Preparation of cross-sectional specimens of ceramic thermal barrier coatings for transmission electron microscopy

During the microstructural examination of ceramic thermal barrier coatings by transmission electron microscopy (TEM), initial efforts for the preparation of cross-sectional thin foils from interface regions by conventional means were mostly failures. Delamination of the Y₂O₃-stabilized ZrO₂ ceramic coating from the nickel-base alloy substrate sometimes occurred during fine polishing at around 80 μm thickness but mostly occurred during dimpling. Because of this sensitivity, special techniques for mechanical handling were developed so that ion milling could give thin enough regions of the metal-ceramic interface. TEM showed convincingly that the highly fragile nature of the coatings is in fact due to the extensive porosity at the interface developed as a result of heat treatment.     

3-D shape modeling for hearing aid design [Applications Corner]

Advances in 3-D scanning and fabrication hardware as well as 3-D geometric design software have transformed a once laborintensive manual manufacturing into an efficient digital process for hearing aid design, resulting in higher quality, reduced cost, and better fitting devices. Future work in this field will continue to focus on increasing automation until the process is fully automatic.     

Shape-driven segmentation of the arterial wall in intravascular ultrasound images

Segmentation of arterial wall boundaries from intravascular images is an important problem for many applications in the study of plaque characteristics, mechanical properties of the arterial wall, its 3-D reconstruction, and its measurements such as lumen size, lumen radius, and wall radius. We present a shape-driven approach to segmentation of the arterial wall from intravascular ultrasound images in the rectangular domain. In a properly built shape space using training data, we constrain the lumen and media-adventitia contours to a smooth, closed geometry, which increases the segmentation quality without any tradeoff with a regularizer term. In addition to a shape prior, we utilize an intensity prior through a nonparametric probability-density-based image energy, with global image measurements rather than pointwise measurements used in previous methods. Furthermore, a detection step is included to address the challenges introduced to the segmentation process by side branches and calcifications. All these features greatly enhance our segmentation method. The tests of our algorithm on a large dataset demonstrate the effectiveness of our approach.     

Surface Characterization of Mild Steel During Atmospheric Corrosion After Being Treated by Sodium Dihydrogen Orthophosphate

Protection of Metals and Physical Chemistry of Surfaces - The objective of this study was to characterize the surfaces of the steel products produced locally during their exposure to the industrial...     

Jacobian Coordinates on Genus 2 Curves

This paper presents a new projective coordinate system and new explicit algorithms which together boost the speed of arithmetic in the divisor class group of genus 2 curves. The proposed formulas generalize the use of Jacobian coordinates on elliptic curves, and their application improves the speed of performing cryptographic scalar multiplications in Jacobians of genus 2 curves over prime fields by an approximate factor of 1.25x. For example, on a single core of an Intel Core i7-3770 (Ivy Bridge), we show that replacing the previous best formulas with our new set improves the cost of generic scalar multiplications from 239,000 to 192,000 cycles and drops the cost of specialized GLV-style scalar multiplications from 155,000 to 123,000 cycles.     

The Production of Low-Alcohol Wines by Aerobic Yeasts

Aerobic yeasts of the genera Pichia and Williopis are commonly regarded as spoilage yeasts of beer and wine by causing turbidity, a surface film of yeast growth and often an excessive estery flavour. However, their ability to utilise sugars oxidatively for cell growth with the production of estery and other flavours of wine with only minimal production of ethanol suggests a method for the production of low-alcohol wines of pleasant “fermented” flavour without the need for additional equipment to remove alcohol by dialysis, reverse osmosis or distillation, or without the excessive sweetness remaining from arrested fermentation. Three strains of Pichia and one of Williopsis were examined for their ability to produce approximately 3%(v/v) ethanol and a good estery and fruity flavour. With normal anaerobic fermentation conditions, or with gentle stirring to prevent formation of a surface film, excessive amounts of alcohol were produced from grape juice of 15% or 20% (w/v) initial sugar concentration. However, an acceptably flavoured wine of alcohol content < 3% was produced by agitation and aeration during fermentation. The ethanol formed in the early stages of culture was oxidised to a final level < 3%, with the production of cell mass and an acceptable flavour.     

The Manavgat Project of Turkey: Water,an Economic Good

In spite of the fact that abundance of water creates problems and sometimes disasters, much of the problem with water lies with its scarcity. Water shortages in a region occur mainly for two reasons. The most important one is associated with climatic conditions, whereas the other has to do with the fact that the location of the water resource does not coincide with where it is needed. This is where engineering and technology come into play along with a handsome amount of capital requirement. As is the case for almost all engineering projects, project economy entails both technical and economic feasibility, which in turn requires that water should be treated as an economic commodity.     

Treatment of non-resectable pelvic malignancies by isolated pelvic perfusion. A preliminary study

Management of non-resectable pelvic tumours by intra-arterial local chemotherapy was shown to be beneficial but systemic toxicity limits its use. To overcome this problem isolated pelvic perfusion (IPP) was introduced as an alternative. This study summarizes our preliminary experience with IPP in the treatment of 18 non-resectable pelvic tumours [recurrent rectal adenocarcinoma (six), soft tissue sarcoma (STS) (five), bone tumour (three), epidermoid carcinoma (two), prostatic adenocarcinoma (one), malignant melanoma (one)]. Results of IPP were regarded as complete remission (CR), partial remission (PR), stable disease (SD) and disease progression (DP) according to the changes in three parameters including; scoring in pain, tumour marker and tumour size measurements. Complete and partial remission were established in five (27%) and seven (39%) patients respectively indicating a benefit ratio of 66%. Objective pain relief was encountered in 53% of the cases. All patients with STS had undergone further surgical treatment after IPP with successful curative resections in four. No residual tumour was found at the laparotomy of the fifth patient. Presenting symptom of the prostatic adenocarcinoma patient was symptomatic hypoglycaemia which resolved completely after IPP. To our knowledge, this represents the first case reported in the English literature in whom tumour related hypoglycaemia was successfully managed by IPP. In conclusion; management of non-resectable pelvic tumours by IPP seems to offer serious palliation and increase in the quality of life without any systemic toxicity. Our preliminary experience suggests even resectability may be achieved in a number of patients especially in those with STS.     

Mechanical properties and morphology of nylon‐6 hybrid composites

In this investigation, the influence of filler type and filler content on the mechanical properties of nylon‐6 is investigated. The mineral fillers were selected on the basis of their shape and size: flake‐like kaolin and talc, spherical glass beads or fibrous wollastonite. These fillers were added to nylon‐6 individually or in mixed combinations. They were added at different percentages varying between 10 and 30% w/w. Samples of the composites were prepared by the injection moulding process. Uniaxial tensile, Izod impact and flexural tests were carried out. Tensile strength, elongation at break, modulus of elasticity and impact energy were obtained and compared. In case of single fillers the results showed that the tensile strength, modulus of elasticity and their flexural values for nylon‐6 composite improve with the increase in filler content while mixed compounds showed no significant changes above 15% + 15% w/w filler. However, for single and mixed filler up to 10% w/w, the impact strength and maximum elongation at break showed significant decrease. In general, the maximum improvement in mechanical the addition of 10–15% w/w filler. Copyright © 2003 Society of Chemical Industry     

Thermo‐economic optimization of superheating and sub‐cooling heat exchangers in vapor‐compressed refrigeration system

In this study, superheating and sub‐cooling heat exchangers in vapor‐compressed refrigeration system are analyzed from thermodynamics and economical (refrigeration system operation cost, investment cost) viewpoints. Using four different refrigerants (R22, R502, R134a and R404a), the temperature of condenser at the interval of (35–55°C) and temperature of evaporator at the interval of (?10 to 10°C) have been obtained from the calculation process. The second law analysis (analysis of irreversibility) of a refrigeration system is carried out and then the whole system is optimized thermo‐economically. As a result of calculations, optimum superheating and sub‐cooling temperatures of heat exchanger (superheating, sub‐cooling) areas corresponding to these temperatures are obtained. Copyright © 2007 John Wiley & Sons, Ltd.