固载杂多酸催化剂气相催化合成乙酸丁酯的研究

在气固相反应体系中研究了酸处理膨润士固载的具有 Keggin结构的四种杂多酸在乙酸丁酯合成中的催化性能。实验结果表明 :同一载体负载不同杂多酸催化活性相似 ;不同载体负载的同一种杂多酸的催化活性与催化剂的表面酸性呈顺变关系。同时考察了反应温度 ,空速 ,酸 /醇比对催化活性的影响。在酸 /醇比为 1 ,温度为 1 2 0℃ ,空速为 3～ 5h- 1时 ,正丁醇和乙酸有较高的转化率 ,选择性接近 1 0 0 %。     

Sun工作站上的一种可视编程工具

本文主要介绍Ｓｕｎ Ｏｐｅｎｗｉｎｄｏｗｓ Ｄｅｖｅｌｏｐｅｒ’ｓ Ｇｕｉｄｅ３．０．１软件的简单使用和主要特点。     

准分子激光心血管治疗机的研究

研制了一台准分子激光心血管治疗机（ＸｅＣｌ３０８ｎｍ），单脉冲能量：８０－２００ｍＪ，平均功率５Ｗ，重复频率：手动单次，１－１００Ｈｚ，单次充气工作寿命：＞１０６脉冲数，脉冲－脉冲的能量不稳定度３％，激光脉宽１５０ｎｓ，光斑发散角（半角）：１．８×０．６ｍｒａｄ，光纤耦合输出＞２０ｍＪ。     

膛阻与小口径弹道炮弹道特性变化的分析

小口径弹道炮在使用初期,弹道特性值偏高,影响产品的验收和标准弹的鉴选.该文用膛阻理论解释弹道炮使用的各个时期的弹道特性变化,并介绍了“光膛”射击后,在弹道曲线下降段进行产品验收以及标准弹鉴选中的实际应用.     

中型孔径小梯段露天石方深孔水压爆破

介绍了一种石方开挖新技术－－露天石方深孔水压爆破技术。用试验的方法，通过和常规石方爆破进行类比，从而研究了此项新技术在中型孔径小梯段应用条件下的各种爆破参数，并进行了定性和定量分析，得到了一些初步的结论。     

Pore‐free mold‐pattern‐transfer method for barrier ribs of HD PDPs

Abstract— Among various barrier‐rib manufacturing processes, the mold‐pattern‐transfer method has potential to reduce processing cost as well as the manufacture of high‐resolution pixels. In this study, the effects of major processing variables of the mold‐pattern‐transfer process on the formation of air‐trapped pores within barrier ribs were examined. The results indicated that with an optimum combination of the processing variables, barrier ribs without trapped defects can be produced, demonstrating the possibility of reducing the number of processing steps and costs of barrier ribs.     

ID-based threshold decryption secure against adaptive chosen-ciphertext attack

This paper proposes an identity-based threshold decryption scheme IB-ThDec and reduces its security to the Bilinear Diffie-Hellman problem. Compared with previous work, this conceals two pairing computations in the ciphertext validity verification procedure. The formal proof of security of this scheme is provided in the random oracle model. Additionally, we show that IB-ThDec can be applied to the threshold key escrow and the mediated cryptosystems.     

Discrete Chemical Release From a Microfluidic Chip

We demonstrate a discrete chemical release method, capable of delivering picoliter volumes of chemical solutions with 100 mum of spatial resolution and 20 mus of response time. The releasing mechanism is based on the transfer of pulsed liquid plugs through a hydrophobic air chamber. A microfluidic chip consisting of such a releasing array (2 times 10) is designed and fabricated. Numerical simulation and experimental testing are performed to verify the working principle. Advantages of this release-on-demand technology include leakage-free, fast response and versatile control of release profile. This new method could be a key enabling technology for precisely controlled release of biochemicals for modern pharmacological and biological research.     

Volumetric three‐dimensional up‐conversion display medium

Abstract— Several rare‐earth‐doped fluoride crystals that are excited to emit visible light by sequential two‐photon absorption have been investigated as display‐medium candidates for static volumetric three‐dimensional displays. Dispersion of powders of these materials in a refractive‐index‐matched polymer is reported because such a medium may result in a scalable display. The scattering problem in such a medium is greatly reduced by index‐matching the polymer to the crystalline particles. An index‐matching condition that optimizes the performance is identified.     

噻二唑二聚物/丁氧基三乙二醇复合物的合成

合成了噻二唑二聚物/丁氧基三乙二醇复合物。反应物的摩尔比及反应温度影响产物作为添加剂加入到润滑脂中的抗烧结性能。在最佳反应条件下,即n(噻二唑二聚物)∶n(丁氧基三乙二醇)=0.5∶1.0,反应温度125℃时,产率为85%。通过分子模拟、红外光谱、13C核磁共振及N、S元素的含量测定,探讨了产物的结构及反应机理。结果表明,噻二唑二聚物与丁氧基三乙二醇的摩尔比越大,在金属表面形成配位的噻二唑环的个数就越多,就会表现出更强的吸附特性,从而表现出更高的抗烧结性能。