泥土中微量六氯环戊二烯的气相色谱分析

采用SE 3 0为固定液进行色谱柱分离 ,用外标定量法测定泥土中的微量六氯环戊二烯 ,结果最小检知量为 0 .18× 10 - 6 ,相关系数为 0 .99992。     

负载Pd的分子筛催化剂上烷烃的异构化反应

采用吡啶吸附红外光谱和氨程序升温脱附法对负载Pd的几种分子筛催化剂(Pd/,βPd/ZSM-22,Pd/SAPO-11)的表面酸性进行了测定,并以正十二烷为模型化合物,在连续流动固定床微型反应器上考察了这几种分子筛催化剂的异构化反应性能。实验结果表明,Pd/β催化剂的酸量大且具有强酸中心;Pd/SAPO-11和Pd/ZSM-22催化剂的酸强度分布类似,但前者的酸量较小,后者的酸量适中。在正十二烷的转化率为65%左右时,对于单、双甲基C12异构体的选择性,Pd/ZSM-22催化剂与Pd/SAPO-11催化剂相近,高于Pd/β催化剂,而催化活性的高低顺序为:Pd/β>Pd/ZSM-22>Pd/SAPO-11,说明Pd/ZSM-22催化剂比较适合于大分子烷烃的异构化反应。在100mL中试装置上,以大庆减四线糠醛精制油为原料,对实验结果进行了验证。     

Bias-temperature instabilities of polysilicon gate HfO/sub 2/ MOSFETs

Bias-temperature instabilities (BTI) of HfO/sub 2/ metal oxide semiconductor field effect transistors (MOSFETs) have been systematically studied for the first time. NMOS positive BTI (PBTI) exhibited a more significant V/sub t/ instability than that of PMOS negative BTI (NBTI), and limited the lifetime of HfO/sub 2/ MOSFETs. Although high-temperature forming gas annealing (HT-FGA) improved the interface quality by passivating the interfacial states with hydrogen, BTI behaviors were not strongly affected by the technique. Charge pumping measurements were extensively used to investigate the nature of the BTI degradation, and it was found that V/sub t/ degradation of NMOS PBTI was primarily caused by charge trapping in bulk HfO/sub 2/ rather than interfacial degradation. Deuterium (D/sub 2/) annealing was found to be an excellent technique to improve BTI immunity as well as to enhance the mobility of HfO/sub 2/ MOSFETs.     

IEEE802.11g研究综述

全面介绍了IEEE802.11g标准的WLAN，详细讲述了IEEE802.11g草案标准的概念、特点、构件及体系结构、发展前景等，并探讨了实现IEEE802.11g WLAN所需的几项关键技术，同时分析了IEEE802.11g标准的网络性能。其关键技术包括直序列扩频调制技术及补码键控技术，包二进制卷积，正交频分复用技术等。有关IEEE802.11g的兼容性，同频共存性，自身的OFDM问题分析将成为研究的热点。     

东营凹陷南斜坡储集层成岩作用及对储集性能的影响

东营凹陷南斜坡孔店组岩石类型以岩屑长石砂岩为主 ,长石砂岩和岩屑砂岩次之 ,其中岩屑长石砂岩含量超过 90 %。砂岩成岩作用包括压实作用、胶结作用、溶蚀作用、交代作用等 ,其中胶结作用使储层原生孔隙迅速变差 ,而溶蚀作用是次生空隙发育的主要因素。孔店组砂岩成岩作用进入晚成岩A期 ,期间经历了早成岩A期、B期。影响成岩作用的主要因素为构造演化背景、岩石成分、沉积环境、孔隙流体性质等。     

Measurement of gain spectrum for Fabry-Perot semiconductor lasers by the Fourier transform method with a deconvolution process

To improve the accuracy of measured gain spectra, which is usually limited by the resolution of the optical spectrum analyzer (OSA), a deconvolution process based on the measured spectrum of a narrow linewidth semiconductor laser is applied in the Fourier transform method. The numerical simulation shows that practical gain spectra can be resumed by the Fourier transform method with the deconvolution process. Taking the OSA resolution to be 0.06, 0.1, and 0.2 nm, the gain-reflectivity product spectra with the difference of about 2% are obtained for a 1550-nm semiconductor laser with the cavity length of 720 /spl mu/m. The spectra obtained by the Fourier transform method without the deconvolution process and the Hakki-Paoli method are presented and compared. The simulation also shows that the Fourier transform method has less sensitivity to noise than the Hakki-Paoli method.     

银铜复合电触点复合强度检测方法的讨论

贵金属及其合金铆钉型复合电触点除了应考核其冷态复合强度之外，还必须增加在热态下复合强度的考核，只有这样才能满足用户在产际运行时对复合触点复合强度的要求。     

Vibration control of a flexible structure using a hybrid mount

This paper presents vibration control of a flexible beam structure using a hybrid mount which consists of elastic rubber and piezoelectric stack actuator. After identifying stiffness and damping properties of the rubber and piezoelectric elements, a mechanical model of the hybrid mount is established. The mount model is then incorporated with the beam structure, and the governing equation of motion is obtained in a state space. A sliding mode controller is designed in order to actively attenuate the vibration of the beam structure subjected to high-frequency and small magnitude excitations. The controller is experimentally realized and measured control responses such as acceleration of the beam structure and force transmission through the hybrid mount are evaluated and presented in both frequency and time domains.