miniature combustion aerosol standard (mini-CAST) burners. By changing the air-fuel ratio, premixing nitrogen into the fuel, and using a catalytic stripper to remove volatile compounds, we produced a wide range of particle morphologies and EC contents. As the EC content decreased, both the instruments underreported the EC mass, but the LII diverged more severely. Upon closer investigation of eight conditions with EC/TC > 0.8, the LII underreporting was found independent of primary particle size, but increased with decreasing geometric mean diameter of the soot agglomerates. As the geometric mean diameter decreased from 160 nm to 50 nm, the differences between the LII and MSS increased from 15% to 50%. The results suggest that in addition to EC content, calibration procedures for the regulatory BC measurements may need to take particle size distributions into account.
© 2016 American Association for Aerosol Research 相似文献
28.
Synthesis of 6-(4-pyridinyI)-substituted Pyrido[2,3-d]pyrimidines and 1,8-Naphthyridinms A series of new 6-(4-pyridinyl)-substituted pyrido-[2,3-d]pyrimidines 2 – 4 and 1,8-naphthyridines 6 , respectively, is described. Cyclisation of 2-amino-5-(4-pyridinyl)-pyridinm-3-carboxamide 1a with diethyl oxalate gives the pyrido-[2,3-d]pyrimidinm 2a . Alkylation of( 2a ) yields the 3-ethylaminoxyrido[2,3-d]pyrimidine derivative 2b . Saponification of 2a , b gives the corresponding carboxylic acids 3a , b , which are decarboxylated by heating above the melting point to give 4a , b . The 2-amino-5-(4-pyridinyl)-pyridinm carboxylic acid derivatives 1 b – e react with ethylmalonylchloridm and diethyl malonate to afford the 1,8-naphthyridines 6b – e . The 1-oxide 7 in a similar reaction gives 8 and the oxdiazole( 9 ) which is converted by ring transformation to the 1,8-naphthyridine 10 . 相似文献
29.
30.
H. Sun D. Wiesenborn P. Rayas-Duarte A. Mohamed K. Hagen 《Journal of the American Oil Chemists' Society》1995,72(12):1551-1555
Amaranth seed (Amaranthus hypochondriacus cv. K432) was processed to obtain oil, reported to be a promising source of squalene. The amaranth seed was ground using
a stone mill, then separated into oil-rich embryonic tissue (or “bran”) and starchy perisperm. Amaranth bran was much more
stable than rice bran when free fatty acid (FFA) content and peroxide value were monitored. Milling at a gap of 0.755 mm did
not result in excessive damage to the starch in the perisperm fraction and yielded a bran fraction that contained more than
three-fourths of the oil and a starchy fraction consisting of more than two-thirds of the seed weight. The bran particles
were too fine for effective bench-scale extraction of the oil. Consequently the bran was extruded into collects prior to extraction.
Two extrusion settings were evaluated regarding the rate of moisture injection, while the bran feed rates were constant. There
was no significant difference in appearance or size between the two dried collets. Collets were extracted with hexane using
an Armfield Extraction/Desolventizing Unit (Model FT 29, Armfield, Ltd., Hampshire, England). Oil recovery averaged 97.7 and
80.0%, respectively. Oil was extracted at high yield from the bran when the bran was extruded into collets. Oil can be obtained
as a coproduct of amaranth starch by milling and separating the fractions of amaranth seed. Milling, extrusion, and extraction
did not decrease significantly the squalene content in amaranth oil, but increased FFA content and peroxide value and changed
tocopherol content of the oil. 相似文献