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81.
M. Nikolo X. Shi E. S. Choi J. Jiang J. D. Weiss E. E. Hellstrom 《Journal of Superconductivity and Novel Magnetism》2014,27(10):2231-2239
Thermally assisted flux flow (TAFF) based on magneto-resistivity and ac susceptibility measurements is studied in a Ba(Fe0.91Co0.09)2As2(T c=25.3 K) sample in magnetic fields up to 18 T. In addition to the upper critical field μ 0 H c2 and the coherence length ξ(0), the flux flow activation energy U(T,H) has also been determined. The resistive transition width is proportional to μ 0 H, in contrast to Tinkham’s theoretical prediction. By applying Fisher’s model, the glass melting transition temperature T g, which occurs in the upper TAFF state and not in the zero resistivity vortex solid regime, is calculated. The onset of TAFF temperature and the crossover temperature T x from TAFF to flux flow are determined. By contrasting the ac susceptibility data with the resistivity data, considerable flux penetration appears even in the zero resistivity state, in addition to ac losses. The H-T phase diagram is drawn and shows weak pinning regime as the field approaches μ 0 H c2, and the strength of the weak pinning decreases to 0 with increasing magnetic field from 0 to 18 T. 相似文献
82.
Efficient Total Chemical Synthesis of 13C=18O Isotopomers of Human Insulin for Isotope‐Edited FTIR
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Dr. Balamurugan Dhayalan Dr. Ann Fitzpatrick Dr. Kalyaneswar Mandal Dr. Jonathan Whittaker Prof. Dr. Michael A. Weiss Prof. Dr. Andrei Tokmakoff Prof. Dr. Stephen B. H. Kent 《Chembiochem : a European journal of chemical biology》2016,17(5):415-420
Isotope‐edited two‐dimensional Fourier transform infrared spectroscopy (2 D FTIR) can potentially provide a unique probe of protein structure and dynamics. However, general methods for the site‐specific incorporation of stable 13C=18O labels into the polypeptide backbone of the protein molecule have not yet been established. Here we describe, as a prototype for the incorporation of specific arrays of isotope labels, the total chemical synthesis—via a key ester insulin intermediate—of 97 % enriched [(1‐13C=18O)PheB24] human insulin: stable‐isotope labeled at a single backbone amide carbonyl. The amino acid sequence as well as the positions of the disulfide bonds and the correctly folded structure were unambiguously confirmed by the X‐ray crystal structure of the synthetic protein molecule. In vitro assays of the isotope labeled [(1‐13C=18O)PheB24] human insulin showed that it had full insulin receptor binding activity. Linear and 2 D IR spectra revealed a distinct red‐shifted amide I carbonyl band peak at 1595 cm?1 resulting from the (1‐13C=18O)PheB24 backbone label. This work illustrates the utility of chemical synthesis to enable the application of advanced physical methods for the elucidation of the molecular basis of protein function. 相似文献
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Christian Gaber David Jocham Hannes Alois Weiss Ole Böttcher Wolfram Volk 《International Journal of Material Forming》2017,10(3):345-351
The prediction of formability is one of the most important tasks in sheet metal forming process simulation. The common criterion for ductile fracture in industrial applications is the Forming Limit Diagram (FLD). This is only applicable for linear strain paths. However, in most industrial simulation cases non-linear strain paths occur. To resolve this problem, a phenomenological approach is introduced, the so-called Generalized Forming Limit Concept (GFLC). The GFLC enables prediction of localized necking on arbitrary non-linear strain paths. Another possibility is the use of the Time Dependent Evaluation Method (TDEM) within the simulation as a failure criteria. During the Numisheet Benchmark 1 (2014) a two-stage forming process was performed with three typical sheet materials (AA5182, DP600 and TRIP 780) and three different blank shapes. The task was to determinate the point in time and space of local instability. Therefore the strain path for the point of maximum local thinning is evaluated. To predict the start of local necking the Generalized Forming Limit Concept (GFLC), the Time Dependent Evaluation Method (TDEM) and the modified TDEM were applied. The results of the simulation are compared with the results of the Benchmark experiment. 相似文献
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G. Weiss 《International journal of control》2013,86(15):1174-1181
We study the possibility of nullifying time-varying systems with memoryless output feedback. The systems we examine are discrete-time linear single-input single-output finite-dimensional time-varying systems. For generic completely controllable and completely observable discrete-time systems, we show that any state at any time can be steered to the origin within finite time. An algorithm for nullification and an upper bound for nullification time, depending only on the system's dimension, are provided. The algorithm is described using a representation of the system in time-varying controller canonical form. We verify that every completely controllable system has such a representation. 相似文献
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Sholom M. Weiss Amit Dhurandhar Robert J. Baseman Brian F. White Ronald Logan Jonathan K. Winslow Daniel Poindexter 《Journal of Intelligent Manufacturing》2016,27(4):751-763
We describe methods for continual prediction of manufactured product quality prior to final testing. In our most expansive modeling approach, an estimated final characteristic of a product is updated after each manufacturing operation. Our initial application is for the manufacture of microprocessors, and we predict final microprocessor speed. Using these predictions, early corrective manufacturing actions may be taken to increase the speed of expected slow wafers (a collection of microprocessors) or reduce the speed of fast wafers. Such predictions may also be used to initiate corrective supply chain management actions. Developing statistical learning models for this task has many complicating factors: (a) a temporally unstable population (b) missing data that is a result of sparsely sampled measurements and (c) relatively few available measurements prior to corrective action opportunities. In a real manufacturing pilot application, our automated models selected 125 fast wafers in real-time. As predicted, those wafers were significantly faster than average. During manufacture, downstream corrective processing restored 25 nominally unacceptable wafers to normal operation. 相似文献
90.
Zohar Bloom-Ackermann Hadas Ganin Ilana Kolodkin-Gal 《Israel journal of chemistry》2016,56(5):302-309
Quorum sensing (QS) is an efficient mode of intercellular communication between bacteria. This mode is regulated by self-produced small chemical signals, activating dedicated receptors once accumulated. Numerous architecturally complex QS cascades are cardinal for governing bacterial behaviors, such as pathogenicity, luminescence, and bacterial competence. Importantly, QS cascades are essential for the formation of bacterial multicellular communities. Once informed via QS cascades, motile cells often organize themselves into conspicuous multicellular structures that carry out specialized tasks. This review focuses on the major QS systems, playing an active role in the rise of complex bacterial communities in different bacterial models. 相似文献